DTA measure 1elso meres Date: 202435:1112 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 917.27 s Mass = 1138.400 mg data_number = 1141 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1965 -0.0373 224.7834 224.8207 265.7874 2.0193 -0.0341 225.0439 225.0780 265.7997 2.8118 -0.0322 225.3154 225.3476 265.8085 3.6053 -0.0325 225.5840 225.6164 265.8207 4.4580 -0.0290 225.8647 225.8938 265.8371 5.2203 -0.0278 226.1199 226.1477 265.8581 6.0418 -0.0240 226.3800 226.4039 265.8778 6.8343 -0.0220 226.6388 226.6608 265.8976 7.6255 -0.0197 226.8939 226.9136 265.9347 8.4783 -0.0162 227.1629 227.1790 265.9916 9.2405 -0.0124 227.4169 227.4293 266.0212 10.0635 -0.0115 227.6925 227.7040 266.0654 10.8555 -0.0127 227.9546 227.9673 266.1236 11.6450 -0.0084 228.1931 228.2015 266.1796 12.4650 -0.0088 228.4636 228.4723 266.2622 13.2550 -0.0071 228.7133 228.7204 266.3395 14.0740 -0.0061 228.9834 228.9895 266.4408 14.8628 -0.0029 229.2469 229.2498 266.5615 15.6513 -0.0018 229.5037 229.5055 266.6778 16.4703 0.0025 229.7506 229.7482 266.7989 17.2593 0.0071 229.9988 229.9917 266.9097 18.0788 0.0069 230.2544 230.2476 267.0516 18.8688 0.0423 230.4931 230.4508 267.1956 19.6588 0.0562 230.7319 230.6757 267.3363 20.4800 0.0581 231.0082 230.9501 267.4881 21.2710 0.0600 231.2366 231.1766 267.6286 22.0928 0.0622 231.4818 231.4196 267.8088 22.8848 0.0603 231.7239 231.6635 267.9567 23.6765 0.0594 231.9723 231.9129 268.1239 24.4990 0.0616 232.2349 232.1733 268.2981 25.2905 0.0613 232.4793 232.4180 268.4819 26.1128 0.0596 232.7206 232.6610 268.6540 26.9048 0.0597 232.9598 232.9001 268.8268 27.6965 0.0590 233.2084 233.1494 268.9962 28.5188 0.0605 233.4563 233.3958 269.1577 29.3105 0.0618 233.6918 233.6301 269.3266 30.1328 0.0670 233.9287 233.8617 269.4895 30.9248 0.0710 234.1670 234.0960 269.6474 31.7165 0.0711 234.4093 234.3382 269.8173 32.5388 0.0678 234.6577 234.5900 269.9793 33.3305 0.0647 234.8939 234.8292 270.1510 34.1528 0.0640 235.1329 235.0689 270.3032 34.9445 0.0626 235.3746 235.3120 270.4566 35.7365 0.0610 235.6113 235.5504 270.6037 36.5585 0.0597 235.8434 235.7836 270.7480 37.3505 0.0594 236.0696 236.0103 270.8926 38.1725 0.0554 236.3230 236.2676 271.0351 38.9645 0.0538 236.5510 236.4972 271.1788 39.7565 0.0529 236.7904 236.7374 271.3159 40.6090 0.0491 237.0355 236.9863 271.4459 41.3715 0.0461 237.2497 237.2036 271.5600 42.1943 0.0429 237.4907 237.4478 271.7135 42.9863 0.0408 237.7209 237.6801 271.8490 43.7743 0.0388 237.9654 237.9265 271.9879 44.6225 0.0366 238.2007 238.1641 272.1146 45.3805 0.0345 238.4247 238.3903 272.2376 46.1988 0.0300 238.6671 238.6371 272.3802 47.0170 0.0282 238.9036 238.8755 272.5217 47.7750 0.0257 239.1180 239.0923 272.6610 48.6230 0.0242 239.3535 239.3293 272.7876 49.4110 0.0218 239.5726 239.5508 272.9100 50.2008 0.0156 239.7937 239.7782 273.0360 51.0193 0.0133 240.0191 240.0058 