DTA measure 14program Test Date: 20231018:1420 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1274.29 s Mass = 1402.200 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.0730 -1.5792 271.2764 272.8556 263.9645 1.8920 -1.5809 271.3078 272.8887 263.9631 2.6830 -1.5819 271.3229 272.9047 263.9683 3.4740 -1.5886 271.3373 272.9259 263.9673 4.3255 -1.5944 271.3641 272.9585 263.9873 5.0875 -1.5969 271.3895 272.9864 263.9799 5.9098 -1.5996 271.4089 273.0084 263.9971 6.7015 -1.6004 271.4285 273.0289 264.0036 7.4935 -1.6048 271.4392 273.0440 264.0263 8.3455 -1.6063 271.4746 273.0809 264.0379 9.1075 -1.6021 271.5003 273.1024 264.0599 9.9295 -1.6033 271.5184 273.1218 264.0740 10.7215 -1.6039 271.5360 273.1398 264.0770 11.5135 -1.6062 271.5530 273.1592 264.0981 12.3655 -1.6075 271.5741 273.1817 264.1493 13.1275 -1.6087 271.6022 273.2109 264.1934 13.9495 -1.6088 271.6176 273.2264 264.2163 14.7415 -1.6090 271.6289 273.2379 264.2612 15.5335 -1.6131 271.6707 273.2838 264.3052 16.3855 -1.6132 271.6902 273.3034 264.3582 17.1475 -1.6171 271.6867 273.3039 264.4072 17.9695 -1.6183 271.7113 273.3296 264.4748 18.7615 -1.6204 271.7285 273.3489 264.5345 19.5530 -1.6256 271.7426 273.3681 264.5952 20.4050 -1.6286 271.7623 273.3909 264.6829 21.1668 -1.6318 271.7946 273.4264 264.7449 21.9895 -1.6384 271.8253 273.4636 264.8259 22.7820 -1.6469 271.8330 273.4799 264.9107 23.5735 -1.6478 271.8471 273.4949 264.9763 24.4260 -1.6496 271.8667 273.5163 265.0604 25.1878 -1.6514 271.8794 273.5308 265.1568 26.0098 -1.6546 271.8879 273.5425 265.2643 26.7993 -1.6532 271.9310 273.5842 265.3551 27.5900 -1.6574 271.9455 273.6029 265.4392 28.4080 -1.6603 271.9653 273.6257 265.5321 29.1960 -1.6636 271.9882 273.6517 265.6403 30.0140 -1.6656 271.9996 273.6652 265.7467 30.8020 -1.6694 272.0343 273.7037 265.8449 31.5900 -1.6722 272.0491 273.7213 265.9200 32.4080 -1.6742 272.0640 273.7382 266.0310 33.1968 -1.6747 272.0860 273.7607 266.1410 34.0170 -1.6773 272.0959 273.7731 266.2473 34.8058 -1.6801 272.1251 273.8052 266.3483 35.5950 -1.6866 272.1727 273.8593 266.4411 36.4460 -1.6889 272.1720 273.8609 266.5603 37.2078 -1.6926 272.2010 273.8935 266.6541 38.0298 -1.6981 272.2313 273.9295 266.7509 38.8233 -1.6957 272.2407 273.9364 266.8577 39.6155 -1.6974 272.2640 273.9614 266.9671 40.4380 -1.6947 272.2797 273.9744 267.0742 41.2298 -1.6965 272.2987 273.9952 267.1682 42.0518 -1.6995 272.3278 274.0273 267.2730 42.8440 -1.7049 272.3549 274.0598 267.3759 43.6355 -1.7095 272.3684 274.0780 267.4776 44.4580 -1.7131 272.3922 274.1053 267.5904 45.2495 -1.7096 272.4149 274.1245 267.6859 46.0718 -1.7138 272.4502 274.1640 267.7867 46.8653 -1.7174 272.4810 274.1984 267.9023 47.6608 -1.7186 272.4841 274.2027 268.0060 48.4890 -1.7186 272.4967 274.2153 268.1040 49.2540 -1.7205 272.5295 274.2500 268.2095 50.1075 -1.7274 272.5626 274.2900 268.3202 