DTA measure 1program4 Date: 2024416:1157 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1139.79 s Mass = 1304.400 mg data_number = 1418 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2223 -0.7915 248.8624 249.6539 266.2640 1.9835 -0.7912 248.9894 249.7806 266.2722 2.8348 -0.7807 249.1516 249.9323 266.2775 3.5965 -0.7756 249.2723 250.0478 266.3016 4.4185 -0.7723 249.4071 250.1794 266.3266 5.2405 -0.7665 249.5613 250.3278 266.3232 6.0025 -0.7624 249.6942 250.4566 266.3534 6.8545 -0.7594 249.8314 250.5908 266.3703 7.6165 -0.7553 249.9619 250.7172 266.3907 8.4385 -0.7511 250.1017 250.8528 266.4071 9.2605 -0.7455 250.2503 250.9958 266.4478 10.0225 -0.7384 250.3624 251.1008 266.4856 10.8745 -0.7336 250.5096 251.2432 266.5324 11.6365 -0.7293 250.6379 251.3672 266.5854 12.4585 -0.7256 250.7850 251.5107 266.6457 13.2803 -0.7211 250.9243 251.6454 266.7152 14.0420 -0.7196 251.0548 251.7744 266.7799 14.8940 -0.7141 251.1824 251.8965 266.8615 15.6555 -0.7075 251.3278 252.0353 266.9413 16.4778 -0.7035 251.4864 252.1899 267.0288 17.2998 -0.6999 251.5942 252.2941 267.1234 18.0615 -0.6969 251.7232 252.4201 267.2280 18.9138 -0.6959 251.8723 252.5682 267.3275 19.7058 -0.6915 251.9986 252.6902 267.4452 20.4975 -0.6882 252.1251 252.8133 267.5643 21.3200 -0.6841 252.2570 252.9411 267.6719 22.0825 -0.6797 252.3789 253.0586 267.7670 22.9353 -0.6758 252.5337 253.2095 267.9046 23.7278 -0.6742 252.6555 253.3297 268.0253 24.5195 -0.6725 252.7826 253.4550 268.1647 25.3420 -0.6681 252.9225 253.5906 268.2964 26.1345 -0.6652 253.0512 253.7164 268.4282 26.9573 -0.6668 253.1905 253.8573 268.5748 27.7478 -0.6689 253.3130 253.9819 268.7069 28.5340 -0.6676 253.4393 254.1069 268.8424 29.3520 -0.6609 253.5816 254.2425 268.9788 30.1100 -0.6618 253.7027 254.3645 269.1078 30.9580 -0.6603 253.8414 254.5016 269.2520 31.7465 -0.6573 253.9706 254.6280 269.3864 32.5350 -0.6544 254.1061 254.7605 269.5209 33.3540 -0.6540 254.2323 254.8863 269.6524 34.1148 -0.6538 254.3633 255.0171 269.7632 34.9645 -0.6484 254.4939 255.1424 269.8892 35.7545 -0.6463 254.6240 255.2702 270.0159 36.5448 -0.6482 254.7575 255.4058 270.1297 37.3665 -0.6481 254.8942 255.5424 270.2661 38.1285 -0.6452 255.0101 255.6553 270.3814 38.9808 -0.6432 255.1339 255.7771 270.4983 39.7725 -0.6451 255.2689 255.9141 270.6135 40.5645 -0.6408 255.4146 256.0553 270.7246 41.3868 -0.6429 255.5475 256.1904 270.8270 42.1485 -0.6415 255.6622 256.3037 270.9302 43.0005 -0.6397 255.7952 256.4349 271.0456 43.7625 -0.6395 255.9195 256.5590 271.1403 44.5845 -0.6395 256.0507 256.6901 271.2495 45.4065 -0.6301 256.1891 256.8192 271.3403 46.1685 -0.6331 256.3149 256.9480 271.4443 47.0205 -0.6333 256.4389 257.0723 271.5391 47.7825 -0.6361 256.5583 257.1944 271.6368 48.6045 -0.6332 256.6851 257.3183 271.7212 49.4265 -0.6364 256.8113 257.4476 271.8223 50.1885 -0.6378 256.9281 257.5660 