273.1609 51.8080 0.0125 240.2421 240.2296 273.2848 52.6285 0.0099 240.4688 240.4590 273.4193 53.4205 0.0078 240.7054 240.6976 273.5481 54.2125 0.0040 240.9317 240.9277 273.6761 55.0345 -0.0009 241.1507 241.1516 273.8113 55.7965 -0.0048 241.3728 241.3776 273.9585 56.6485 -0.0057 241.6029 241.6086 274.0798 57.4405 -0.0075 241.8358 241.8433 274.2067 58.2325 -0.0126 242.0499 242.0625 274.3318 59.0545 -0.0169 242.2682 242.2851 274.4686 59.8465 -0.0215 242.5041 242.5256 274.5994 60.6685 -0.0265 242.7421 242.7687 274.7143 61.4605 -0.0292 242.9430 242.9722 274.8607 62.2518 -0.0301 243.1644 243.1945 274.9845 63.0743 -0.0330 243.3868 243.4198 275.1116 63.8658 -0.0385 243.5933 243.6319 275.2538 64.6880 -0.0406 243.8216 243.8622 275.3892 65.4800 -0.0451 244.0372 244.0823 275.5170 66.2715 -0.0474 244.2513 244.2987 275.6240 67.1238 -0.0509 244.4874 244.5383 275.7560 67.8858 -0.0538 244.7000 244.7538 275.8887 68.7078 -0.0578 244.9145 244.9723 276.0127 69.4998 -0.0616 245.1288 245.1903 276.1389 70.2915 -0.0665 245.3416 245.4081 276.2783 71.1438 -0.0668 245.5812 245.6480 276.4111 71.9055 -0.0701 245.7805 245.8506 276.5361 72.7278 -0.0759 246.0015 246.0774 276.6591 73.5500 -0.0817 246.2276 246.3093 276.7949 74.3125 -0.0838 246.4133 246.4971 276.9147 75.1645 -0.0891 246.6235 246.7127 277.0340 75.9263 -0.0945 246.8270 246.9214 277.1704 76.7450 -0.0980 247.0527 247.1507 277.3016 77.5630 -0.1025 247.2737 247.3762 277.4325 78.3210 -0.1067 247.4603 247.5669 277.5790 79.1695 -0.1117 247.6966 247.8083 277.7032 79.9280 -0.1141 247.8938 248.0079 277.8170 80.7460 -0.1199 248.0970 248.2168 277.9462 81.5640 -0.1230 248.3168 248.4398 278.0676 82.3220 -0.1252 248.5114 248.6365 278.1975 83.1705 -0.1317 248.7278 248.8596 278.3362 83.9590 -0.1354 248.9270 249.0624 278.4768 84.7493 -0.1430 249.1324 249.2754 278.5863 85.5695 -0.1452 249.3522 249.4974 278.7133 86.3315 -0.1497 249.5605 249.7102 278.8294 87.1835 -0.1509 249.7713 249.9222 278.9799 87.9758 -0.1534 249.9813 250.1347 279.0862 88.7675 -0.1608 250.1787 250.3395 279.2280 89.5898 -0.1655 250.4008 250.5664 279.3564 90.3515 -0.1694 250.5857 250.7551 279.4767 91.2035 -0.1747 250.7980 250.9727 279.5987 91.9958 -0.1794 250.9953 251.1746 279.7362 92.7875 -0.1880 251.2037 251.3917 279.8853 93.6095 -0.1917 251.4240 251.6157 280.0015 94.3715 -0.1933 251.6143 251.8076 280.1117 95.2235 -0.1999 251.8290 252.0289 280.2428 96.0155 -0.2047 252.0143 252.2190 280.3651 96.8075 -0.2088 252.2359 252.4447 280.4881 97.6308 -0.2143 252.4278 252.6421 280.6258 98.3935 -0.2195 252.6220 252.8415 280.7632 99.2455 -0.2232 252.8310 253.0542 280.9087 100.0375 -0.2257 253.0273 253.2530 281.0416 100.8305 -0.2296 253.2246 253.4543 281.1907 101.6528 -0.2367 253.4330 253.6697 281.3336 102.4153 -0.2414 253.6184 253.8597 281.4838 103.2675 -0.2470 253.8404 254.0874 281.6294 104.0593 -0.2496 254.0286 