DTA measure 1elso Date: 2024326:111 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 899.94 s Mass = 1367.600 mg data_number = 1115 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3095 0.3931 224.6002 224.2070 265.6069 2.1615 0.3936 224.8852 224.4917 265.6263 2.9243 0.3970 225.1253 224.7283 265.6283 3.7465 0.3981 225.4113 225.0131 265.6493 4.5685 0.3995 225.6909 225.2914 265.6662 5.3303 0.3980 225.9417 225.5437 265.6823 6.1825 0.3976 226.2069 225.8093 265.7098 6.9443 0.4000 226.4654 226.0654 265.7334 7.7658 0.4022 226.7297 226.3275 265.7590 8.5883 0.4009 226.9891 226.5882 265.8132 9.3498 0.4015 227.2252 226.8237 265.8525 10.2020 0.4045 227.5197 227.1152 265.9256 10.9635 0.4030 227.7668 227.3638 265.9875 11.7865 0.3994 228.0168 227.6174 266.0773 12.6088 0.4026 228.2786 227.8760 266.1415 13.3705 0.4053 228.5307 228.1254 266.1985 14.2228 0.4031 228.7947 228.3916 266.3074 14.9918 0.4057 229.0507 228.6450 266.4094 15.8198 0.4040 229.2944 228.8904 266.5174 16.6118 0.4023 229.5502 229.1478 266.6533 17.4035 0.4034 229.7875 229.3842 266.7667 18.2563 0.4041 230.0612 229.6571 266.9162 19.0178 0.4044 230.2958 229.8914 267.0397 19.8360 0.4058 230.5556 230.1498 267.1798 20.6240 0.4056 230.7998 230.3942 267.3203 21.4120 0.4083 231.0432 230.6349 267.4546 22.2300 0.4095 231.2884 230.8789 267.6146 23.0180 0.4109 231.5469 231.1359 267.7518 23.8370 0.4078 231.7790 231.3713 267.9039 24.6253 0.4024 232.0204 231.6180 268.0660 25.4148 0.3998 232.2598 231.8600 268.2278 26.2343 0.3943 232.5098 232.1155 268.3903 27.0233 0.3910 232.7493 232.3583 268.5333 27.8438 0.3913 233.0029 232.6115 268.6975 28.6350 0.3873 233.2231 232.8358 268.8649 29.4265 0.3852 233.4584 233.0732 269.0224 30.2488 0.3864 233.7067 233.3203 269.1924 31.0105 0.3837 233.9279 233.5442 269.3448 31.8628 0.3803 234.1805 233.8002 269.5090 32.6548 0.3766 234.4102 234.0336 269.6757 33.4465 0.3735 234.6622 234.2887 269.8366 34.2685 0.3712 234.8920 234.5207 270.0127 35.0305 0.3668 235.1212 234.7544 270.1703 35.8840 0.3653 235.3847 235.0193 270.3347 36.6465 0.3577 235.5990 235.2413 270.4738 37.4688 0.3573 235.8171 235.4598 270.6326 38.2908 0.3553 236.0774 235.7220 270.7723 39.0525 0.3495 236.3088 235.9593 270.9120 39.9045 0.3467 236.5568 236.2101 271.0681 40.6665 0.3440 236.7843 236.4403 271.2146 41.4885 0.3443 237.0138 236.6695 271.3681 42.3105 0.3407 237.2608 236.9201 271.5129 43.0725 0.3397 237.4697 237.1299 271.6443 43.9245 0.3313 237.7087 237.3774 271.8113 44.7165 0.3273 237.9339 237.6066 271.9553 45.5095 0.3240 238.1561 237.8321 272.1078 46.3318 0.3214 238.4034 238.0820 272.2534 47.0945 0.3169 238.6195 238.3026 272.3730 47.9460 0.3142 238.8634 238.5492 272.5186 48.7383 0.3099 239.0792 238.7693 272.6526 49.5305 0.3049 239.2963 238.9915 272.7652 50.3528 0.3000 239.5519 239.2519 272.9086 51.1430 0.2997 239.7672 239.4675 273.0344 51.9610 0.2932 239.9913 239.6981 273.1711 52.7493 0.2895 240.1997 239.9101 273.2911 53.5373 0.2840 240.4253 240.1412 273.4030 54.3555 0.2826 240.6588 240.3762 273.5251 55.1438 0.2761 240.8854 240.6094 273.6308 