50.8695 -1.7313 272.5859 274.3172 268.4333 51.6915 -1.7359 272.6168 274.3526 268.5357 52.4835 -1.7351 272.6437 274.3789 268.6388 53.2755 -1.7394 272.6813 274.4208 268.7336 54.1280 -1.7396 272.6993 274.4389 268.8534 54.8905 -1.7404 272.7381 274.4785 268.9526 55.7125 -1.7443 272.7477 274.4920 269.0548 56.5045 -1.7485 272.7733 274.5217 269.1440 57.2960 -1.7512 272.7923 274.5435 269.2418 58.1480 -1.7536 272.8239 274.5775 269.3536 58.9100 -1.7566 272.8555 274.6122 269.4566 59.7303 -1.7610 272.8873 274.6482 269.5580 60.5175 -1.7644 272.9126 274.6770 269.6662 61.3060 -1.7664 272.9284 274.6947 269.7641 62.1243 -1.7654 272.9634 274.7289 269.8693 62.9135 -1.7677 272.9892 274.7569 269.9938 63.7310 -1.7697 273.0077 274.7774 270.1039 64.5195 -1.7708 273.0300 274.8008 270.2063 65.3070 -1.7712 273.0825 274.8537 270.3182 66.1260 -1.7746 273.0971 274.8717 270.4145 66.9160 -1.7771 273.1367 274.9138 270.5352 67.7363 -1.7759 273.1650 274.9409 270.6492 68.5253 -1.7781 273.1912 274.9693 270.7482 69.3158 -1.7831 273.2201 275.0032 270.8529 70.1375 -1.7895 273.2459 275.0355 270.9742 70.9295 -1.7924 273.2894 275.0819 271.0653 71.7508 -1.7922 273.3118 275.1039 271.1805 72.5435 -1.7879 273.3509 275.1388 271.2989 73.3345 -1.7882 273.3731 275.1613 271.3965 74.1583 -1.7936 273.4044 275.1980 271.5034 74.9220 -1.7961 273.4434 275.2395 271.6128 75.7743 -1.7969 273.4747 275.2716 271.7337 76.5363 -1.7990 273.5001 275.2991 271.8426 77.3580 -1.8001 273.5304 275.3305 271.9482 78.1803 -1.8033 273.5670 275.3703 272.0368 78.9415 -1.8031 273.6038 275.4068 272.1269 79.7940 -1.8085 273.6473 275.4558 272.2549 80.5573 -1.8104 273.6778 275.4882 272.3468 81.3808 -1.8115 273.7070 275.5185 272.4647 82.2030 -1.8170 273.7356 275.5526 272.5682 82.9645 -1.8216 273.7701 275.5917 272.6640 83.8173 -1.8233 273.8167 275.6399 272.7816 84.5918 -1.8232 273.8585 275.6817 272.8649 85.4148 -1.8275 273.9111 275.7386 272.9842 86.2075 -1.8340 273.9263 275.7604 273.0691 86.9995 -1.8365 273.9563 275.7928 273.1792 87.8215 -1.8409 273.9955 275.8364 273.2891 88.6135 -1.8332 274.0236 275.8568 273.4024 89.4355 -1.8290 274.0793 275.9083 273.4834 90.2275 -1.8309 274.1118 275.9426 273.5817 91.0205 -1.8354 274.1424 275.9778 273.6808 91.8378 -1.8359 274.2098 276.0457 273.7843 92.6245 -1.8416 274.2399 276.0816 273.8599 93.4440 -1.8467 274.2687 276.1154 273.9633 94.2323 -1.8475 274.3123 276.1598 274.0683 95.0210 -1.8453 274.3475 276.1927 274.1749 95.8393 -1.8506 274.3861 276.2367 274.2778 96.6280 -1.8585 274.4243 276.2828 274.3736 97.4468 -1.8592 274.4566 276.3158 274.4726 98.2355 -1.8567 274.5080 276.3647 274.5664 99.0258 -1.8551 274.5487 276.4038 274.6683 99.8775 -1.8545 274.5871 276.4415 274.7582 100.6395 -1.8542 274.6319 276.4862 274.8451 101.4615 -1.8557 274.6698 276.5255 274.9422 102.2535 -1.8570 274.7192 276.5762 275.0245 103.0455 -1.8561 274.7571 276.6132 