DTA measure 2program3 Date: 2024416:1132 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1606.65 s Mass = 1304.400 mg data_number = 999 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5060 -4.1009 425.2368 429.3377 418.4073 4.1198 -4.1050 425.3855 429.4905 418.4224 5.7186 -4.1126 425.5294 429.6420 418.4050 7.3331 -4.1216 425.6725 429.7941 418.3736 8.9333 -4.1272 425.8187 429.9460 418.3211 10.5635 -4.1299 425.9567 430.0865 418.2193 12.1638 -4.1346 426.1001 430.2347 418.1022 13.7623 -4.1401 426.2318 430.3720 417.9613 15.3690 -4.1430 426.3719 430.5149 417.7943 16.9600 -4.1470 426.4911 430.6381 417.6152 18.5821 -4.1508 426.6218 430.7726 417.4269 20.1753 -4.1543 426.7398 430.8941 417.2208 21.7841 -4.1581 426.8665 431.0245 417.0063 23.3798 -4.1640 426.9745 431.1386 416.7830 24.9936 -4.1666 427.0953 431.2620 416.5337 26.6078 -4.1694 427.2256 431.3950 416.2930 28.2066 -4.1734 427.3246 431.4980 416.0547 29.8211 -4.1752 427.4195 431.5947 415.8227 31.4216 -4.1750 427.5392 431.7142 415.5728 33.0356 -4.1782 427.6505 431.8287 415.3330 34.6496 -4.1827 427.7398 431.9225 415.1342 36.2485 -4.1569 427.8307 431.9877 414.9207 37.8625 -4.1348 427.9308 432.0656 414.7160 39.4615 -4.1497 428.0160 432.1658 414.5194 41.0754 -4.1527 428.1099 432.2627 414.3463 42.6895 -4.1589 428.1730 432.3319 414.1707 44.2878 -4.1446 428.2598 432.4044 413.9963 45.8998 -4.1882 428.3354 432.5236 413.8261 47.4915 -4.1738 428.4032 432.5770 413.6428 49.0974 -4.1616 428.4785 432.6400 413.4635 50.7053 -4.1879 428.5258 432.7136 413.2807 52.2986 -4.2026 428.5975 432.8001 413.1053 53.9074 -4.2060 428.6470 432.8531 412.9132 55.5044 -4.1778 428.7006 432.8784 412.7369 57.1033 -4.1792 428.7423 432.9216 412.5334 58.7320 -4.2016 428.8212 433.0228 412.3532 60.3308 -4.2176 428.8602 433.0778 412.1679 61.9298 -4.2243 428.8990 433.1232 411.9776 63.5436 -4.2263 428.9438 433.1701 411.7702 65.1426 -4.2222 428.9811 433.2033 411.5846 66.7718 -4.2257 429.0152 433.2409 411.3911 68.3706 -4.2367 429.0555 433.2922 411.1848 69.9696 -4.2436 429.0778 433.3214 410.9966 71.5836 -4.2471 429.0985 433.3456 410.7958 73.1833 -4.2492 429.1266 433.3758 410.5936 74.8125 -4.2540 429.1424 433.3964 410.3988 76.4116 -4.2547 429.1571 433.4119 410.2049 78.0096 -4.2565 429.1728 433.4293 410.0152 79.6010 -4.2621 429.2013 433.4634 409.8369 81.2070 -4.2645 429.2025 433.4670 409.6383 82.8088 -4.2667 429.2159 433.4826 409.4458 84.4308 -4.2718 429.2167 433.4885 409.2353 86.0243 -4.2794 429.2024 433.4818 409.0370 87.6824 -4.2830 429.2037 433.4867 408.8240 89.2955 -4.2924 429.2163 433.5087 408.6066 90.9095 -4.2968 429.1977 433.4945 408.4066 92.5085 -4.2974 429.1843 433.4817 408.1908 94.1075 -4.3089 429.1632 433.4722 407.9889 95.7365 -4.3095 