DTA measure 1program3 Date: 2024416:113 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 914.69 s Mass = 1304.400 mg data_number = 1138 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.0688 0.4055 225.0697 224.6642 265.7682 1.8908 0.4089 225.3370 224.9281 265.7662 2.7118 0.4101 225.6281 225.2180 265.7704 3.4735 0.4094 225.8705 225.4611 265.7725 4.3258 0.4119 226.1468 225.7349 265.7959 5.1180 0.4138 226.3982 225.9845 265.7950 5.9095 0.4161 226.6638 226.2477 265.8051 6.7318 0.4176 226.9426 226.5250 265.8452 7.4935 0.4177 227.1730 226.7553 265.8756 8.3555 0.4181 227.4708 227.0527 265.9153 9.1255 0.4183 227.7207 227.3024 265.9513 9.9478 0.4164 227.9948 227.5783 266.0175 10.7398 0.4175 228.2309 227.8135 266.0898 11.5315 0.4174 228.4795 228.0621 266.1542 12.3538 0.4195 228.7623 228.3428 266.2226 13.1455 0.4202 229.0072 228.5870 266.3123 13.9678 0.4203 229.2786 228.8583 266.4004 14.7595 0.4212 229.5251 229.1040 266.4942 15.5515 0.4211 229.7550 229.3339 266.5981 16.4035 0.4204 230.0388 229.6184 266.7301 17.1688 0.4194 230.2805 229.8611 266.8691 17.9915 0.4194 230.5408 230.1213 266.9792 18.7835 0.4190 230.7832 230.3642 267.1301 19.5765 0.4180 231.0190 230.6011 267.2895 20.4290 0.4160 231.2845 230.8685 267.4520 21.1915 0.4142 231.5232 231.1090 267.5902 22.0135 0.4152 231.8033 231.3882 267.7522 22.8055 0.4131 232.0479 231.6348 267.9088 23.5943 0.4109 232.2859 231.8750 268.0594 24.4425 0.4115 232.5321 232.1205 268.2374 25.2008 0.4087 232.7619 232.3532 268.4044 26.0185 0.4078 233.0202 232.6124 268.5800 26.8070 0.4068 233.2572 232.8504 268.7307 27.5960 0.4059 233.5103 233.1044 268.9174 28.4440 0.4057 233.7542 233.3485 269.1093 29.2128 0.4040 233.9893 233.5853 269.2658 30.0318 0.4010 234.2268 233.8258 269.4276 30.8203 0.3993 234.4602 234.0610 269.5848 31.6105 0.3956 234.6907 234.2952 269.7374 32.4608 0.3941 234.9503 234.5561 269.9089 33.2218 0.3940 235.1980 234.8040 270.0649 34.0435 0.3910 235.4369 235.0459 270.2199 34.8355 0.3888 235.6665 235.2777 270.3670 35.6275 0.3883 235.8991 235.5108 270.5321 36.4495 0.3863 236.1524 235.7661 270.6705 37.2415 0.3832 236.3777 235.9945 270.8096 38.0635 0.3834 236.6149 236.2315 270.9648 38.8555 0.3793 236.8441 236.4648 271.1116 39.6473 0.3805 237.1052 236.7247 271.2356 40.4693 0.3784 237.3378 236.9594 271.3727 41.2610 0.3732 237.5489 237.1757 271.4942 42.0830 0.3700 237.7852 237.4152 271.6189 42.8753 0.3711 238.0288 237.6577 271.7518 43.6665 0.3675 238.2751 237.9076 271.8839 44.5195 0.3649 238.5168 238.1519 272.0233 45.2815 0.3634 238.7318 238.3684 272.1517 46.1038 0.3608 238.9656 238.6047 272.2951 46.9260 0.3603 239.1951 238.8348 272.4108 47.6885 0.3566 239.4141 239.0575 272.5362 48.5408 0.3541 239.6827 239.3286 272.6684 49.3025 0.3510 239.8853 239.5343 272.7871 50.1248 0.3526 240.1205 239.7679 272.9232 50.9470 0.3495 240.3427 239.9932 273.0543 51.7095 0.3481 240.5539 240.2058 273.1795 