DTA measure 1meres2 Test Date: 2023920:1459 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 5.00 C/min Mtime = 947.52 s Mass = 1436.900 mg data_number = 1176 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.0905 -0.2286 265.6996 265.9282 267.7525 2.1193 -0.2237 265.7338 265.9575 267.7528 2.9115 -0.2201 265.7598 265.9799 267.7523 3.7028 -0.2159 265.7868 266.0028 267.7534 4.5248 -0.2125 265.8121 266.0246 267.7567 5.2855 -0.2087 265.8352 266.0440 267.7565 6.1375 -0.2047 265.8619 266.0666 267.7568 6.9295 -0.2011 265.8903 266.0915 267.7585 7.7215 -0.1973 265.9181 266.1153 267.7608 8.5435 -0.1936 265.9489 266.1426 267.7633 9.3055 -0.1904 265.9728 266.1633 267.7649 10.1575 -0.1869 266.0010 266.1879 267.7693 10.9198 -0.1835 266.0248 266.2082 267.7744 11.7410 -0.1801 266.0491 266.2293 267.7805 12.5615 -0.1769 266.0729 266.2498 267.7913 13.3235 -0.1736 266.0971 266.2707 267.8045 14.1755 -0.1704 266.1236 266.2940 267.8201 14.9375 -0.1676 266.1468 266.3144 267.8350 15.7588 -0.1637 266.1720 266.3358 267.8559 16.5515 -0.1601 266.1934 266.3535 267.8785 17.3418 -0.1571 266.2167 266.3738 267.9060 18.1940 -0.1536 266.2412 266.3948 267.9412 18.9563 -0.1511 266.2628 266.4139 267.9769 19.7778 -0.1485 266.2880 266.4365 268.0193 20.5700 -0.1457 266.3102 266.4560 268.0649 21.3615 -0.1433 266.3334 266.4768 268.1130 22.1843 -0.1408 266.3584 266.4992 268.1677 22.9458 -0.1387 266.3821 266.5207 268.2233 23.7978 -0.1355 266.4066 266.5422 268.2916 24.5900 -0.1326 266.4299 266.5626 268.3619 25.3815 -0.1291 266.4540 266.5831 268.4348 26.2038 -0.1273 266.4778 266.6051 268.5159 26.9655 -0.1259 266.5005 266.6264 268.5925 27.8175 -0.1246 266.5264 266.6510 268.6833 28.5840 -0.1230 266.5502 266.6731 268.7689 29.4075 -0.1219 266.5749 266.6968 268.8688 30.1995 -0.1204 266.6012 266.7215 268.9706 30.9915 -0.1183 266.6227 266.7410 269.0769 31.8435 -0.1143 266.6491 266.7633 269.1972 32.6055 -0.1119 266.6721 266.7840 269.3081 33.4275 -0.1104 266.6954 266.8058 269.4327 34.2195 -0.1081 266.7204 266.8285 269.5552 35.0115 -0.1057 266.7434 266.8491 269.6809 35.8335 -0.1038 266.7676 266.8714 269.8178 36.6255 -0.1037 266.7922 266.8959 269.9536 37.4475 -0.1046 266.8191 266.9237 270.0960 38.2395 -0.1057 266.8442 266.9499 270.2385 39.0315 -0.1069 266.8715 266.9784 270.3818 39.8555 -0.1080 266.9007 267.0087 270.5326 40.6175 -0.1089 266.9253 267.0342 270.6731 41.4690 -0.1099 266.9497 267.0596 270.8354 42.2313 -0.1109 266.9725 267.0835 270.9819 43.0533 -0.1124 267.0011 267.1134 271.1436 43.8753 -0.1140 267.0277 267.1416 271.3043 44.6365 -0.1150 267.0524 267.1674 271.4553 45.4890 -0.1164 267.0819 267.1983 271.6269 46.2510 -0.1179 267.1093 267.2272 271.7802 47.0730 -0.1194 267.1355 267.2549 271.9469 47.8653 -0.1210 267.1609 267.2818 272.1071 48.6568 -0.1223 267.1882 267.3105 272.2691 49.4788 -0.1239 267.2159 267.3398 272.4341 50.2708 -0.1263 