429.1532 433.4627 407.7772 97.3355 -4.3131 429.1382 433.4512 407.5786 98.9494 -4.3179 429.1185 433.4364 407.3724 100.5501 -4.3178 429.1028 433.4205 407.1785 102.1510 -4.3200 429.0591 433.3791 406.9916 103.7684 -4.3247 429.0422 433.3670 406.7902 105.3836 -4.3231 428.9986 433.3216 406.6048 106.9836 -4.3328 428.9819 433.3147 406.4232 108.5826 -4.3491 428.9437 433.2928 406.2232 110.1970 -4.3403 428.9122 433.2526 406.0285 111.7910 -4.3569 428.8690 433.2259 405.8307 113.3971 -4.3619 428.8240 433.1860 405.6369 115.0050 -4.3657 428.7814 433.1471 405.4095 116.5963 -4.3544 428.7334 433.0878 405.2035 118.2078 -4.3474 428.6855 433.0329 404.9995 119.8649 -4.3427 428.6259 432.9685 404.7791 121.4766 -4.3601 428.5775 432.9375 404.5794 123.0906 -4.3669 428.5277 432.8946 404.3779 124.7046 -4.3687 428.4648 432.8335 404.1666 126.3056 -4.3697 428.4153 432.7850 403.9576 127.9196 -4.3720 428.3463 432.7183 403.7499 129.5185 -4.3764 428.2889 432.6653 403.5509 131.1175 -4.3802 428.2172 432.5974 403.3592 132.7465 -4.3826 428.1500 432.5325 403.1660 134.3463 -4.3831 428.0710 432.4540 402.9640 135.9615 -4.3828 428.0068 432.3896 402.7735 137.5605 -4.3900 427.9405 432.3305 402.5768 139.1594 -4.3927 427.8537 432.2465 402.3852 140.7890 -4.3952 427.7858 432.1809 402.1977 142.4024 -4.3980 427.7089 432.1069 401.9930 143.9945 -4.3999 427.6304 432.0303 401.8092 145.5856 -4.4056 427.5387 431.9443 401.6017 147.1915 -4.4074 427.4616 431.8690 401.3980 148.8136 -4.4111 427.3698 431.7809 401.1857 150.4064 -4.4125 427.2824 431.6948 400.9853 152.0160 -4.4124 427.1882 431.6007 400.7726 153.6145 -4.4192 427.0886 431.5078 400.5754 155.2138 -4.4180 427.0113 431.4293 400.3500 156.8443 -4.4192 426.9060 431.3252 400.1492 158.4429 -4.4222 426.8189 431.2411 399.9387 160.0568 -4.4256 426.7250 431.1506 399.7313 161.6558 -4.4288 426.6147 431.0435 399.5334 163.2698 -4.4294 426.5154 430.9447 399.3186 164.8708 -4.4299 426.4178 430.8477 399.1317 166.5018 -4.4325 426.3158 430.7483 398.9254 168.1006 -4.4346 426.2168 430.6514 398.7315 169.7150 -4.4346 426.0863 430.5209 398.5339 171.3151 -4.4379 425.9814 430.4192 398.3267 172.9295 -4.4380 425.8846 430.3226 398.1411 174.5429 -4.4400 425.7572 430.1973 397.9434 176.1350 -4.4382 425.6531 430.0913 397.7538 177.7410 -4.4434 425.5408 429.9842 397.5689 179.3325 -4.4463 425.4227 429.8691 397.3585 180.9405 -4.4454 425.3019 429.7473 397.1406 182.5505 -4.4478 425.2023 429.6501 396.9266 184.1485 -4.4501 425.0751 429.5252 396.7148 185.7619 -4.4501 424.9517 429.4019 396.4931 187.3605 -4.4533 424.8267 429.2800 396.2894 188.9745 -4.4523 424.7023 429.1546 396.0634 190.5886 -4.4523 424.5852 429.0375 395.8548 192.1875 -4.4554 424.4485 428.9039 395.6377 193.8015 -4.4537 424.3301 