271.9094 51.0405 -0.6335 257.0885 257.7220 272.0002 51.8023 -0.6255 257.1995 257.8250 272.0978 52.6243 -0.6285 257.3197 257.9482 272.2054 53.4463 -0.6327 257.4658 258.0985 272.3017 54.2075 -0.6346 257.5983 258.2329 272.3790 55.0608 -0.6360 257.7436 258.3796 272.4627 55.8225 -0.6362 257.8594 258.4956 272.5409 56.6448 -0.6372 257.9913 258.6285 272.6251 57.4368 -0.6379 258.1121 258.7500 272.7251 58.2285 -0.6334 258.2384 258.8717 272.8251 59.0853 -0.6364 258.3814 259.0178 272.9396 59.8485 -0.6381 258.4952 259.1333 273.0280 60.6703 -0.6337 258.6277 259.2614 273.1530 61.4585 -0.6341 258.7518 259.3860 273.2428 62.2473 -0.6359 258.8725 259.5083 273.3449 63.0655 -0.6374 258.9986 259.6360 273.4526 63.8540 -0.6361 259.1148 259.7509 273.5579 64.6728 -0.6373 259.2574 259.8947 273.6526 65.4618 -0.6373 259.3857 260.0230 273.7624 66.2520 -0.6393 259.4990 260.1384 273.8783 67.0730 -0.6378 259.6284 260.2663 273.9873 67.8348 -0.6340 259.7452 260.3792 274.0869 68.6870 -0.6299 259.8734 260.5033 274.2072 69.4780 -0.6319 260.0221 260.6540 274.3053 70.2688 -0.6324 260.1426 260.7750 274.4090 71.0908 -0.6348 260.2630 260.8978 274.5370 71.8525 -0.6341 260.3888 261.0229 274.6421 72.7048 -0.6333 260.5171 261.1504 274.7503 73.4668 -0.6325 260.6368 261.2693 274.8604 74.2888 -0.6361 260.7668 261.4028 274.9598 75.1108 -0.6353 260.8948 261.5301 275.0697 75.8725 -0.6377 261.0122 261.6498 275.1559 76.7248 -0.6420 261.1522 261.7942 275.2796 77.4868 -0.6404 261.2598 261.9002 275.3939 78.3085 -0.6434 261.4074 262.0508 275.4997 79.1308 -0.6458 261.5283 262.1741 275.6215 79.8925 -0.6430 261.6530 262.2960 275.7197 80.7448 -0.6421 261.7802 262.4223 275.8268 81.5065 -0.6457 261.9039 262.5496 275.9206 82.3288 -0.6516 262.0152 262.6668 276.0317 83.1205 -0.6530 262.1283 262.7813 276.1505 83.9125 -0.6568 262.2571 262.9139 276.2413 84.7645 -0.6572 262.3893 263.0465 276.3610 85.5265 -0.6576 262.4952 263.1528 276.4728 86.3485 -0.6581 262.6365 263.2945 276.5783 87.1405 -0.6612 262.7677 263.4288 276.6812 87.9325 -0.6621 262.8988 263.5609 276.7841 88.7845 -0.6614 263.0176 263.6790 276.8908 89.5465 -0.6594 263.1491 263.8085 276.9828 90.3683 -0.6605 263.2683 263.9288 277.1009 91.1605 -0.6632 263.3848 264.0481 277.2144 91.9525 -0.6690 263.5164 264.1854 277.3257 92.8015 -0.6671 263.6495 264.3166 277.4208 93.5570 -0.6643 263.7666 264.4309 277.5074 94.3743 -0.6656 263.9097 264.5753 277.6178 95.1625 -0.6673 264.0093 264.6765 277.7308 95.9513 -0.6699 264.1235 264.7934 277.8316 96.7713 -0.6742 264.2526 264.9268 277.9394 97.5608 -0.6775 264.3804 265.0579 278.0365 98.3788 -0.6792 264.4974 265.1766 278.1399 99.1670 -0.6814 264.6218 265.3032 278.2454 99.9550 -0.6809 264.7432 265.4241 278.3543 100.8045 -0.6839 264.8663 265.5502 278.4600 101.5653 -0.6799 264.9941 265.6740 278.5649 102.3855 -0.6811 265.1111 265.7921 278.6671 103.1768 -0.6838 265.2253 