254.2783 281.7820 104.8515 -0.2547 254.2210 254.4757 281.9246 105.6743 -0.2599 254.4054 254.6652 282.0701 106.4365 -0.2668 254.5992 254.8660 282.2076 107.2888 -0.2698 254.8216 255.0914 282.3687 108.0505 -0.2733 255.0021 255.2754 282.5265 108.8693 -0.2809 255.2070 255.4880 282.6772 109.6570 -0.2851 255.4059 255.6910 282.8198 110.4450 -0.2869 255.5834 255.8703 282.9559 111.2938 -0.2942 255.8097 256.1039 283.1037 112.0520 -0.2949 255.9870 256.2819 283.2569 112.8710 -0.3033 256.1848 256.4881 283.3815 113.6595 -0.3112 256.3683 256.6795 283.5158 114.4485 -0.3152 256.5753 256.8905 283.6396 115.2968 -0.3214 256.7685 257.0900 283.7839 116.0563 -0.3257 256.9527 257.2784 283.9164 116.8770 -0.3304 257.1555 257.4859 284.0405 117.6695 -0.3351 257.3329 257.6680 284.1435 118.4605 -0.3431 257.5248 257.8679 284.2784 119.2830 -0.3486 257.7260 258.0747 284.4134 120.0448 -0.3538 257.9200 258.2738 284.5395 120.8970 -0.3603 258.1116 258.4719 284.6866 121.6895 -0.3648 258.2984 258.6632 284.7997 122.4805 -0.3679 258.4824 258.8504 284.9048 123.3030 -0.3737 258.6854 259.0591 285.0357 124.0645 -0.3805 258.8598 259.2403 285.1606 124.9168 -0.3889 259.0621 259.4511 285.2914 125.6785 -0.3945 259.2404 259.6350 285.4015 126.5008 -0.4012 259.4374 259.8386 285.5216 127.3238 -0.4056 259.6328 260.0384 285.6360 128.0855 -0.4084 259.8237 260.2321 285.7585 128.9378 -0.4083 260.0132 260.4215 285.8846 129.6995 -0.4157 260.1890 260.6047 285.9976 130.5218 -0.4224 260.3828 260.8052 286.1239 131.3180 -0.4258 260.5806 261.0064 286.2417 132.1095 -0.4294 260.7601 261.1895 286.3548 132.9315 -0.4370 260.9434 261.3804 286.4756 133.7235 -0.4423 261.1222 261.5645 286.5887 134.5455 -0.4464 261.3176 261.7641 286.7327 135.3375 -0.4529 261.5052 261.9581 286.8507 136.1295 -0.4590 261.6880 262.1469 286.9769 136.9515 -0.4638 261.8913 262.3551 287.1148 137.7435 -0.4694 262.0705 262.5399 287.2500 138.5655 -0.4735 262.2575 262.7310 287.3859 139.3575 -0.4793 262.4500 262.9293 287.5209 140.1485 -0.4846 262.6228 263.1074 287.6692 140.9668 -0.5047 262.8175 263.3222 287.8002 141.7550 -0.5643 262.9949 263.5591 287.9403 142.5730 -0.5683 263.1830 263.7513 288.0848 143.3608 -0.5495 263.3585 263.9081 288.2337 144.1500 -0.5459 263.5422 264.0882 288.3614 144.9683 -0.5466 263.7310 264.2776 288.5123 145.7570 -0.5427 263.9054 264.4481 288.6692 146.5758 -0.5385 264.0930 264.6315 288.8030 147.3645 -0.5445 264.2708 264.8153 288.9283 148.1543 -0.5548 264.4658 265.0206 289.0836 149.0048 -0.5550 264.6499 265.2049 289.2347 149.7655 -0.5521 264.8158 265.3679 289.3657 150.5865 -0.5546 264.9999 265.5545 289.5110 151.3785 -0.5611 265.1924 265.7535 289.6596 152.1705 -0.5651 265.3606 265.9257 289.7900 152.9925 -0.5712 265.5499 266.1210 289.9446 153.7845 -0.5768 265.7200 266.2968 290.0894 154.6065 -0.5856 265.8971 266.4827 290.2470 155.3985 -0.5883 266.0757 266.6640 290.3819 