267.2431 267.3694 272.5922 51.0928 -0.1278 267.2720 267.3998 272.7580 51.8845 -0.1291 267.2987 267.4278 272.9142 52.6765 -0.1317 267.3264 267.4581 273.0689 53.4985 -0.1339 267.3563 267.4902 273.2308 54.2605 -0.1372 267.3854 267.5226 273.3774 55.1125 -0.1411 267.4197 267.5608 273.5381 55.9045 -0.1439 267.4500 267.5939 273.6879 56.6965 -0.1476 267.4824 267.6299 273.8341 57.5185 -0.1515 267.5137 267.6653 273.9812 58.2828 -0.1550 267.5417 267.6966 274.1177 59.1355 -0.1589 267.5744 267.7333 274.2668 59.9000 -0.1623 267.6068 267.7691 274.3974 60.7245 -0.1660 267.6411 267.8071 274.5345 61.5188 -0.1698 267.6723 267.8421 274.6640 62.3125 -0.1735 267.7041 267.8776 274.7898 63.1345 -0.1776 267.7389 267.9165 274.9172 63.8965 -0.1818 267.7731 267.9548 275.0307 64.7485 -0.1862 267.8074 267.9936 275.1540 65.5105 -0.1899 267.8387 268.0286 275.2600 66.3325 -0.1942 267.8693 268.0636 275.3745 67.1543 -0.1985 267.9026 268.1011 275.4859 67.9163 -0.2028 267.9347 268.1375 275.5823 68.7680 -0.2076 267.9732 268.1808 275.6870 69.5303 -0.2119 268.0066 268.2185 275.7795 70.3518 -0.2165 268.0397 268.2561 275.8788 71.1443 -0.2212 268.0743 268.2955 275.9710 71.9358 -0.2258 268.1081 268.3339 276.0600 72.7880 -0.2308 268.1443 268.3752 276.1498 73.5528 -0.2351 268.1805 268.4155 276.2287 74.3748 -0.2399 268.2171 268.4570 276.3104 75.1668 -0.2439 268.2494 268.4933 276.3878 75.9585 -0.2488 268.2851 268.5339 276.4638 76.7808 -0.2532 268.3214 268.5746 276.5388 77.5425 -0.2572 268.3542 268.6115 276.6065 78.3948 -0.2621 268.3944 268.6565 276.6794 79.1868 -0.2665 268.4328 268.6993 276.7479 79.9785 -0.2707 268.4695 268.7402 276.8143 80.8005 -0.2748 268.5071 268.7818 276.8795 81.5625 -0.2784 268.5435 268.8219 276.9383 82.4145 -0.2827 268.5837 268.8664 277.0033 83.1770 -0.2870 268.6185 268.9055 277.0625 84.0005 -0.2915 268.6554 268.9468 277.1229 84.7925 -0.2954 268.6912 268.9866 277.1812 85.5845 -0.3001 268.7288 269.0289 277.2384 86.4365 -0.3050 268.7708 269.0758 277.2984 87.1985 -0.3090 268.8072 269.1162 277.3530 88.0205 -0.3132 268.8460 269.1591 277.4130 88.8125 -0.3175 268.8854 269.2029 277.4705 89.6045 -0.3217 268.9245 269.2461 277.5280 90.4275 -0.3256 268.9639 269.2895 277.5903 91.1900 -0.3292 268.9999 269.3290 277.6453 92.0435 -0.3334 269.0397 269.3731 277.7102 92.8355 -0.3372 269.0757 269.4129 277.7730 93.6270 -0.3413 269.1125 269.4538 277.8375 94.4493 -0.3455 269.1531 269.4986 277.9049 95.2110 -0.3492 269.1903 269.5394 277.9687 96.0630 -0.3535 269.2328 269.5863 278.0437 96.8253 -0.3570 269.2719 269.6289 278.1124 97.6468 -0.3609 269.3153 269.6762 278.1873 98.4690 -0.3646 269.3576 269.7222 278.2660 99.2305 -0.3685 269.3953 269.7638 278.3421 100.0830 -0.3727 269.4381 269.8108 278.4255 100.8450 -0.3767 269.4800 269.8567 278.5025 101.6663 -0.3811 269.5224 269.9035 278.5909 102.4880 -0.3853 269.5630 269.9482 278.6815 103.2495 -0.3892 269.6007 269.9899 278.7684 104.1018 -0.3937 269.6467 270.0404 278.8710 104.8638 -0.3978 269.6868 270.0846 278.9632 105.6858 -0.4026 269.7289 270.1315 279.0619 106.4778 -0.4071 269.7709 270.1780 279.1608 107.2695 -0.4101 269.8116 270.2217 279.2610 108.1215 -0.4074 269.8572 270.2646 279.3710 108.8838 -0.4058 269.8962 270.3020 279.4702 109.7055 -0.4058 269.9412 270.3470 279.5827 110.4975 -0.4098 269.9821 270.3919 279.6930 111.2895 -0.4164 270.0239 270.4403 279.8045 112.1115 -0.4238 270.0689 270.4927 279.9219 112.9035 -0.4306 270.1126 270.5433 280.0371 113.7255 -0.4371 270.1578 270.5949 280.1578 114.5190 -0.4433 270.2004 270.6438 280.2797 115.3115 -0.4495 270.2454 270.6949 280.3995 116.1335 -0.4555 270.2917 270.7472 280.5272 116.8955 -0.4609 270.3317 270.7927 280.6457 117.7475 -0.4670 270.3847 270.8517 280.7785 118.5395 -0.4725 270.4300 270.9025 280.9041 119.3315 -0.4777 270.4749 270.9526 281.0281 120.1533 -0.4832 270.5227 271.0059 281.1614 120.9155 -0.4883 270.5659 271.0542 281.2877 121.7670 -0.4943 270.6151 271.1094 281.4273 122.5293 -0.4996 270.6599 271.1596 281.5496 123.3508 -0.5055 270.7076 271.2132 281.6850 124.1433 -0.5114 270.7517 271.2630 281.8161 124.9348 -0.5169 270.7951 271.3120 281.9480 125.7873 -0.5230 270.8431 271.3660 282.0912 126.5490 -0.5282 270.8896 271.4178 282.2167 127.3708 -0.5341 270.9425 271.4766 282.3538 128.1630 -0.5399 270.9897 271.5296 282.4840 128.9548 -0.5452 271.0368 271.5820 282.6154 129.7770 -0.5509 271.0878 271.6387 282.7528 130.5385 -0.5561 271.1360 271.6921 282.8825 131.3908 -0.5617 271.1887 271.7503 283.0214 132.1825 -0.5677 271.2367 271.8044 283.1511 132.9745 -0.5740 271.2875 271.8614 283.2807 133.7965 -0.5804 271.3407 271.9211 283.4152 134.5585 -0.5863 271.3907 271.9770 283.5380 135.4098 -0.5927 271.4470 272.0397 283.6756 136.1715 -0.5985 271.4993 272.0978 283.7950 136.9935 -0.6046 271.5571 272.1617 283.9215 137.7855 -0.6104 271.6059 272.2162 284.0453 138.5775 -0.6165 271.6546 272.2711 284.1649 139.4295 -0.6232 271.7109 272.3341 284.2912 140.1915 -0.6293 271.7612 272.3906 284.4002 141.0135 -0.6356 271.8117 272.4473 284.5191 141.8055 -0.6415 271.8646 272.5062 284.6309 142.5975 -0.6474 271.9207 272.5682 284.7411 143.4210 -0.6540 271.9771 272.6311 284.8545 144.1868 -0.6598 272.0269 272.6867 284.9587 145.0435 -0.6663 272.0832 272.7495 285.0725 145.8055 -0.6720 272.1342 272.8061 285.1735 146.6275 -0.6778 272.1877 272.8656 285.2814 147.4195 -0.6840 272.2413 272.9253 285.3844 148.2110 -0.6900 272.2961 272.9861 285.4848 149.0630 -0.6966 272.3563 273.0528 285.5894 149.8250 -0.7026 272.4119 273.1145 285.6832 150.6468 -0.7089 272.4704 273.1793 285.7810 151.4393 -0.7150 272.5256 273.2406 285.8766 152.2315 -0.7208 272.5814 273.3022 285.9698 153.0543 -0.7270 272.6395 273.3665 286.0646 153.8158 -0.7325 272.6923 273.4248 286.1515 154.6678 -0.7385 272.7539 273.4925 