52.5628 0.3451 240.7930 240.4479 273.3192 53.3245 0.3424 241.0323 240.6899 273.4377 54.1468 0.3421 241.2650 240.9228 273.5674 54.9685 0.3404 241.4726 241.1322 273.6905 55.7270 0.3387 241.6853 241.3467 273.8000 56.5750 0.3341 241.9396 241.6055 273.9382 57.3330 0.3339 242.1635 241.8296 274.0651 58.1510 0.3282 242.3966 242.0684 274.1999 58.9693 0.3252 242.6181 242.2929 274.3127 59.7318 0.3239 242.8243 242.5004 274.4306 60.5818 0.3213 243.0468 242.7255 274.5788 61.3400 0.3187 243.2635 242.9448 274.6846 62.1593 0.3170 243.5157 243.1987 274.8171 62.9490 0.3137 243.7113 243.3976 274.9389 63.7385 0.3101 243.9198 243.6097 275.0592 64.5885 0.3070 244.1515 243.8446 275.1941 65.3505 0.3081 244.3660 244.0579 275.3075 66.1728 0.3078 244.5911 244.2833 275.4439 66.9648 0.3051 244.8155 244.5103 275.5681 67.7565 0.3050 245.0332 244.7282 275.6936 68.5785 0.3032 245.2400 244.9368 275.7955 69.3405 0.2963 245.4505 245.1542 275.9014 70.1925 0.2982 245.6944 245.3962 276.0316 70.9848 0.2967 245.9171 245.6203 276.1648 71.7765 0.2932 246.1355 245.8423 276.2924 72.5985 0.2899 246.3530 246.0631 276.4443 73.3605 0.2873 246.5618 246.2745 276.5665 74.2125 0.2892 246.7717 246.4825 276.7220 74.9773 0.2858 246.9723 246.6866 276.8452 75.8025 0.2818 247.2075 246.9257 277.0189 76.6245 0.2791 247.4302 247.1511 277.1541 77.3865 0.2772 247.6520 247.3747 277.2737 78.2385 0.2758 247.8638 247.5879 277.4358 79.0005 0.2712 248.0764 247.8052 277.5579 79.8263 0.2691 248.2791 248.0101 277.6931 80.6275 0.2696 248.4827 248.2132 277.8438 81.4205 0.2649 248.6945 248.4297 277.9952 82.2423 0.2646 248.8940 248.6293 278.1466 83.0035 0.2606 249.1115 248.8509 278.2825 83.8560 0.2600 249.3209 249.0609 278.4498 84.6178 0.2555 249.5275 249.2720 278.6025 85.4398 0.2519 249.7419 249.4900 278.7644 86.2620 0.2513 249.9590 249.7077 278.9020 87.0245 0.2484 250.1568 249.9084 279.0439 87.8740 0.2439 250.3789 250.1350 279.1870 88.6323 0.2412 250.5807 250.3395 279.3106 89.4500 0.2370 250.7959 250.5589 279.4499 90.2385 0.2359 251.0025 250.7667 279.5823 91.0275 0.2338 251.2160 250.9822 279.7138 91.8753 0.2305 251.4439 251.2134 279.8556 92.6333 0.2308 251.6276 251.3968 279.9814 93.4523 0.2264 251.8419 251.6155 280.1119 94.2708 0.2250 252.0435 251.8185 280.2459 95.0293 0.2234 252.2412 252.0178 280.3664 95.8790 0.2221 252.4538 252.2317 280.5016 96.6400 0.2187 252.6374 252.4187 280.6170 97.4620 0.2179 252.8437 252.6258 280.7503 98.2543 0.2139 253.0556 252.8417 280.8574 99.0455 0.2100 253.2487 253.0387 280.9983 99.8978 0.2090 253.4588 253.2498 281.1349 100.6598 0.2062 253.6556 253.4494 281.2271 101.4820 0.2032 253.8635 253.6603 281.3515 102.2738 0.2012 254.0722 253.8710 281.4647 103.0655 0.1988 254.2588 254.0599 281.5949 103.8880 0.1975 254.4641 254.2665 281.7286 104.6795 0.1963 254.6631 254.4668 281.8488 105.5018 0.1946 254.8655 254.6709 281.9596 106.2938 0.1916 255.0609 254.8693 282.0812 