428.7839 395.4262 195.4031 -4.4534 424.2014 428.6548 395.2042 197.0035 -4.4551 424.0809 428.5360 395.0111 198.6331 -4.4570 423.9451 428.4021 394.7978 200.2321 -4.4545 423.8252 428.2797 394.5848 201.8308 -4.4502 423.6796 428.1298 394.3695 203.4446 -4.4557 423.5363 427.9920 394.1806 205.0436 -4.4574 423.4136 427.8710 393.9928 206.6565 -4.4571 423.2749 427.7320 393.7888 208.2631 -4.4574 423.1389 427.5963 393.5821 209.8545 -4.4581 423.0135 427.4715 393.3765 211.4471 -4.4570 422.8639 427.3209 393.1739 213.0396 -4.4571 422.7216 427.1788 392.9822 214.6628 -4.4574 422.5843 427.0418 392.7969 216.2584 -4.4588 422.4443 426.9031 392.6001 217.8716 -4.4604 422.3018 426.7622 392.3940 219.4706 -4.4594 422.1582 426.6177 392.2050 221.0699 -4.4586 422.0108 426.4694 392.0172 222.6686 -4.4584 421.8737 426.3321 391.8323 224.2978 -4.4572 421.7304 426.1876 391.6351 225.8966 -4.4577 421.5791 426.0368 391.4537 227.4956 -4.4579 421.4406 425.8985 391.2397 229.1096 -4.4602 421.2779 425.7382 391.0206 230.7085 -4.4576 421.1428 425.6003 390.8223 232.3375 -4.4556 420.9783 425.4339 390.6024 233.9365 -4.4561 420.8280 425.2841 390.3823 235.5355 -4.4538 420.6678 425.1216 390.1760 237.1389 -4.4550 420.5237 424.9788 389.9779 238.7546 -4.4537 420.3625 424.8162 389.7670 240.3654 -4.4506 420.2189 424.6695 389.5591 241.9565 -4.4514 420.0602 424.5116 389.3535 243.5635 -4.4493 419.9178 424.3671 389.1509 245.1551 -4.4475 419.7642 424.2116 388.9441 246.7635 -4.4455 419.6021 424.0476 388.7519 248.3729 -4.4455 419.4454 423.8909 388.5394 249.9848 -4.4453 419.2910 423.7363 388.3348 251.5835 -4.4429 419.1299 423.5728 388.1378 253.1824 -4.4418 418.9668 423.4085 387.9545 254.7963 -4.4389 418.8011 423.2401 387.7432 256.4109 -4.4372 418.6410 423.0782 387.5460 258.0138 -4.4366 418.4858 422.9224 387.3595 259.6289 -4.4353 418.3279 422.7633 387.1418 261.2286 -4.4347 418.1462 422.5809 386.9506 262.8276 -4.4342 417.9991 422.4333 386.7345 264.4566 -4.4301 417.8389 422.2690 386.5304 266.0558 -4.4316 417.6658 422.0975 386.3058 267.6696 -4.4300 417.5083 421.9382 386.0781 269.2690 -4.4273 417.3420 421.7693 385.8636 270.8685 -4.4251 417.1770 421.6021 385.6514 272.4940 -4.4219 416.9988 421.4207 385.4246 274.0850 -4.4199 416.8409 421.2608 385.2147 275.6910 -4.4179 416.6642 421.0821 385.0022 277.2830 -4.4187 416.4937 420.9124 384.7837 278.8921 -4.4166 416.3282 420.7448 384.5818 280.5013 -4.4140 416.1572 420.5712 384.3436 282.1135 -4.4124 416.0008 420.4132 384.1396 283.7126 -4.4090 415.8138 420.2227 383.9395 285.3115 -4.4059 415.6473 420.0532 383.7138 286.9255 -4.4039 415.4850 419.8889 383.5002 288.5478 -4.4021 415.3021 419.7042 383.2817 290.1465 -4.3990 415.1290 419.5281 383.0731 291.7455 -4.3958 414.9588 419.3546 