286.2477 155.4465 -0.7442 272.8082 273.5524 286.3378 156.2688 -0.7504 272.8670 273.6174 286.4295 157.0605 -0.7565 272.9251 273.6816 286.5162 157.8525 -0.7624 272.9833 273.7457 286.6012 158.6753 -0.7684 273.0448 273.8132 286.6854 159.4375 -0.7745 273.1001 273.8746 286.7649 160.2895 -0.7811 273.1617 273.9429 286.8537 161.0515 -0.7870 273.2166 274.0036 286.9319 161.8735 -0.7930 273.2757 274.0687 287.0139 162.6955 -0.7985 273.3359 274.1344 287.0979 163.4575 -0.8036 273.3928 274.1964 287.1755 164.3095 -0.8092 273.4552 274.2644 287.2606 165.0715 -0.8146 273.5108 274.3254 287.3373 165.8935 -0.8204 273.5723 274.3928 287.4197 166.6855 -0.8258 273.6311 274.4569 287.4993 167.4775 -0.8309 273.6891 274.5199 287.5791 168.3295 -0.8364 273.7540 274.5904 287.6619 169.0915 -0.8416 273.8116 274.6532 287.7357 169.9135 -0.8472 273.8726 274.7198 287.8180 170.7055 -0.8525 273.9319 274.7844 287.8971 171.4975 -0.8580 273.9917 274.8497 287.9762 172.3193 -0.8635 274.0537 274.9173 288.0585 173.0820 -0.8685 274.1107 274.9793 288.1370 173.9353 -0.8745 274.1771 275.0516 288.2268 174.7275 -0.8797 274.2379 275.1176 288.3102 175.5220 -0.8848 274.2978 275.1826 288.3948 176.3203 -0.8900 274.3586 275.2486 288.4797 177.1115 -0.8948 274.4206 275.3154 288.5657 177.9640 -0.9006 274.4861 275.3867 288.6616 178.7263 -0.9057 274.5450 275.4507 288.7472 179.5480 -0.9110 274.6093 275.5203 288.8411 180.3405 -0.9159 274.6727 275.5886 288.9322 181.1338 -0.9207 274.7352 275.6559 289.0268 181.9583 -0.9259 274.8005 275.7264 289.1253 182.7195 -0.9308 274.8599 275.7907 289.2197 183.5718 -0.9367 274.9279 275.8646 289.3241 184.3635 -0.9418 274.9927 275.9345 289.4218 185.1555 -0.9468 275.0552 276.0020 289.5213 185.9775 -0.9518 275.1180 276.0698 289.6260 186.7395 -0.9563 275.1757 276.1320 289.7263 187.5915 -0.9618 275.2429 276.2048 289.8430 188.3535 -0.9668 275.3045 276.2713 289.9458 189.1755 -0.9717 275.3708 276.3425 290.0617 189.9975 -0.9770 275.4364 276.4133 290.1763 190.7595 -0.9819 275.4984 276.4803 290.2823 191.6115 -0.9870 275.5660 276.5530 290.4054 192.3735 -0.9918 275.6290 276.6208 290.5175 193.1955 -0.9970 275.6968 276.6938 290.6371 194.0175 -1.0021 275.7659 276.7681 290.7570 194.7795 -1.0068 275.8305 276.8373 290.8712 195.6315 -1.0122 275.9037 276.9158 290.9980 196.3993 -1.0173 275.9655 276.9828 291.1136 197.2235 -1.0229 276.0331 277.0560 291.2423 198.0155 -1.0280 276.0990 277.1270 291.3639 198.8075 -1.0332 276.1649 277.1982 291.4869 199.6293 -1.0384 276.2344 277.2728 291.6165 200.4213 -1.0437 276.3018 277.3455 291.7401 201.2428 -1.0490 276.3711 277.4201 291.8692 202.0340 -1.0540 276.4369 277.4910 291.9936 202.8258 -1.0594 276.5054 277.5649 292.1207 203.6483 -1.0637 276.5750 277.6387 292.2511 204.4098 -1.0665 276.6392 277.7057 292.3739 205.2620 -1.0722 276.7142 277.7864 292.5118 206.0540 -1.0693 276.7862 277.8555 292.6353 206.8448 -1.0679 