107.0855 0.1910 255.2716 255.0806 282.2090 107.9090 0.1879 255.4936 255.3057 282.3488 108.6715 0.1852 255.6865 255.5012 282.4545 109.5238 0.1823 255.8709 255.6886 282.5911 110.3158 0.1797 256.0681 255.8885 282.7299 111.1218 0.1792 256.2682 256.0890 282.8515 111.9138 0.1764 256.4748 256.2984 282.9729 112.7055 0.1710 256.6642 256.4931 283.1276 113.5575 0.1708 256.8773 256.7065 283.2521 114.3195 0.1671 257.0611 256.8940 283.3899 115.1415 0.1656 257.2720 257.1064 283.5276 115.9335 0.1634 257.4542 257.2908 283.6623 116.7265 0.1613 257.6374 257.4761 283.8022 117.5790 0.1589 257.8641 257.7052 283.9549 118.3415 0.1536 258.0343 257.8807 284.0929 119.1635 0.1507 258.2395 258.0888 284.2323 119.9553 0.1502 258.4396 258.2894 284.3785 120.7440 0.1481 258.6295 258.4814 284.5080 121.5725 0.1477 258.8351 258.6873 284.6568 122.3308 0.1466 259.0110 258.8644 284.7983 123.1795 0.1440 259.2011 259.0571 284.9551 123.9680 0.1412 259.4057 259.2646 285.0831 124.7570 0.1393 259.6057 259.4665 285.2168 125.5750 0.1365 259.8057 259.6692 285.3731 126.3630 0.1342 259.9945 259.8603 285.5093 127.1818 0.1305 260.1969 260.0664 285.6676 127.9703 0.1296 260.3636 260.2340 285.7791 128.7613 0.1268 260.5705 260.4438 285.9255 129.5815 0.1236 260.7707 260.6471 286.0632 130.3730 0.1199 260.9566 260.8366 286.1970 131.1945 0.1163 261.1473 261.0310 286.3421 131.9865 0.1142 261.3350 261.2209 286.4888 132.7785 0.1110 261.5219 261.4109 286.6318 133.6005 0.1095 261.7148 261.6053 286.7376 134.3925 0.1060 261.8988 261.7928 286.8731 135.2145 0.1059 262.0972 261.9913 286.9850 136.0065 0.1035 262.2905 262.1870 287.0993 136.7985 0.1010 262.4747 262.3737 287.2167 137.6205 0.0978 262.6647 262.5669 287.3626 138.4125 0.0945 262.8540 262.7595 287.4808 139.2343 0.0937 263.0476 262.9540 287.6107 140.0263 0.0917 263.2445 263.1528 287.7250 140.8178 0.0883 263.4312 263.3429 287.8373 141.6403 0.0884 263.6066 263.5182 287.9460 142.4320 0.0871 263.7841 263.6970 288.0612 143.2540 0.0819 263.9781 263.8962 288.1835 144.0458 0.0799 264.1667 264.0868 288.3043 144.8375 0.0787 264.3473 264.2686 288.4338 145.6903 0.0791 264.5492 264.4700 288.5649 146.4525 0.0757 264.7393 264.6636 288.6750 147.2748 0.0708 264.9264 264.8555 288.8153 148.0668 0.0755 265.1088 265.0333 288.9373 148.8585 0.0723 265.2891 265.2167 289.0713 149.7108 0.0666 265.4835 265.4169 289.2277 150.4725 0.0662 265.6638 265.5976 289.3394 151.2948 0.0637 265.8606 265.7969 289.4700 152.0943 0.0624 266.0420 265.9796 289.6136 152.8850 0.0610 266.2191 266.1581 289.7379 153.7030 0.0595 266.3965 266.3370 289.8832 154.4910 0.0572 266.5964 266.5392 290.0224 155.3090 0.0549 266.7725 266.7177 290.1569 156.0970 0.0535 266.9660 266.9125 290.2747 156.8855 0.0522 267.1470 267.0948 290.4129 157.7365 0.0475 267.3236 267.2760 290.5598 158.4950 0.0469 267.5010 267.4542 290.6776 159.3138 0.0446 267.7048 267.6602 290.8218 160.1338 0.0417 267.8769 