265.9091 278.7856 103.9688 -0.6866 265.3502 266.0368 278.8728 104.8205 -0.6916 265.4736 266.1652 278.9813 105.5825 -0.6869 265.6073 266.2942 279.0761 106.4045 -0.6922 265.7223 266.4145 279.1829 107.1965 -0.6990 265.8500 266.5490 279.2938 107.9883 -0.7019 265.9757 266.6776 279.3842 108.8138 -0.7015 266.0932 266.7948 279.4919 109.5768 -0.7044 266.1975 266.9019 279.5890 110.4290 -0.7069 266.3401 267.0469 279.6961 111.2210 -0.7069 266.4643 267.1712 279.7922 112.0128 -0.7085 266.5910 267.2995 279.8975 112.8348 -0.7118 266.7026 267.4143 279.9998 113.5965 -0.7134 266.8347 267.5481 280.1069 114.4490 -0.7145 266.9704 267.6849 280.2236 115.2033 -0.7162 267.0782 267.7944 280.3183 116.0628 -0.7146 267.1964 267.9110 280.4170 116.8245 -0.7220 267.3025 268.0245 280.5114 117.6468 -0.7235 267.4452 268.1687 280.6121 118.4688 -0.7273 267.5594 268.2866 280.6974 119.2305 -0.7281 267.6857 268.4138 280.7999 120.0833 -0.7289 267.7981 268.5270 280.9064 120.8760 -0.7339 267.9318 268.6657 281.0068 121.6675 -0.7372 268.0454 268.7826 281.1165 122.4908 -0.7360 268.1595 268.8955 281.2288 123.2525 -0.7381 268.2884 269.0265 281.3413 124.1053 -0.7432 268.4065 269.1496 281.4628 124.8930 -0.7434 268.5307 269.2741 281.5813 125.6800 -0.7468 268.6423 269.3891 281.6927 126.4980 -0.7444 268.7633 269.5076 281.7975 127.2878 -0.7464 268.8928 269.6392 281.9209 128.1070 -0.7511 269.0283 269.7794 282.0438 128.8960 -0.7491 269.1493 269.8985 282.1595 129.6840 -0.7579 269.2615 270.0194 282.2737 130.5040 -0.7625 269.3921 270.1546 282.4070 131.2958 -0.7698 269.5109 270.2807 282.5198 132.1148 -0.7767 269.6386 270.4152 282.6435 132.9030 -0.7754 269.7507 270.5262 282.7633 133.6923 -0.7762 269.8561 270.6323 282.8839 134.5135 -0.7766 269.9909 270.7675 282.9988 135.3038 -0.7786 270.1023 270.8809 283.1155 136.1265 -0.7813 270.2290 271.0103 283.2332 136.9185 -0.7860 270.3365 271.1224 283.3351 137.7105 -0.7884 270.4743 271.2627 283.4328 138.5328 -0.7933 270.5901 271.3834 283.5502 139.3245 -0.7968 270.7067 271.5035 283.6502 140.1468 -0.8006 270.8327 271.6333 283.7517 140.9385 -0.8020 270.9594 271.7614 283.8518 141.7305 -0.8063 271.0798 271.8861 283.9554 142.5525 -0.8083 271.1906 271.9990 284.0554 143.3455 -0.7982 271.3216 272.1198 284.1439 144.1685 -0.7921 271.4377 272.2298 284.2423 144.9605 -0.7929 271.5558 272.3487 284.3349 145.7525 -0.7927 271.6681 272.4608 284.4348 146.6045 -0.7961 271.8106 272.6067 284.5529 147.3665 -0.8015 271.9244 272.7259 284.6421 148.1893 -0.8105 272.0357 272.8462 284.7194 148.9815 -0.8128 272.1624 272.9751 284.8249 149.7735 -0.8121 272.2856 273.0977 284.9219 150.6253 -0.8160 272.4101 273.2260 285.0245 151.3873 -0.8189 272.5204 273.3393 285.1195 152.2090 -0.8153 272.6496 273.4648 285.2058 153.0010 -0.8161 272.7589 273.5749 285.2918 153.7935 -0.8264 272.8934 273.7198 285.3824 154.6458 -0.8312 273.0312 273.8624 285.4806 