156.1905 -0.5937 266.2546 266.8483 290.5038 157.0128 -0.5976 266.4591 267.0567 290.6600 157.7755 -0.6062 266.6327 267.2389 290.7878 158.6275 -0.6105 266.8265 267.4370 290.9582 159.4195 -0.6156 266.9961 267.6116 291.0689 160.2115 -0.6212 267.1636 267.7847 291.1865 161.0335 -0.6252 267.3553 267.9806 291.3149 161.7963 -0.6289 267.5157 268.1446 291.4370 162.6503 -0.6336 267.7196 268.3532 291.5688 163.4420 -0.6395 267.8990 268.5384 291.6791 164.2335 -0.6464 268.0605 268.7069 291.7949 165.0558 -0.6545 268.2326 268.8870 291.9239 165.8175 -0.6623 268.4107 269.0730 292.0481 166.6698 -0.6661 268.6054 269.2714 292.1751 167.4618 -0.6682 268.7799 269.4481 292.2866 168.2535 -0.6756 268.9476 269.6232 292.4019 169.0758 -0.7045 269.1331 269.8376 292.5154 169.8375 -0.7457 269.2905 270.0362 292.6348 170.6898 -0.7721 269.4829 270.2550 292.7647 171.4818 -0.7607 269.6605 270.4212 292.8744 172.2730 -0.7790 269.8351 270.6140 292.9955 173.0910 -0.7526 270.0287 270.7813 293.1428 173.8490 -0.7512 270.1938 270.9450 293.2714 174.7000 -0.7577 270.3755 271.1332 293.4061 175.4890 -0.7678 270.5444 271.3122 293.5259 176.2770 -0.7737 270.7112 271.4848 293.6603 177.0950 -0.7832 270.8894 271.6726 293.8051 177.8830 -0.7747 271.0553 271.8300 293.9373 178.7025 -0.7691 271.2382 272.0073 294.0715 179.4918 -0.7718 271.4136 272.1854 294.1946 180.2825 -0.7762 271.5899 272.3661 294.3412 181.1040 -0.7846 271.7705 272.5552 294.4782 181.8955 -0.8017 271.9344 272.7361 294.6051 182.7178 -0.8101 272.1197 272.9299 294.7519 183.5098 -0.8138 272.2943 273.1081 294.8814 184.3015 -0.8192 272.4575 273.2768 295.0143 185.1238 -0.8178 272.6248 273.4426 295.1725 185.9155 -0.8636 272.8034 273.6669 295.2928 186.7378 -0.8180 272.9733 273.7913 295.4184 187.5298 -0.7924 273.1301 273.9225 295.5608 188.3215 -0.7892 273.3020 274.0911 295.7050 189.1435 -0.7939 273.4905 274.2844 295.8467 189.9355 -0.7973 273.6627 274.4600 295.9886 190.7578 -0.8030 273.8468 274.6497 296.1189 191.5498 -0.8339 274.0046 274.8385 296.2545 192.3415 -0.8498 274.1705 275.0203 296.3806 193.1635 -0.8243 274.3414 275.1657 296.5279 193.9555 -0.8205 274.5049 275.3254 296.6741 194.7775 -0.8238 274.6914 275.5152 296.8046 195.5695 -0.8288 274.8511 275.6799 296.9567 196.3615 -0.8342 275.0353 275.8695 297.0834 197.2140 -0.8411 275.2084 276.0495 297.2226 197.9765 -0.8453 275.3698 276.2151 297.3493 198.7993 -0.8523 275.5541 276.4064 297.4912 199.5915 -0.8603 275.7285 276.5888 297.6220 200.3835 -0.8718 275.8802 276.7520 297.7587 201.2355 -0.8816 276.0734 276.9549 297.8898 201.9973 -0.8858 276.2222 277.1080 298.0346 202.8188 -0.8909 276.4073 277.2982 298.1889 203.6413 -0.8952 276.5717 277.4669 298.3212 204.4035 -0.8937 276.7345 277.6282 298.4538 205.2548 -0.8995 276.9040 277.8035 298.6015 206.0133 -0.9043 277.0860 277.9902 298.7120 206.8310 -0.9085 277.2489 278.1573 298.8516 207.6193 -0.9098 277.4217 