267.8352 290.9580 160.8948 0.0400 268.0408 268.0007 291.0873 161.7458 0.0370 268.2244 268.1874 291.2362 162.5065 0.0353 268.4135 268.3782 291.3444 163.3288 0.0335 268.5992 268.5657 291.4802 164.1508 0.0299 268.7898 268.7599 291.6230 164.9125 0.0299 268.9614 268.9316 291.7552 165.7645 0.0281 269.1521 269.1240 291.9226 166.5265 0.0258 269.3320 269.3062 292.0481 167.3488 0.0288 269.5062 269.4774 292.1731 168.1708 0.0264 269.6946 269.6682 292.3140 168.9325 0.0241 269.8748 269.8507 292.4432 169.7845 0.0227 270.0761 270.0534 292.5864 170.5465 0.0182 270.2499 270.2317 292.7111 171.3685 0.0163 270.4091 270.3929 292.8500 172.1905 0.0199 270.6078 270.5879 292.9849 172.9525 0.0181 270.7827 270.7646 293.1041 173.8045 0.0156 270.9614 270.9458 293.2433 174.5965 0.0126 271.1386 271.1260 293.3774 175.3885 0.0128 271.3207 271.3078 293.5270 176.2105 0.0110 271.5016 271.4906 293.6594 176.9725 0.0104 271.6806 271.6701 293.7797 177.8245 0.0100 271.8595 271.8496 293.9225 178.6165 0.0094 272.0308 272.0214 294.0506 179.4095 0.0062 272.2081 272.2019 294.1910 180.2315 0.0072 272.3998 272.3926 294.3114 180.9933 0.0061 272.5566 272.5504 294.4470 181.8450 0.0044 272.7600 272.7556 294.5745 182.6405 0.0049 272.9411 272.9362 294.7093 183.4335 0.0001 273.0946 273.0946 294.8581 184.2555 -0.0010 273.2856 273.2866 294.9834 185.0140 -0.0011 273.4636 273.4647 295.1095 185.8633 0.0011 273.6594 273.6583 295.2510 186.6213 -0.0001 273.8132 273.8133 295.3607 187.4400 -0.0007 273.9971 273.9978 295.5022 188.2285 -0.0023 274.1645 274.1668 295.6356 189.0165 -0.0049 274.3440 274.3489 295.7465 189.8650 -0.0037 274.5020 274.5057 295.8897 190.6238 -0.0040 274.6704 274.6744 296.0160 191.4423 -0.0059 274.8557 274.8616 296.1446 192.2613 -0.0048 275.0347 275.0395 296.2726 193.0213 -0.0068 275.2079 275.2146 296.4045 193.8725 -0.0096 275.3932 275.4028 296.5370 194.6345 -0.0106 275.5614 275.5720 296.6653 195.4563 -0.0095 275.7485 275.7580 296.8143 196.2483 -0.0117 275.9058 275.9174 296.9385 197.0395 -0.0118 276.0827 276.0945 297.0649 197.8920 -0.0088 276.2704 276.2793 297.2116 198.6540 -0.0127 276.4306 276.4434 297.3196 199.4758 -0.0158 276.6088 276.6246 297.4669 200.2680 -0.0143 276.7956 276.8099 297.5840 201.0595 -0.0142 276.9522 276.9663 297.7059 201.9120 -0.0123 277.1448 277.1571 297.8496 202.6735 -0.0123 277.3042 277.3164 297.9720 203.4958 -0.0163 277.4862 277.5025 298.1029 204.2878 -0.0159 277.6520 277.6679 298.2250 205.0795 -0.0164 277.8286 277.8450 298.3450 205.9318 -0.0167 278.0110 278.0278 298.5076 206.6935 -0.0169 278.1922 278.2090 298.6197 207.5158 -0.0168 278.3535 278.3703 298.7563 208.3078 -0.0183 278.5249 278.5432 298.8749 209.0995 -0.0185 278.6822 278.7007 299.0072 209.9218 -0.0187 278.8606 278.8793 299.1407 210.7135 -0.0170 279.0325 279.0495 299.2755 211.5365 -0.0203 279.2187 279.2390 299.4085 212.3288 -0.0165 279.3813 279.3978 299.5384 213.1215 -0.0181 