155.4075 -0.8313 273.1387 273.9701 285.5786 156.2298 -0.8303 273.2548 274.0851 285.6779 157.0480 -0.8347 273.3563 274.1910 285.7785 157.8050 -0.8354 273.4826 274.3180 285.8689 158.6530 -0.8360 273.6162 274.4522 285.9979 159.4110 -0.8392 273.7240 274.5633 286.1073 160.2305 -0.8408 273.8491 274.6899 286.2084 161.0495 -0.8455 273.9785 274.8239 286.3271 161.8083 -0.8482 274.0728 274.9210 286.4391 162.6563 -0.8496 274.2008 275.0504 286.5710 163.4453 -0.8520 274.3266 275.1786 286.6841 164.2355 -0.8550 274.4404 275.2954 286.7919 165.0570 -0.8586 274.5694 275.4280 286.9125 165.8183 -0.8599 274.6752 275.5351 287.0230 166.6698 -0.8616 274.8036 275.6652 287.1402 167.4620 -0.8641 274.9162 275.7804 287.2457 168.2535 -0.8670 275.0341 275.9011 287.3666 169.0758 -0.8699 275.1546 276.0245 287.5000 169.8375 -0.8711 275.2702 276.1413 287.6100 170.6898 -0.8694 275.4041 276.2735 287.7425 171.4515 -0.8727 275.5211 276.3938 287.8398 172.2738 -0.8789 275.6228 276.5018 287.9697 173.0958 -0.8800 275.7482 276.6281 288.1014 173.8575 -0.8741 275.8640 276.7380 288.2117 174.7098 -0.8786 276.0048 276.8834 288.3310 175.4715 -0.8872 276.0970 276.9842 288.4520 176.2938 -0.8895 276.2265 277.1160 288.5566 177.1160 -0.8841 276.3450 277.2291 288.6647 177.8785 -0.8916 276.4642 277.3558 288.7543 178.7308 -0.8972 276.5852 277.4823 288.8643 179.4925 -0.8992 276.7107 277.6099 288.9581 180.3148 -0.9042 276.8270 277.7313 289.0633 181.1385 -0.9067 276.9553 277.8620 289.1810 181.9015 -0.9100 277.0484 277.9584 289.2541 182.7538 -0.9126 277.1827 278.0953 289.3671 183.5155 -0.9174 277.3023 278.2197 289.4568 184.3383 -0.9200 277.4313 278.3513 289.5585 185.1605 -0.9131 277.5487 278.4618 289.6451 185.9225 -0.9123 277.6499 278.5623 289.7266 186.7745 -0.9136 277.7794 278.6929 289.8199 187.5365 -0.9146 277.9046 278.8192 289.9063 188.3585 -0.9163 278.0029 278.9192 290.0031 189.1803 -0.9212 278.1386 279.0598 290.1123 189.9400 -0.9227 278.2610 279.1837 290.1880 190.7885 -0.9238 278.3809 279.3047 290.2879 191.5470 -0.9279 278.4670 279.3949 290.3716 192.3650 -0.9330 278.6015 279.5345 290.4659 193.1533 -0.9354 278.7207 279.6561 290.5687 193.9430 -0.9349 278.8314 279.7663 290.6751 194.7918 -0.9364 278.9575 279.8939 290.7838 195.5518 -0.9442 279.0745 280.0187 290.8837 196.3728 -0.9492 279.1938 280.1430 290.9963 197.1648 -0.9529 279.3081 280.2610 291.1029 197.9565 -0.9557 279.4365 280.3922 291.2184 198.7780 -0.9556 279.5687 280.5243 291.3361 199.5695 -0.9568 279.6764 280.6332 291.4381 200.3915 -0.9564 279.7895 280.7460 291.5418 201.1835 -0.9593 279.8982 280.8576 291.6625 201.9755 -0.9612 280.0266 280.9878 291.7730 202.7975 -0.9647 280.1488 281.1136 291.8814 203.5595 -0.9670 280.2498 281.2168 291.9777 204.4115 -0.9719 280.3887 281.3606 292.1090 205.2035 -0.9734 280.5009 281.4743 292.2161 205.9955 -0.9757 280.6210 281.5967 292.3376 206.8175 -0.9778 280.7511 