276.8556 277.9235 292.7591 207.6668 -1.0537 276.9286 277.9823 292.8880 208.4288 -1.0561 276.9949 278.0510 293.0055 209.2820 -1.0683 277.0680 278.1362 293.1385 210.0435 -1.0782 277.1334 278.2116 293.2557 210.8655 -1.0878 277.2052 278.2930 293.3780 211.6875 -1.0971 277.2779 278.3750 293.5002 212.4495 -1.1052 277.3446 278.4498 293.6108 213.3015 -1.1114 277.4211 278.5325 293.7333 214.0635 -1.1172 277.4916 278.6088 293.8440 214.8855 -1.1227 277.5669 278.6896 293.9636 215.6775 -1.1225 277.6407 278.7632 294.0775 216.4793 -1.1297 277.7118 278.8415 294.1902 217.2795 -1.1368 277.7849 278.9217 294.2998 218.0715 -1.1446 277.8543 278.9989 294.4092 218.9235 -1.1524 277.9329 279.0853 294.5261 219.6855 -1.1596 278.0029 279.1625 294.6309 220.5075 -1.1674 278.0772 279.2446 294.7409 221.2995 -1.1746 278.1489 279.3235 294.8436 222.0915 -1.1816 278.2207 279.4022 294.9433 222.9150 -1.1885 278.2960 279.4845 295.0452 223.6775 -1.1946 278.3668 279.5614 295.1405 224.5295 -1.2013 278.4456 279.6469 295.2429 225.2915 -1.2071 278.5154 279.7225 295.3358 226.1133 -1.2131 278.5910 279.8041 295.4332 226.9353 -1.2191 278.6659 279.8849 295.5274 227.6968 -1.2247 278.7368 279.9615 295.6111 228.5493 -1.2314 278.8180 280.0494 295.7059 229.3113 -1.2367 278.8904 280.1270 295.7867 230.1328 -1.2424 278.9667 280.2090 295.8749 230.9253 -1.2476 279.0401 280.2878 295.9606 231.7168 -1.2532 279.1144 280.3676 296.0426 232.5388 -1.2588 279.1900 280.4489 296.1288 233.3005 -1.2641 279.2624 280.5265 296.2092 234.1528 -1.2690 279.3440 280.6130 296.2999 234.9448 -1.2738 279.4188 280.6926 296.3798 235.7365 -1.2787 279.4961 280.7748 296.4595 236.5588 -1.2837 279.5754 280.8591 296.5437 237.3283 -1.2886 279.6467 280.9353 296.6238 238.1825 -1.2943 279.7261 281.0203 296.7098 238.9445 -1.2994 279.8001 281.0995 296.7865 239.7665 -1.3047 279.8769 281.1816 296.8692 240.5585 -1.3094 279.9521 281.2615 296.9494 241.3505 -1.3137 280.0277 281.3415 297.0315 242.1728 -1.3183 280.1084 281.4267 297.1171 242.9345 -1.3222 280.1793 281.5015 297.1970 243.7865 -1.3270 280.2610 281.5880 297.2868 244.5493 -1.3311 280.3358 281.6669 297.3710 245.3715 -1.3359 280.4148 281.7508 297.4602 246.1935 -1.3407 280.4942 281.8348 297.5487 246.9580 -1.3451 280.5690 281.9140 297.6313 247.7528 -1.3498 280.6447 281.9944 297.7177 248.6055 -1.3548 280.7271 282.0819 297.8141 249.3678 -1.3592 280.8031 282.1623 297.9009 250.1905 -1.3636 280.8842 282.2478 297.9954 251.0163 -1.3681 280.9677 282.3358 298.0904 251.7793 -1.3723 281.0409 282.4132 298.1808 252.6013 -1.3771 281.1217 282.4987 298.2805 253.3933 -1.3815 281.1989 282.5804 298.3800 254.2150 -1.3861 281.2771 282.6632 298.4809 255.0073 -1.3905 281.3558 282.7463 298.5843 255.7990 -1.3946 281.4345 282.8291 298.6853 256.6248 -1.3987 281.5173 282.9161 298.7926 257.4023 -1.4028 281.5940 282.9967 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