279.5645 279.5827 299.6653 213.9435 -0.0162 279.7345 279.7506 299.8059 214.7355 -0.0184 279.8946 279.9130 299.9354 215.5575 -0.0176 280.0646 280.0822 300.0602 216.3485 -0.0179 280.2267 280.2445 300.1769 217.1368 -0.0169 280.3992 280.4161 300.3084 217.9550 -0.0175 280.5764 280.5940 300.4459 218.7430 -0.0193 280.7440 280.7633 300.5744 219.5610 -0.0181 280.9286 280.9467 300.7143 220.3490 -0.0186 281.0810 281.0996 300.8409 221.1370 -0.0189 281.2527 281.2716 300.9807 221.9553 -0.0173 281.4139 281.4312 301.1359 222.7440 -0.0180 281.5964 281.6145 301.2537 223.5628 -0.0191 281.7729 281.7919 301.4084 224.3518 -0.0183 281.9415 281.9598 301.5529 225.1423 -0.0193 282.1174 282.1368 301.7001 225.9635 -0.0196 282.2749 282.2945 301.8558 226.7555 -0.0194 282.4484 282.4679 302.0050 227.5775 -0.0166 282.6173 282.6340 302.1569 228.3695 -0.0195 282.7953 282.8148 302.3051 229.1615 -0.0165 282.9535 282.9699 302.4549 229.9835 -0.0166 283.1186 283.1352 302.6065 230.7455 -0.0188 283.2641 283.2829 302.7350 231.5975 -0.0203 283.4412 283.4616 302.9029 232.3595 -0.0194 283.6090 283.6283 303.0333 233.1815 -0.0215 283.7918 283.8133 303.1578 233.9813 -0.0194 283.9446 283.9641 303.2958 234.7745 -0.0186 284.1146 284.1332 303.4250 235.6270 -0.0187 284.3040 284.3227 303.5758 236.3895 -0.0193 284.4528 284.4721 303.6929 237.2115 -0.0188 284.6271 284.6460 303.8173 238.0035 -0.0170 284.8164 284.8334 303.9603 238.7955 -0.0173 284.9845 285.0018 304.0938 239.6175 -0.0199 285.1343 285.1543 304.2025 240.4085 -0.0219 285.3044 285.3263 304.3250 241.2310 -0.0219 285.4873 285.5092 304.4481 242.0228 -0.0205 285.6381 285.6586 304.5805 242.8145 -0.0221 285.7929 285.8150 304.7156 243.6393 -0.0230 285.9565 285.9794 304.8407 244.4108 -0.0210 286.1319 286.1529 304.9539 245.2628 -0.0177 286.3067 286.3244 305.0851 246.0245 -0.0183 286.4745 286.4929 305.2093 246.8468 -0.0195 286.6457 286.6652 305.3297 247.6690 -0.0173 286.8129 286.8302 305.4606 248.4315 -0.0183 286.9747 286.9931 305.5786 249.2830 -0.0180 287.1375 287.1554 305.6996 250.0410 -0.0202 287.3066 287.3268 305.8131 250.8590 -0.0188 287.4822 287.5010 305.9349 251.6478 -0.0201 287.6286 287.6487 306.0590 252.4380 -0.0199 287.7957 287.8157 306.1781 253.2860 -0.0169 287.9666 287.9835 306.2910 254.0440 -0.0159 288.1157 288.1316 306.4131 254.8630 -0.0160 288.3019 288.3180 306.5438 255.6518 -0.0169 288.4533 288.4702 306.6661 256.4415 -0.0169 288.6153 288.6322 306.7914 257.2928 -0.0168 288.8069 288.8237 306.9276 258.0540 -0.0179 288.9589 288.9768 307.0665 258.8758 -0.0160 289.1130 289.1290 307.2112 259.6668 -0.0162 289.2775 289.2937 307.3451 260.4585 -0.0150 289.4378 289.4529 307.4771 261.3108 -0.0131 289.6164 289.6295 307.6214 262.0725 -0.0138 289.7733 289.7871 307.7559 262.8948 -0.0156 289.9612 289.9768 307.9022 263.6868 -0.0155 290.1158 290.1313 308.0330 264.4785 -0.0162 290.2830 290.2993 308.1748 265.3008 -0.0143 290.4432 