275.1231 103.8675 -1.8567 274.8024 276.6591 275.2110 104.6450 -1.8625 274.8381 276.7006 275.2935 105.4835 -1.8644 274.8829 276.7473 275.4063 106.2455 -1.8657 274.9231 276.7888 275.4842 107.0975 -1.8656 274.9748 276.8404 275.5907 107.8895 -1.8687 275.0211 276.8898 275.6741 108.6815 -1.8699 275.0673 276.9372 275.7731 109.5035 -1.8758 275.1211 276.9968 275.8636 110.2655 -1.8751 275.1506 277.0257 275.9506 111.1175 -1.8780 275.1868 277.0648 276.0412 111.9095 -1.8798 275.2281 277.1080 276.1349 112.7013 -1.8787 275.2725 277.1512 276.2237 113.5235 -1.8802 275.3360 277.2162 276.3022 114.2855 -1.8803 275.3811 277.2614 276.3965 115.1370 -1.8824 275.4357 277.3181 276.4861 115.9290 -1.8842 275.4710 277.3552 276.6054 116.7215 -1.8843 275.5179 277.4022 276.6953 117.5440 -1.8839 275.5641 277.4480 276.7796 118.3358 -1.8832 275.6132 277.4963 276.8773 119.1578 -1.8843 275.6627 277.5471 276.9767 119.9500 -1.8823 275.7173 277.5996 277.0815 120.7425 -1.8825 275.7665 277.6490 277.1841 121.5650 -1.8805 275.8203 277.7008 277.2858 122.3565 -1.8755 275.8591 277.7347 277.4052 123.1788 -1.8756 275.9094 277.7850 277.4969 123.9670 -1.8766 275.9602 277.8368 277.5807 124.7560 -1.8773 276.0030 277.8803 277.6860 125.5745 -1.8766 276.0695 277.9462 277.8037 126.3330 -1.8753 276.1175 277.9928 277.9075 127.1815 -1.8757 276.1720 278.0477 278.0007 127.9705 -1.8748 276.2100 278.0849 278.0809 128.7600 -1.8728 276.2732 278.1460 278.1795 129.5788 -1.8706 276.3182 278.1888 278.2907 130.3680 -1.8731 276.3725 278.2456 278.3852 131.1875 -1.8731 276.4248 278.2979 278.4881 131.9780 -1.8750 276.4776 278.3526 278.5922 132.7695 -1.8767 276.5291 278.4059 278.6983 133.5920 -1.8778 276.5843 278.4620 278.8097 134.3535 -1.8803 276.6302 278.5105 278.8961 135.2108 -1.8785 276.6871 278.5656 278.9938 135.9728 -1.8775 276.7473 278.6249 279.0753 136.7948 -1.8793 276.7897 278.6691 279.1664 137.6170 -1.8803 276.8514 278.7318 279.2706 138.3785 -1.8805 276.8998 278.7804 279.3764 139.2310 -1.8788 276.9678 278.8466 279.4996 139.9928 -1.8815 277.0156 278.8971 279.5688 140.8145 -1.8806 277.0758 278.9564 279.6780 141.6373 -1.8828 277.1236 279.0064 279.7808 142.3995 -1.8832 277.1890 279.0723 279.8605 143.2515 -1.8818 277.2529 279.1347 279.9602 144.0135 -1.8776 277.3038 279.1814 280.0575 144.8355 -1.8770 277.3389 279.2159 280.1631 145.6578 -1.8766 277.3950 279.2717 280.2682 146.4205 -1.8842 277.4588 279.3430 280.3611 147.2725 -1.8815 277.5246 279.4061 280.5043 148.0345 -1.8791 277.5819 279.4610 280.5859 148.8565 -1.8788 277.6433 279.5221 280.6868 149.6785 -1.8801 277.6935 279.5736 280.8030 150.4405 -1.8826 277.7564 279.6390 280.9059 151.2930 -1.8818 277.8089 279.6906 281.0227 152.0555 -1.8805 277.8668 279.7473 281.1244 152.8770 -1.8794 277.9346 279.8140 281.2414 153.6993 -1.8786 278.0174 279.8961 281.3678 154.4605 -1.8795 278.0789 279.9584 281.4651 155.3130 -1.8797 278.1166 279.9962 281.5819 156.0710 -1.8801 278.1742 280.0543 281.6944 156.8890 -1.8816 278.2324 280.1140 281.8048 157.7078 -1.8802 278.2887 280.1689 281.9288 158.4660 -1.8794 278.3523 280.2317 282.0365 159.3153 -1.8775 278.4294 280.3069 282.1558 160.0740 -1.8767 278.4666 280.3433 282.2673 160.8918 -1.8810 278.5234 280.4044 282.3705 161.7103 -1.8864 278.5962 280.4827 282.4921 162.4705 -1.8859 278.6591 280.5451 282.5926 163.3198 -1.8845 278.7365 280.6210 282.7319 164.0790 -1.8861 278.7834 280.6695 282.8274 164.9005 -1.8893 278.8442 280.7335 282.9355 165.7225 -1.8869 278.9112 280.7981 283.0485 166.4840 -1.8864 278.9786 280.8650 283.1593 167.3373 -1.8870 279.0567 280.9437 283.2707 168.0990 -1.8867 279.1138 281.0005 283.3860 168.9208 -1.8863 279.1707 281.0570 283.5071 169.7133 -1.8860 279.2312 281.1171 283.6172 170.5045 -1.8846 279.2788 281.1635 283.7206 171.3573 -1.8844 279.3593 281.2437 283.8369 172.1190 -1.8840 279.4267 281.3106 283.9431 172.9408 -1.8825 279.4908 281.3732 284.0549 173.7640 -1.8822 279.5462 281.4284 284.1699 174.5258 -1.8729 279.6122 281.4851 284.2659 175.3780 -1.8707 279.6967 281.5674 284.3792 176.1700 -1.8726 279.7542 281.6268 284.4829 176.9615 -1.8788 279.8413 281.7201 284.5786 177.7838 -1.8859 279.8927 281.7786 284.6759 178.5755 -1.8868 279.9627 281.8495 284.7804 179.3978 -1.8873 280.0240 281.9113 284.8877 180.1898 -1.8885 280.0985 281.9870 284.9649 180.9815 -1.8901 280.1700 282.0601 285.0674 181.8038 -1.8900 280.2362 282.1262 285.1561 182.5955 -1.8896 280.3019 282.1915 285.2408 183.4185 -1.8913 280.3863 282.2776 285.3440 184.2105 -1.8906 280.4539 282.3445 285.4225 185.0030 -1.8888 280.5159 282.4046 285.5078 185.8258 -1.8883 280.5946 282.4830 285.6102 186.6185 -1.8866 280.6693 282.5560 285.6866 187.4405 -1.8840 280.7232 282.6072 285.7728 188.2325 -1.8862 280.7949 282.6811 285.8711 189.0218 -1.8874 280.8752 282.7626 285.9518 189.8700 -1.8834 280.9202 282.8036 286.0546 190.6283 -1.8839 280.9925 282.8763 286.1388 191.4478 -1.8848 281.0854 282.9702 286.2270 192.2360 -1.8835 281.1601 283.0436 286.3223 193.0240 -1.8838 281.2183 283.1021 286.4073 193.8720 -1.8817 281.3204 283.2021 286.5010 194.6300 -1.8829 281.3751 283.2580 286.6062 195.4490 -1.8827 281.4297 283.3124 286.6985 196.2688 -1.8823 281.4958 283.3782 286.7936 197.0305 -1.8841 281.5666 283.4507 286.8913 197.8825 -1.8859 281.6550 283.5409 286.9850 198.6445 -1.8881 281.7081 283.5962 287.0833 199.4665 -1.8873 281.8091 283.6963 287.1878 200.2585 -1.8852 281.8721 283.7573 287.2819 201.0505 -1.8860 281.9435 283.8295 287.3624 201.9025 -1.8850 282.0294 283.9144 287.4805 202.6645 -1.8850 282.0871 283.9721 287.5900 203.4865 -1.8839 282.1601 284.0440 287.6853 204.2785 -1.8831 282.2531 284.1362 287.7880 205.0705 -1.8827 282.3037 284.1864 287.8573 205.9225 -1.8841 282.4115 284.2956 287.9817 206.6845 -1.8851 282.4650 