382.8801 293.3595 -4.3949 414.7844 419.1793 382.6694 294.9585 -4.3929 414.6206 419.0135 382.4721 296.5880 -4.3872 414.4362 418.8234 382.2663 298.1883 -4.3861 414.2512 418.6373 382.0655 299.8040 -4.3863 414.0787 418.4651 381.8596 301.4036 -4.3831 413.8995 418.2826 381.6459 303.0026 -4.3794 413.7211 418.1005 381.4619 304.6263 -4.3757 413.5381 417.9137 381.2451 306.2323 -4.3698 413.3623 417.7321 381.0490 307.8270 -4.3709 413.1972 417.5681 380.8612 309.4313 -4.3687 413.0192 417.3878 380.6649 311.0236 -4.3665 412.8346 417.2010 380.4542 312.6499 -4.3628 412.6593 417.0221 380.2599 314.2484 -4.3589 412.4748 416.8337 380.0742 315.8468 -4.3557 412.2917 416.6473 379.8723 317.4606 -4.3530 412.1057 416.4587 379.6781 319.0596 -4.3501 411.9145 416.2646 379.4848 320.6738 -4.3498 411.7503 416.1001 379.2837 322.2886 -4.3463 411.5727 415.9190 379.0775 323.9036 -4.3439 411.3802 415.7242 378.8546 325.5026 -4.3404 411.2093 415.5497 378.6533 327.1016 -4.3382 411.0240 415.3622 378.4405 328.7306 -4.3340 410.8502 415.1842 378.2224 330.3445 -4.3309 410.6624 414.9933 378.0116 331.9435 -4.3289 410.4733 414.8022 377.7984 333.5425 -4.3255 410.2858 414.6113 377.5832 335.1564 -4.3197 410.1121 414.4318 377.3602 336.7644 -4.3164 409.9168 414.2332 377.1471 338.3725 -4.3133 409.7290 414.0423 376.9323 339.9718 -4.3083 409.5508 413.8591 376.7128 341.5634 -4.3078 409.3693 413.6771 376.5125 343.1565 -4.3033 409.1914 413.4948 376.2996 344.7816 -4.2997 409.0037 413.3034 376.0970 346.3805 -4.2981 408.8145 413.1127 375.8691 347.9795 -4.2955 408.6322 412.9277 375.6665 349.5860 -4.2896 408.4337 412.7234 375.4666 351.1924 -4.2846 408.2624 412.5470 375.2580 352.7913 -4.2821 408.0779 412.3600 375.0632 354.4051 -4.2793 407.8952 412.1745 374.8358 356.0194 -4.2765 407.7018 411.9783 374.6380 357.6178 -4.2727 407.5064 411.7790 374.4315 359.2316 -4.2696 407.3052 411.5747 374.2372 360.8313 -4.2651 407.1130 411.3781 374.0425 362.4306 -4.2625 406.9414 411.2039 373.8404 364.0446 -4.2586 406.7413 410.9999 373.6278 365.6596 -4.2546 406.5513 410.8059 373.4515 367.2596 -4.2519 406.3849 410.6368 373.2467 368.8573 -4.2483 406.1847 410.4330 373.0494 370.4656 -4.2436 405.9881 410.2317 372.8596 372.0570 -4.2389 405.8068 410.0457 372.6564 373.6788 -4.2359 405.6171 409.8530 372.4651 375.2716 -4.2309 405.4283 409.6592 372.2702 376.8674 -4.2277 405.2369 409.4645 372.0594 378.4796 -4.2243 405.0372 409.2615 371.8650 380.0786 -4.2192 404.8530 409.0722 371.6450 381.6925 -4.2155 404.6541 408.8696 371.4131 383.2915 -4.2129 404.4719 408.6848 371.2025 384.9055 -4.2066 404.2824 408.4890 370.9929 386.5045 -4.2051 404.0774 408.2825 370.7705 388.1035 -4.2009 403.8885 408.0893 370.5685 389.7325 -4.1979 403.6997 407.8975 370.3396 