290.4575 308.3254 266.0925 -0.0137 290.5843 290.5980 308.4738 266.9148 -0.0141 290.7545 290.7686 308.6114 267.7065 -0.0126 290.9202 290.9328 308.7628 268.4985 -0.0139 291.0778 291.0917 308.9039 269.3513 -0.0137 291.2452 291.2589 309.0637 270.1135 -0.0137 291.4105 291.4242 309.1986 270.9355 -0.0141 291.5692 291.5834 309.3643 271.7275 -0.0124 291.7457 291.7581 309.4885 272.5195 -0.0125 291.8980 291.9105 309.6450 273.3715 -0.0113 292.0705 292.0818 309.7877 274.1335 -0.0128 292.2315 292.2443 309.9181 274.9555 -0.0130 292.4016 292.4146 310.0596 275.7475 -0.0112 292.5597 292.5709 310.1975 276.5395 -0.0090 292.7129 292.7220 310.3135 277.3915 -0.0096 292.8766 292.8862 310.4431 278.1535 -0.0103 293.0345 293.0447 310.5522 278.9750 -0.0081 293.2085 293.2166 310.6835 279.7675 -0.0080 293.3855 293.3935 310.8097 280.5585 -0.0080 293.5315 293.5395 310.9418 281.4103 -0.0068 293.7010 293.7078 311.0651 282.1683 -0.0041 293.8517 293.8558 311.1810 282.9873 -0.0063 294.0364 294.0426 311.3122 283.7758 -0.0047 294.1872 294.1919 311.4194 284.5638 -0.0044 294.3502 294.3546 311.5350 285.4120 -0.0020 294.5154 294.5174 311.6634 286.1698 -0.0029 294.6651 294.6680 311.7613 286.9885 -0.0028 294.8291 294.8320 311.8886 287.8080 -0.0049 294.9995 295.0044 312.0066 288.5678 -0.0061 295.1404 295.1466 312.1175 289.4173 -0.0009 295.3085 295.3094 312.2759 290.2075 -0.0000 295.4675 295.4675 312.3904 290.9985 -0.0004 295.6222 295.6226 312.5171 291.8205 0.0014 295.7880 295.7866 312.6635 292.5825 0.0024 295.9587 295.9563 312.7801 293.4345 0.0006 296.1003 296.0998 312.9284 294.1963 0.0023 296.2616 296.2593 313.0466 295.0278 0.0016 296.4366 296.4350 313.1684 295.8293 0.0036 296.6000 296.5964 313.3162 296.6205 0.0005 296.7595 296.7590 313.4674 297.4428 0.0029 296.9071 296.9042 313.6052 298.2048 0.0035 297.0713 297.0678 313.7283 299.0568 0.0015 297.2374 297.2359 313.8732 299.8490 0.0038 297.4025 297.3987 314.0121 300.6405 0.0067 297.5499 297.5432 314.1471 301.4628 -0.0037 297.7202 297.7239 314.2793 302.2245 -0.0018 297.8772 297.8790 314.4088 303.0768 -0.0014 298.0484 298.0497 314.5428 303.8688 -0.0085 298.1991 298.2076 314.6902 304.6605 -0.0095 298.3619 298.3714 314.8250 305.4828 -0.0065 298.5232 298.5297 314.9632 306.3048 0.0020 298.6831 298.6812 315.1041 307.0965 0.0171 298.8324 298.8153 315.2473 307.9493 0.0184 299.0090 298.9906 315.3961 308.7115 0.0173 299.1791 299.1618 315.5044 309.5338 0.0203 299.3228 299.3025 315.6483 310.3560 0.0216 299.4962 299.4746 315.7894 311.1185 0.0229 299.6356 299.6128 315.9113 311.9710 0.0264 299.8150 299.7886 316.0673 312.7335 0.0269 299.9794 299.9526 316.1935 313.5540 0.0279 300.1355 300.1076 316.3458 314.3720 0.0297 300.2870 300.2573 316.4635 315.1300 0.0319 300.4260 300.3941 316.5798 315.9830 0.0353 300.5868 300.5516 316.7360 316.7410 0.0368 300.7583 300.7215 316.8686 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