55.9618 0.2717 241.1047 240.8330 273.7595 56.7500 0.2688 241.3238 241.0550 273.8761 57.5385 0.2633 241.5460 241.2827 273.9891 58.3895 0.2557 241.7998 241.5441 274.1125 59.1510 0.2518 242.0079 241.7561 274.2186 59.9723 0.2471 242.2260 241.9789 274.3383 60.7645 0.2432 242.4276 242.1843 274.4673 61.5560 0.2407 242.6312 242.3905 274.5758 62.4085 0.2339 242.8847 242.6508 274.6915 63.1700 0.2304 243.0923 242.8618 274.8342 63.9923 0.2241 243.3118 243.0876 274.9675 64.7843 0.2189 243.5414 243.3225 275.0938 65.5755 0.2164 243.7461 243.5298 275.2243 66.4280 0.2133 243.9688 243.7555 275.3631 67.1898 0.2057 244.1742 243.9685 275.4859 68.0118 0.2008 244.4036 244.2028 275.6271 68.8038 0.1953 244.6160 244.4207 275.7547 69.5955 0.1918 244.8270 244.6352 275.8869 70.4478 0.1851 245.0418 244.8568 276.0434 71.2095 0.1809 245.2529 245.0719 276.1566 72.0318 0.1729 245.4690 245.2962 276.2882 72.8538 0.1687 245.6765 245.5078 276.4298 73.6155 0.1639 245.9022 245.7383 276.5722 74.4678 0.1635 246.1269 245.9634 276.7090 75.2295 0.1554 246.3189 246.1634 276.8221 76.0518 0.1502 246.5309 246.3807 276.9659 76.8738 0.1465 246.7466 246.6000 277.1170 77.6355 0.1414 246.9304 246.7890 277.2589 78.4875 0.1363 247.1688 247.0324 277.4033 79.2798 0.1293 247.3777 247.2483 277.5387 80.0725 0.1226 247.5892 247.4666 277.6724 80.8945 0.1166 247.8032 247.6866 277.8204 81.6565 0.1139 248.0065 247.8925 277.9593 82.5085 0.1146 248.2209 248.1064 278.0899 83.2975 0.1105 248.4125 248.3019 278.2155 84.0860 0.1043 248.6326 248.5284 278.3634 84.9043 0.0947 248.8505 248.7558 278.5080 85.6630 0.0876 249.0400 248.9524 278.6364 86.5133 0.0833 249.2589 249.1755 278.7782 87.2740 0.0787 249.4534 249.3748 278.9030 88.0920 0.0736 249.6642 249.5907 279.0429 88.8803 0.0656 249.8562 249.7905 279.1586 89.6708 0.0599 250.0440 249.9842 279.3021 90.5198 0.0592 250.2546 250.1953 279.4616 91.2798 0.0532 250.4627 250.4095 279.5740 92.1015 0.0447 250.6870 250.6424 279.7316 92.8935 0.0400 250.8837 250.8437 279.8516 93.6848 0.0359 251.0889 251.0530 279.9905 94.5358 0.0290 251.2807 251.2517 280.1374 95.2975 0.0220 251.4875 251.4656 280.2585 96.1195 0.0154 251.6906 251.6752 280.3996 96.8873 0.0086 251.8697 251.8611 280.5098 97.7175 0.0061 252.1037 252.0976 280.6425 98.5395 0.0016 252.3049 252.3033 280.7997 99.3015 -0.0035 252.4905 252.4940 280.9249 100.1535 -0.0121 252.7080 252.7201 281.0784 100.9155 -0.0125 252.8886 252.9011 281.2101 101.7375 -0.0200 253.0917 253.1116 281.3317 102.5295 -0.0298 253.3033 253.3331 281.4503 103.3215 -0.0345 253.4858 253.5203 281.6045 104.1735 -0.0408 253.6961 253.7369 281.7350 104.9355 -0.0465 253.8997 253.9463 281.8701 105.7580 -0.0506 254.0905 254.1412 281.9889 106.5505 -0.0566 254.2805 254.3371 282.1211 107.3468 -0.0599 254.4704 254.5304 282.2610 108.1690 -0.0677 254.6713 254.7390 282.3906 108.9305 -0.0744 254.8680 254.9424 282.5139 109.7833 -0.0830 255.0846 255.1676 282.6764 110.5758 -0.0871 255.2652 255.3523 282.8031 111.3685 -0.0921 255.4634 255.5555 282.9514 112.1910 -0.0994 255.6758 255.7751 283.0695 112.9535 -0.1044 255.8566 