281.7289 292.4438 207.5793 -0.9756 280.8485 281.8241 292.5481 208.4315 -0.9741 280.9800 281.9542 292.6646 209.1930 -0.9762 281.0915 282.0676 292.7712 210.0148 -0.9792 281.2097 282.1889 292.8785 210.8368 -0.9836 281.3267 282.3102 292.9902 211.5985 -0.9876 281.4450 282.4326 293.0950 212.4508 -0.9906 281.5695 282.5601 293.2102 213.2128 -0.9929 281.6661 282.6590 293.3289 214.0355 -0.9948 281.7998 282.7946 293.4498 214.8580 -0.9953 281.9324 282.9277 293.5521 215.6205 -1.0006 282.0315 283.0321 293.6634 216.4728 -1.0006 282.1429 283.1435 293.7853 217.2345 -1.0038 282.2562 283.2600 293.8969 218.0568 -1.0080 282.4052 283.4133 293.9941 218.8790 -1.0114 282.5289 283.5404 294.1125 219.6415 -1.0146 282.6248 283.6394 294.2186 220.4943 -1.0165 282.7563 283.7728 294.3145 221.2565 -1.0199 282.8613 283.8813 294.4278 222.0760 -1.0211 282.9765 283.9976 294.5253 222.8643 -1.0239 283.0972 284.1211 294.6370 223.6530 -1.0253 283.2162 284.2414 294.7559 224.5018 -1.0297 283.3401 284.3698 294.8731 225.2625 -1.0300 283.4459 284.4759 294.9637 226.0830 -1.0325 283.5607 284.5932 295.0596 226.8715 -1.0356 283.6740 284.7096 295.1770 227.6623 -1.0391 283.7935 284.8326 295.2871 228.4838 -1.0399 283.9163 284.9562 295.3829 229.2733 -1.0406 284.0302 285.0708 295.4879 230.0938 -1.0435 284.1640 285.2075 295.6085 230.8848 -1.0480 284.2630 285.3110 295.7105 231.6765 -1.0507 284.3769 285.4276 295.8213 232.4988 -1.0519 284.5100 285.5619 295.9341 233.2605 -1.0544 284.6164 285.6708 296.0400 234.1128 -1.0585 284.7371 285.7956 296.1402 234.9048 -1.0621 284.8572 285.9193 296.2422 235.6985 -1.0628 284.9714 286.0341 296.3369 236.5208 -1.0644 285.0796 286.1440 296.4381 237.2825 -1.0674 285.2083 286.2757 296.5370 238.1348 -1.0681 285.3289 286.3970 296.6517 238.9265 -1.0725 285.4311 286.5035 296.7540 239.7185 -1.0747 285.5544 286.6291 296.8651 240.5405 -1.0767 285.6787 286.7555 296.9643 241.3025 -1.0797 285.7946 286.8744 297.0613 242.1545 -1.0807 285.8983 286.9791 297.1620 242.9465 -1.0818 286.0167 287.0985 297.2673 243.7385 -1.0867 286.1420 287.2287 297.3637 244.5608 -1.0873 286.2609 287.3482 297.4758 245.3235 -1.0895 286.3961 287.4856 297.5690 246.1760 -1.0927 286.5159 287.6086 297.6781 246.9685 -1.0971 286.6197 287.7168 297.7828 247.7615 -1.0981 286.7414 287.8396 297.8788 248.5835 -1.0997 286.8663 287.9659 297.9746 249.3460 -1.1027 286.9807 288.0834 298.0791 250.1985 -1.1047 287.0952 288.1999 298.1887 250.9608 -1.1081 287.1943 288.3024 298.2792 251.7828 -1.1089 287.3208 288.4297 298.3973 252.6050 -1.1112 287.4528 288.5640 298.4919 253.3670 -1.1149 287.5643 288.6792 298.5854 254.2158 -1.1172 287.6901 288.8073 298.6809 254.9743 -1.1202 287.8006 288.9208 298.7905 255.7938 -1.1199 287.9078 289.0277 298.8985 256.6128 -1.1211 288.0387 289.1598 298.9958 257.3715 -1.1245 288.1401 289.2647 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