284.3501 288.0630 207.5063 -1.8854 282.5412 284.4266 288.1478 208.2983 -1.8855 282.6192 284.5047 288.2619 209.0898 -1.8837 282.7002 284.5840 288.3866 209.9423 -1.8842 282.7780 284.6622 288.4873 210.7038 -1.8837 282.8484 284.7321 288.5852 211.5258 -1.8843 282.9208 284.8052 288.6768 212.3180 -1.8856 282.9871 284.8727 288.7906 213.1095 -1.8841 283.0722 284.9563 288.9086 213.9620 -1.8845 283.1503 285.0348 289.0340 214.7238 -1.8838 283.2217 285.1055 289.1374 215.5458 -1.8812 283.3018 285.1830 289.2560 216.3380 -1.8826 283.3728 285.2553 289.3616 217.1308 -1.8808 283.4588 285.3396 289.4680 217.9578 -1.8793 283.5362 285.4155 289.5964 218.7495 -1.8783 283.6145 285.4928 289.7265 219.5725 -1.8798 283.6955 285.5753 289.8566 220.3645 -1.8798 283.7847 285.6645 289.9609 221.1540 -1.8758 283.8528 285.7286 290.0807 221.9720 -1.8781 283.9405 285.8187 290.1890 222.7300 -1.8775 283.9990 285.8765 290.3071 223.5780 -1.8756 284.0799 285.9556 290.4352 224.3663 -1.8764 284.1531 286.0295 290.5521 225.1550 -1.8769 284.2165 286.0934 290.6583 225.9735 -1.8747 284.3123 286.1870 290.7745 226.7328 -1.8738 284.3791 286.2529 290.8766 227.5825 -1.8755 284.4608 286.3363 290.9967 228.3710 -1.8765 284.5533 286.4298 291.0896 229.1603 -1.8770 284.6195 286.4964 291.1916 229.9818 -1.8744 284.7164 286.5908 291.3089 230.7435 -1.8734 284.7902 286.6636 291.4161 231.5958 -1.8751 284.8829 286.7580 291.5071 232.3578 -1.8749 284.9544 286.8293 291.6180 233.1798 -1.8727 285.0357 286.9084 291.7001 234.0018 -1.8728 285.1313 287.0041 291.7865 234.7635 -1.8723 285.2207 287.0929 291.8871 235.6158 -1.8694 285.2929 287.1622 291.9861 236.3775 -1.8726 285.3652 287.2378 292.0506 237.1998 -1.8713 285.4475 287.3188 292.1391 237.9918 -1.8730 285.5301 287.4031 292.2324 238.7835 -1.8733 285.6157 287.4890 292.3069 239.6355 -1.8736 285.7024 287.5760 292.3978 240.3975 -1.8734 285.7789 287.6523 292.4898 241.2195 -1.8737 285.8634 287.7371 292.5863 242.0115 -1.8756 285.9299 287.8055 292.6802 242.8035 -1.8742 286.0279 287.9021 292.7813 243.6555 -1.8731 286.1242 287.9973 292.8933 244.4175 -1.8729 286.1879 288.0607 292.9775 245.2395 -1.8715 286.2641 288.1356 293.0747 246.0315 -1.8710 286.3448 288.2158 293.1788 246.8235 -1.8725 286.4424 288.3149 293.2724 247.6455 -1.8701 286.5356 288.4057 293.3792 248.4368 -1.8692 286.6170 288.4862 293.4875 249.2595 -1.8700 286.7060 288.5760 293.6043 250.0520 -1.8687 286.7854 288.6542 293.6924 250.8445 -1.8687 286.8675 288.7362 293.8021 251.6670 -1.8671 286.9466 288.8137 293.9043 252.4573 -1.8669 287.0281 288.8950 294.0099 253.2770 -1.8676 287.1135 288.9810 294.1334 254.0640 -1.8670 287.1928 289.0598 294.2270 254.8535 -1.8682 287.2856 289.1538 294.3198 255.6718 -1.8697 287.3753 289.2450 294.4281 256.4605 -1.8693 287.4515 289.3208 294.5387 257.2795 -1.8635 287.5399 289.4034 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