255.9610 283.1902 113.8058 -0.1109 256.0614 256.1724 283.3206 114.5675 -0.1156 256.2398 256.3554 283.4570 115.3898 -0.1217 256.4492 256.5708 283.5785 116.2098 -0.1278 256.6427 256.7705 283.7315 116.9670 -0.1334 256.8333 256.9668 283.8452 117.8150 -0.1381 257.0259 257.1639 283.9693 118.5730 -0.1459 257.1963 257.3422 284.1113 119.3910 -0.1531 257.3987 257.5518 284.2650 120.2093 -0.1573 257.5985 257.7557 284.3901 120.9680 -0.1645 257.7737 257.9382 284.5230 121.8175 -0.1717 257.9769 258.1487 284.6714 122.5765 -0.1746 258.1585 258.3331 284.7882 123.3958 -0.1821 258.3617 258.5438 284.9271 124.2150 -0.1885 258.5498 258.7382 285.0674 124.9765 -0.1967 258.7364 258.9332 285.1888 125.8288 -0.1985 258.9372 259.1357 285.3104 126.5905 -0.2039 259.1128 259.3167 285.4528 127.4128 -0.2084 259.3267 259.5351 285.5787 128.2040 -0.2132 259.5056 259.7188 285.6993 128.9955 -0.2183 259.6901 259.9084 285.8462 129.8178 -0.2252 259.8588 260.0840 285.9805 130.6095 -0.2318 260.0547 260.2865 286.0981 131.4318 -0.2360 260.2437 260.4797 286.2497 132.2238 -0.2427 260.4354 260.6780 286.3858 133.0155 -0.2492 260.6223 260.8716 286.4966 133.8375 -0.2541 260.8279 261.0820 286.6312 134.6295 -0.2594 261.0318 261.2911 286.7627 135.4525 -0.2668 261.2040 261.4708 286.8975 136.2448 -0.2727 261.3684 261.6411 287.0305 137.0365 -0.2788 261.5580 261.8367 287.1572 137.8618 -0.2797 261.7562 262.0359 287.3088 138.6245 -0.2860 261.9484 262.2344 287.4051 139.4765 -0.2937 262.1443 262.4380 287.5534 140.2685 -0.3015 262.3207 262.6222 287.6933 141.0605 -0.3080 262.4965 262.8045 287.8075 141.8828 -0.3116 262.6902 263.0018 287.9398 142.6455 -0.3173 262.8671 263.1844 288.0743 143.4975 -0.3260 263.0568 263.3829 288.2046 144.2895 -0.3315 263.2364 263.5680 288.3446 145.0825 -0.3390 263.4115 263.7505 288.4522 145.9048 -0.3447 263.6144 263.9591 288.5901 146.6675 -0.3505 263.7868 264.1373 288.7056 147.5195 -0.3559 263.9985 264.3544 288.8314 148.3093 -0.3563 264.1585 264.5147 288.9575 149.0973 -0.3607 264.3515 264.7122 289.0964 149.9155 -0.3667 264.5195 264.8862 289.2198 150.6733 -0.3726 264.7042 265.0768 289.3450 151.5230 -0.3820 264.8919 265.2738 289.4815 152.3120 -0.3871 265.0669 265.4539 289.6060 153.0998 -0.3908 265.2574 265.6482 289.7352 153.9188 -0.3956 265.4407 265.8363 289.8842 154.6780 -0.4020 265.6031 266.0051 289.9995 155.5285 -0.4062 265.7995 266.2057 290.1320 156.3185 -0.4113 265.9753 266.3865 290.2478 157.1105 -0.4203 266.1385 266.5588 290.3792 157.9320 -0.4235 266.3141 266.7376 290.5149 158.6933 -0.4273 266.5002 266.9275 290.6317 159.5455 -0.4360 266.6981 267.1340 290.7630 160.3075 -0.4406 266.8678 267.3084 290.8795 161.1295 -0.4447 267.0472 267.4919 291.0261 161.9513 -0.4491 267.2394 267.6885 291.1599 162.7130 -0.4547 267.4021 267.8568 291.2816 163.5653 -0.4618 267.5897 268.0515 291.4216 164.3273 -0.4665 267.7655 268.2320 291.5365 165.1488 -0.4706 267.9562 268.4268 291.6686 165.9710 -0.4761 268.1310 268.6071 291.7972 166.7325 -0.4826 268.3048 268.7874 291.9191 167.5853 -0.4876 268.4857 268.9732 292.0519 168.3478 -0.4893 268.6668 