391.3315 -4.1931 403.5118 407.7048 370.1289 392.9455 -4.1890 403.3187 407.5077 369.8978 394.5444 -4.1861 403.1128 407.2989 369.6989 396.1440 -4.1798 402.9297 407.1096 369.4880 397.7726 -4.1748 402.7478 406.9226 369.2575 399.3726 -4.1707 402.5481 406.7189 369.0490 400.9858 -4.1658 402.3421 406.5079 368.8424 402.5784 -4.1634 402.1445 406.3079 368.6307 404.1703 -4.1598 401.9573 406.1171 368.4300 405.7929 -4.1567 401.7617 405.9183 368.2128 407.3861 -4.1484 401.5808 405.7293 368.0031 408.9970 -4.1435 401.3905 405.5341 367.7984 410.5944 -4.1388 401.1962 405.3350 367.5865 412.1919 -4.1352 400.9915 405.1267 367.3842 413.8058 -4.1322 400.8044 404.9366 367.1774 415.4208 -4.1270 400.6049 404.7319 366.9671 417.0196 -4.1232 400.4138 404.5370 366.7612 418.6346 -4.1161 400.2130 404.3291 366.5465 420.2346 -4.1126 400.0072 404.1197 366.3550 421.8486 -4.1086 399.8098 403.9184 366.1609 423.4636 -4.1047 399.6067 403.7114 365.9424 425.0626 -4.1000 399.4197 403.5196 365.7452 426.6770 -4.0968 399.2243 403.3211 365.5482 428.2765 -4.0925 399.0330 403.1255 365.3414 429.8905 -4.0875 398.8268 402.9143 365.1579 431.5045 -4.0791 398.6359 402.7150 364.9483 433.1019 -4.0786 398.4495 402.5281 364.7587 434.6939 -4.0729 398.2437 402.3166 364.5523 436.3005 -4.0664 398.0451 402.1115 364.3752 437.8930 -4.0651 397.8478 401.9129 364.1763 439.5179 -4.0622 397.6539 401.7161 363.9483 441.1148 -4.0561 397.4497 401.5058 363.7410 442.7125 -4.0528 397.2560 401.3087 363.5338 444.3115 -4.0499 397.0558 401.1057 363.3366 445.9255 -4.0444 396.8587 400.9031 363.1032 447.5395 -4.0413 396.6583 400.6995 362.8863 449.1535 -4.0367 396.4608 400.4975 362.6614 450.7525 -4.0354 396.2651 400.3005 362.4492 452.3521 -4.0336 396.0771 400.1106 362.2217 453.9663 -4.0248 395.8785 399.9033 361.9976 455.5800 -4.0213 395.6691 399.6905 361.7714 457.1939 -4.0182 395.4703 399.4885 361.5686 458.7936 -4.0129 395.2761 399.2889 361.3450 460.3926 -4.0069 395.0684 399.0753 361.1451 462.0066 -4.0022 394.8692 398.8714 360.9059 463.6206 -3.9968 394.6580 398.6548 360.6851 465.2311 -3.9899 394.4739 398.4638 360.4710 466.8220 -3.9850 394.2757 398.2606 360.2544 468.4135 -3.9807 394.0762 398.0569 360.0369 470.0218 -3.9758 393.8673 397.8431 359.8120 471.6330 -3.9725 393.6820 397.6545 359.6119 473.2443 -3.9723 393.4757 397.4480 359.3962 474.8416 -3.9670 393.2604 397.2275 359.1926 476.4406 -3.9606 393.0733 397.0339 358.9726 478.0546 -3.9570 392.8765 396.8336 358.7563 479.6686 -3.9511 392.6737 396.6248 358.5479 481.2678 -3.9449 392.4621 396.4071 358.3389 482.8830 -3.9397 392.2612 396.2009 358.1343 484.4830 -3.9369 392.0568 395.9937 357.9318 486.0825 -3.9348 391.8851 395.8198 357.7168 487.7115 -3.9282 391.6640 395.5921 357.4897 489.3105 -3.9244 391.4701 395.3945 357.2949 490.9249 -3.9196 391.2547 395.1743 357.0892 492.5254 -3.9153 391.0572 394.9725 356.8698 494.1265 -3.9083 390.8679 394.7762 356.6870 495.7413 -3.9034 390.6730 394.5764 356.4754 497.3554 -3.8989 390.4568 394.3557 356.2803 498.9491 -3.8952 390.2446 394.1398 356.0838 500.5568 -3.8908 390.0505 393.9413 355.8942 502.1489 -3.8867 389.8444 393.7311 355.6866 503.7570 -3.8799 389.6318 393.5117 355.4843 505.3655 -3.8746 389.4308 393.3054 355.2958 506.9783 -3.8713 389.2407 393.1119 355.0982 508.5771 -3.8670 389.0374 392.9045 354.8951 510.1759 -3.8635 388.8315 392.6950 354.7001 511.7899 -3.8597 388.6335 392.4932 354.4967 513.4039 -3.8541 388.4244 392.2785 354.3127 515.0026 -3.8474 388.2332 392.0806 354.1097 516.6166 -3.8412 388.0296 391.8707 353.9319 518.2156 -3.8364 387.8119 391.6482 353.7394 519.8446 -3.8336 387.6208 391.4544 353.5410 521.4438 -3.8289 387.4111 391.2400 353.3389 523.0575 -3.8260 387.1981 391.0242 353.1259 524.6566 -3.8191 386.9981 390.8172 352.9174 526.2713 -3.8168 386.8002 390.6171 352.7092 527.9013 -3.8095 386.5978 390.4073 352.4915 529.5008 -3.8039 386.4012 390.2051 352.2867 531.0929 -3.7991 386.1862 389.9853 352.0816 532.6994 -3.7954 385.9854 389.7808 351.8733 534.2910 -3.7914 385.7874 389.5788 351.6661 535.9129 -3.7844 385.5911 389.3755 351.4436 537.5089 -3.7786 385.3958 389.1744 351.2392 539.1191 -3.7738 385.1920 388.9658 351.0274 540.7181 -3.7661 384.9765 388.7427 350.8223 542.3325 -3.7607 384.7817 388.5424 350.6082 543.9465 -3.7545 384.5824 388.3369 350.3936 545.5455 -3.7502 384.3777 388.1279 350.1923 547.1595 -3.7475 384.1701 387.9175 349.9850 548.7585 -3.7396 383.9720 387.7116 349.7834 550.3721 -3.7363 383.7622 387.4985 349.5673 551.9861 -3.7303 383.5650 387.2953 349.3777 553.5858 -3.7248 383.3673 387.0921 349.1577 555.2000 -3.7197 383.1551 386.8749 348.9470 556.8001 -3.7153 382.9443 386.6596 348.7522 558.4146 -3.7092 382.7410 386.4502 348.5443 560.0296 -3.7049 382.5431 386.2481 348.3380 561.6425 -3.7009 382.3413 386.0422 348.1413 563.2341 -3.6975 382.1403 385.8378 347.9413 564.8258 -3.6890 381.9454 385.6344 347.7321 566.4479 -3.6885 381.7502 385.4387 347.5355 568.0553 -3.6795 381.5261 385.2056 347.3178 569.6504 -3.6761 381.3276 385.0037 347.1138 571.2478 -3.6717 381.1258 384.7976 346.8926 572.8616 -3.6662 380.9298 384.5960 346.6791 574.4690 -3.6621 380.7208 384.3829 346.4541 576.0918 -3.6563 380.5206 384.1770 346.2394 577.6906 -3.6529 380.3120 383.9649 346.0274 579.2896 -3.6491 380.0971 383.7462 345.8148 580.9036 -3.6420 379.9077 383.5497 345.5904 582.5026 -3.6363 379.7014 383.3377 345.3783 584.1315 -3.6309 379.4930 383.1238 345.1607 585.7305 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