278.3315 299.0009 208.4073 -0.9147 277.5709 278.4856 299.1362 209.2560 -0.9175 277.7473 278.6648 299.2740 210.0143 -0.9229 277.9036 278.8265 299.4017 210.8338 -0.9302 278.0847 279.0149 299.5532 211.6523 -0.9353 278.2455 279.1809 299.6731 212.4120 -0.9394 278.4084 279.3479 299.8023 213.2615 -0.9423 278.5841 279.5263 299.9468 214.0525 -0.9588 278.7495 279.7083 300.0932 214.8443 -0.9723 278.9044 279.8766 300.2442 215.6663 -0.9646 279.0809 280.0455 300.3859 216.4283 -0.9633 279.2298 280.1931 300.4869 217.2805 -0.9695 279.4232 280.3928 300.6444 218.0720 -0.9762 279.5962 280.5724 300.7683 218.8635 -0.9826 279.7536 280.7363 300.8860 219.6860 -0.9883 279.9162 280.9045 301.0355 220.4475 -0.9924 280.0815 281.0739 301.1561 221.3000 -0.9946 280.2643 281.2589 301.3003 222.0918 -0.9982 280.4382 281.4364 301.4255 222.8835 -1.0041 280.5829 281.5869 301.5671 223.7058 -1.0077 280.7447 281.7524 301.6964 224.4675 -1.0119 280.8989 281.9108 301.8171 225.3200 -1.0166 281.0811 282.0977 301.9724 226.1118 -1.0233 281.2400 282.2633 302.0979 226.9035 -1.0258 281.3923 282.4180 302.2324 227.7258 -1.0290 281.5600 282.5890 302.3641 228.5175 -1.0355 281.7340 282.7695 302.4873 229.3405 -1.0412 281.9049 282.9461 302.6168 230.1328 -1.0445 282.0670 283.1115 302.7554 230.9245 -1.0496 282.2321 283.2817 302.8866 231.7465 -1.0549 282.3997 283.4546 303.0247 232.5385 -1.0602 282.5711 283.6313 303.1443 233.3615 -1.0632 282.7317 283.7949 303.2863 234.1535 -1.0696 282.9013 283.9709 303.4101 234.9455 -1.0764 283.0625 284.1389 303.5442 235.7675 -1.0822 283.2230 284.3052 303.6844 236.5595 -1.0839 283.3990 284.4829 303.8142 237.3800 -1.0867 283.5737 284.6604 303.9511 238.1678 -1.0923 283.7266 284.8189 304.0706 238.9560 -1.0945 283.9010 284.9955 304.1965 239.7745 -1.1001 284.0478 285.1478 304.3336 240.5330 -1.1032 284.2069 285.3102 304.4459 241.3810 -1.1069 284.3790 285.4860 304.5787 242.1690 -1.1107 284.5362 285.6469 304.6952 242.9580 -1.1183 284.6990 285.8173 304.8230 243.7763 -1.1223 284.8563 285.9786 304.9570 244.5650 -1.1259 285.0058 286.1317 305.0853 245.3853 -1.1293 285.1842 286.3135 305.2183 246.1755 -1.1322 285.3536 286.4857 305.3584 246.9665 -1.1381 285.5109 286.6490 305.4795 247.7885 -1.1405 285.6823 286.8227 305.6031 248.5505 -1.1468 285.8268 286.9736 305.7182 249.4025 -1.1530 286.0119 287.1649 305.8562 250.1645 -1.1586 286.1613 287.3199 305.9908 250.9865 -1.1610 286.3264 287.4873 306.1056 251.8085 -1.1652 286.4796 287.6448 306.2274 252.5705 -1.1705 286.6533 287.8239 306.3443 253.4225 -1.1763 286.8172 287.9935 306.4693 254.1845 -1.1821 286.9729 288.1551 306.6035 255.0065 -1.1847 287.1148 288.2995 306.7202 255.8285 -1.1866 287.2761 288.4627 306.8625 256.5905 -1.1914 287.4428 288.6342 306.9667 257.4425 -1.1960 287.6186 288.8146 307.0955 258.2043 -1.2021 287.7705 288.9726 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