269.1561 292.1701 169.1698 -0.4944 268.8384 269.3328 292.2991 169.9918 -0.5024 269.0197 269.5221 292.4283 170.7535 -0.5052 269.1876 269.6928 292.5579 171.6058 -0.5116 269.3841 269.8957 292.6846 172.3978 -0.5176 269.5579 270.0756 292.8378 173.1895 -0.5225 269.7237 270.2462 292.9688 174.0118 -0.5277 269.8991 270.4267 293.1085 174.7735 -0.5322 270.0760 270.6082 293.2423 175.6258 -0.5417 270.2588 270.8006 293.4004 176.4178 -0.5445 270.4220 270.9665 293.5418 177.2095 -0.5504 270.6112 271.1616 293.6885 178.0315 -0.5541 270.7952 271.3493 293.8416 178.7935 -0.5585 270.9485 271.5070 293.9595 179.6460 -0.5645 271.1374 271.7018 294.1146 180.4360 -0.5701 271.3162 271.8863 294.2527 181.2240 -0.5745 271.4870 272.0615 294.4104 182.0423 -0.5816 271.6531 272.2347 294.5554 182.8010 -0.5845 271.8316 272.4161 294.7125 183.6490 -0.5893 272.0159 272.6052 294.8573 184.4370 -0.5940 272.1694 272.7634 294.9799 185.2250 -0.5990 272.3442 272.9432 295.1333 186.0448 -0.6096 272.5246 273.1342 295.2633 186.8340 -0.6133 272.6907 273.3040 295.3861 187.6545 -0.6161 272.8674 273.4835 295.5285 188.4433 -0.6203 273.0358 273.6561 295.6727 189.2338 -0.6263 273.2080 273.8343 295.7963 190.0845 -0.6360 273.4000 274.0361 295.9247 190.8465 -0.6376 273.5541 274.1918 296.0345 191.6685 -0.6436 273.7187 274.3623 296.1672 192.4605 -0.6510 273.8962 274.5472 296.2828 193.2525 -0.6562 274.0726 274.7288 296.4003 194.1045 -0.6589 274.2469 274.9057 296.5426 194.8665 -0.6648 274.4013 275.0661 296.6601 195.6885 -0.6698 274.5874 275.2572 296.7825 196.4805 -0.6753 274.7352 275.4106 296.9152 197.2725 -0.6830 274.9143 275.5973 297.0373 198.1245 -0.6856 275.1056 275.7911 297.1597 198.8865 -0.6885 275.2803 275.9687 297.2672 199.7085 -0.6928 275.4448 276.1376 297.3922 200.5305 -0.6980 275.6159 276.3139 297.5158 201.2925 -0.7031 275.7771 276.4801 297.6229 202.1445 -0.7093 275.9591 276.6684 297.7526 202.9065 -0.7127 276.1320 276.8447 297.8697 203.7283 -0.7184 276.2923 277.0107 297.9988 204.5505 -0.7240 276.4689 277.1929 298.1232 205.3120 -0.7300 276.6200 277.3500 298.2532 206.1733 -0.7340 276.8103 277.5442 298.3877 206.9348 -0.7364 276.9666 277.7030 298.5178 207.7575 -0.7388 277.1422 277.8810 298.6640 208.5498 -0.7466 277.3066 278.0532 298.8007 209.3425 -0.7532 277.4712 278.2244 298.9238 210.1953 -0.7577 277.6653 278.4231 299.0639 210.9575 -0.7614 277.7990 278.5604 299.1971 211.7795 -0.7651 277.9821 278.7472 299.3306 212.5980 -0.7669 278.1582 278.9252 299.4841 213.3560 -0.7740 278.3168 279.0908 299.6082 214.2040 -0.7790 278.4835 279.2626 299.7556 214.9620 -0.7841 278.6484 279.4324 299.8905 215.7800 -0.7903 278.8214 279.6117 300.0408 216.5980 -0.7915 278.9963 279.7877 300.1729 217.3565 -0.7972 279.1411 279.9383 300.3047 218.2058 -0.8036 279.3120 280.1156 300.4366 218.9643 -0.8100 279.4757 280.2857 300.5603 219.7845 -0.8133 279.6391 280.4524 300.7055 220.6048 -0.8144 279.8136 280.6280 300.8342 221.3663 -0.8220 279.9734 280.7954 300.9670 222.2180 -0.8273 280.1409 280.9681 301.1261 222.9795 -0.8311 280.2905 281.1216 301.2493 223.8018 -0.8361 280.4579 281.2940 301.3865 224.6240 -0.8424 280.6494 281.4918 301.5213 225.3855 -0.8471 280.7985 281.6456 301.6666 226.2378 -0.8508 280.9732 281.8240 301.8052 226.9995 -0.8551 281.1350 281.9902 301.9373 227.8218 -0.8595 281.2852 282.1447 302.0737 228.6438 -0.8649 281.4573 282.3222 302.2121 229.4055 -0.8718 281.6139 282.4857 302.3429 230.2578 -0.8771 281.7880 282.6651 302.4842 231.0195 -0.8841 281.9397 282.8238 302.6098 231.8418 -0.8899 282.1139 283.0038 302.7571 232.6335 -0.8935 282.2656 283.1591 302.8916 233.4255 -0.9004 282.4372 283.3376 303.0359 234.2783 -0.9049 282.6209 283.5258 303.1704 235.0405 -0.9100 282.7815 283.6915 303.3003 235.8625 -0.9135 282.9604 283.8739 303.4262 236.6845 -0.9159 283.1032 284.0190 303.5672 237.4465 -0.9195 283.2547 284.1741 303.7097 238.2985 -0.9256 283.4280 284.3535 303.8499 239.0605 -0.9298 283.5931 284.5230 303.9591 239.8825 -0.9351 283.7401 284.6752 304.1024 240.6765 -0.9403 283.9105 284.8508 304.2287 241.4705 -0.9471 284.0581 285.0052 304.3723 242.3230 -0.9529 284.2413 285.1942 304.5126 243.0853 -0.9567 284.4057 285.3623 304.6368 243.9083 -0.9607 284.5569 285.5177 304.7797 244.7003 -0.9661 284.7473 285.7134 304.9230 245.4890 -0.9696 284.9051 285.8747 305.0512 246.3083 -0.9797 285.0583 286.0379 305.1924 247.0665 -0.9870 285.2115 286.1986 305.3206 247.9158 -0.9847 285.3831 286.3677 305.4631 248.7055 -0.9880 285.5475 286.5355 305.6066 249.4940 -0.9947 285.6848 286.6796 305.7502 250.3123 -0.9985 285.8550 286.8534 305.8823 251.0710 -1.0024 286.0196 287.0220 305.9962 251.9205 -1.0088 286.1871 287.1959 306.1198 252.7100 -1.0119 286.3420 287.3539 306.2575 253.5003 -1.0160 286.5030 287.5190 306.4087 254.3215 -1.0207 286.6750 287.6957 306.5370 255.0835 -1.0269 286.8266 287.8535 306.6629 255.9355 -1.0307 286.9873 288.0180 306.8219 256.6975 -1.0363 287.1457 288.1820 306.9491 257.5195 -1.0412 287.2899 288.3311 307.0818 258.3115 -1.0434 287.4449 288.4883 307.2257 259.1035 -1.0495 287.6257 288.6752 307.3501 259.9555 -1.0532 287.8102 288.8634 307.5058 260.7175 -1.0550 287.9596 289.0146 307.6128 261.5390 -1.0605 288.1180 289.1785 307.7629 262.3315 -1.0637 288.2622 289.3259 307.8919 263.1233 -1.0696 288.4077 289.4773 308.0306 263.9453 -1.0767 288.5927 289.6694 308.1726 264.7370 -1.0805 288.7465 289.8270 308.2894 265.5590 -1.0833 288.9140 289.9973 308.4318 266.3508 -1.0864 289.0744 290.1608 308.5691 267.1428 -1.0921 289.2292 290.3213 308.6909 267.9648 -1.0963 289.3942 290.4905 308.8456 268.7265 -1.1047 289.5566 290.6613 308.9804 269.5788 -1.1077 289.7152 290.8228 309.1285 270.3708 -1.1126 289.8626 290.9752 309.2522 271.1625 -1.1169 290.0143 291.1312 309.3835 271.9850 -1.1236 290.1919 291.3155 309.5188 272.7475 -1.1264 290.3404 291.4668 309.6479 273.5998 -1.1305 290.5203 291.6508 309.7836 274.3918 -1.1348 290.6575 291.7923 309.9286 275.1845 -1.1389 290.8253 291.9642 310.0572 276.0070 -1.1417 290.9825 292.1242 310.1849 276.7693 -1.1473 291.1348 292.2821 310.3150 277.6180 -1.1509 291.3074 292.4583 310.4653 278.3760 -1.1558 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