DTA measure 1pb3 Date: 202443:133 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1018.99 s Mass = 1410.100 mg data_number = 1264 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.0885 -1.0886 263.0748 264.1634 264.2256 1.8780 -1.0915 263.0701 264.1616 264.2395 2.7283 -1.0901 263.0811 264.1711 264.2393 3.4890 -1.0874 263.0743 264.1617 264.2235 4.3090 -1.0872 263.0632 264.1503 264.2293 5.1295 -1.0873 263.0768 264.1641 264.2189 5.8895 -1.0846 263.0996 264.1843 264.2183 6.7405 -1.0854 263.1118 264.1972 264.2266 7.5008 -1.0849 263.1076 264.1925 264.2317 8.3213 -1.0860 263.1156 264.2016 264.2472 9.1423 -1.0855 263.1070 264.1925 264.2540 9.9028 -1.0878 263.1316 264.2194 264.2672 10.7548 -1.0910 263.1514 264.2424 264.2672 11.5148 -1.0898 263.1414 264.2312 264.2883 12.4723 -1.0873 263.1569 264.2441 264.3184 13.3690 -1.0882 263.1600 264.2482 264.3310 14.1298 -1.0877 263.1515 264.2392 264.3707 14.9518 -1.0864 263.1606 264.2470 264.4145 15.7428 -1.0873 263.1670 264.2543 264.4532 16.5338 -1.0873 263.1908 264.2780 264.5053 17.3548 -1.0839 263.1975 264.2814 264.5273 18.1458 -1.0870 263.1960 264.2830 264.5647 18.9670 -1.0871 263.2090 264.2960 264.6315 19.7575 -1.0873 263.2059 264.2932 264.6995 20.5480 -1.0880 263.2063 264.2943 264.7671 21.3975 -1.0869 263.1994 264.2863 264.8564 22.1580 -1.0897 263.1968 264.2866 264.9316 22.9790 -1.0894 263.2249 264.3143 265.0134 23.7695 -1.0873 263.2360 264.3233 265.1088 24.5600 -1.0926 263.2429 264.3355 265.1734 25.4105 -1.0930 263.2493 264.3423 265.2689 26.1708 -1.0919 263.2554 264.3473 265.3669 26.9920 -1.0945 263.2612 264.3556 265.4804 27.8125 -1.0961 263.2664 264.3625 265.5953 28.5730 -1.0986 263.2835 264.3820 265.7110 29.4235 -1.1027 263.2878 264.3904 265.8437 30.1838 -1.1129 263.3069 264.4197 265.9411 31.0048 -1.1148 263.2992 264.4140 266.0686 31.8240 -1.1190 263.3092 264.4282 266.2102 32.5833 -1.1196 263.3051 264.4246 266.3387 33.4333 -1.1113 263.3164 264.4276 266.4859 34.2235 -1.1079 263.3169 264.4248 266.6245 35.0135 -1.1079 263.3471 264.4549 266.7593 35.8350 -1.1091 263.3418 264.4509 266.9039 36.5958 -1.1130 263.3574 264.4704 267.0622 37.4480 -1.1161 263.3835 264.4996 267.2087 38.2088 -1.1159 263.3792 264.4952 267.3507 39.0303 -1.1194 263.3826 264.5020 267.5099 39.8510 -1.1260 263.4004 264.5264 267.6652 40.6108 -1.1281 263.4138 264.5420 267.8070 41.4628 -1.1271 263.4118 264.5388 267.9792 42.2238 -1.1309 263.4144 264.5453 268.1126 43.1883 -1.1365 263.4448 264.5813 268.2962 44.0575 -1.1380 263.4538 264.5918 268.4829 44.8185 -1.1381 263.4623 264.6005 268.6293 45.6703 -1.1400 263.4764 264.6165 268.8010 46.4615 -1.1434 263.5033 264.6467 268.9672 47.2523 -1.1438 263.5134 264.6572 269.1260 48.0725 -1.1460 263.5238 264.6698 269.2952 48.8328 -1.1492 263.5259 264.6751 269.4541 49.6843 -1.1546 263.5679 264.7224 269.6186 50.4755 -1.1607 263.5685 264.7292 269.7752 51.2663 -1.1625 263.5734 264.7359 269.9263 52.0865 -1.1649 263.5850 264.7499 270.0950 52.8483 -1.1677 263.6003 264.7680 270.2297 53.7053 -1.1724 263.6037 264.7761 270.3964 54.4648 -1.1769 263.6373 264.8142 270.5481 55.2860 -1.1788 263.6538 264.8326 270.6956 56.0775 -1.1810 263.6704 264.8514 270.8467 56.8688 -1.1812 263.6759 264.8571 270.9993 57.7203 -1.1844 263.6962 264.8806 271.1486 58.4800 -1.1868 263.7243 264.9110 271.2962 59.3005 -1.1882 263.7411 264.9293 271.4425 60.0915 -1.1926 263.7697 264.9624 271.5769 60.8818 -1.1961 263.7877 264.9838 271.7555 61.7328 -1.2005 263.8007 265.0011 271.8863 62.4928 -1.2020 263.8185 265.0205 272.0393 63.3143 -1.2067 263.8517 265.0584 272.1834 64.1050 -1.2106 263.8701 265.0807 272.3191 64.8950 -1.2116 263.8709 265.0825 272.4408 65.7460 -1.2161 263.8984 265.1146 272.5683 66.5055 -1.2185 263.9223 265.1409 272.7003 67.3250 -1.2212 263.9396 265.1608 272.8199 68.1458 -1.2259 263.9789 265.2048 272.9628 68.9068 -1.2325 263.9973 265.2299 273.0814 69.7575 -1.2336 264.0055 265.2392 273.2239 70.5178 -1.2349 264.0278 265.2627 273.3330 71.3388 -1.2354 264.0600 265.2953 273.4900 72.1580 -1.2361 264.0693 265.3054 273.5843 72.9178 -1.2406 264.0923 265.3328 273.6992 73.9085 -1.2478 264.1569 265.4046 273.8400 74.7465 -1.2487 264.1757 265.4245 273.9611 75.5380 -1.2502 264.1760 265.4262 274.0796 76.3595 -1.2519 264.2027 265.4546 274.1834 77.1498 -1.2530 264.2439 265.4969 274.3102 77.9710 -1.2560 264.2655 265.5214 274.4316 78.7618 -1.2586 264.2944 265.5530 274.5321 79.5523 -1.2665 264.3270 265.5935 274.6383 80.4033 -1.2722 264.3590 265.6312 274.7523 81.1633 -1.2743 264.3610 265.6354 274.8574 81.9840 -1.2771 264.3885 265.6655 274.9822 82.7755 -1.2793 264.4210 265.7004 275.0686 83.5660 -1.2802 264.4485 265.7288 275.1938 84.4170 -1.2816 264.4858 265.7674 275.3060 85.1775 -1.2830 264.5325 265.8155 275.4166 85.9980 -1.2825 264.5614 265.8438 275.5119 86.7885 -1.2850 264.5674 265.8524 275.6096 87.5785 -1.2868 264.5919 265.8787 275.7265 88.4298 -1.2887 264.6305 265.9193 275.8489 89.1900 -1.2899 264.6691 265.9590 275.9458 90.0113 -1.2942 264.6919 265.9861 276.0690 90.8030 -1.2970 264.7261 266.0231 276.1763 91.5938 -1.2975 264.7619 266.0593 276.2752 92.4155 -1.2999 264.7925 266.0924 276.3879 93.2058 -1.3023 264.8315 266.1338 276.5177 94.0270 -1.3053 264.8771 266.1824 276.6312 94.8178 -1.3129 264.8946 266.2075 276.7430 95.6088 -1.3179 264.9321 266.2499 276.8490 96.4308 -1.3194 264.9726 266.2921 276.9670 97.2215 -1.3245 265.0062 266.3307 277.0901 98.0433 -1.3250 265.0469 266.3719 277.2188 98.8345 -1.3255 265.0701 266.3957 277.3383 99.6265 -1.3279 265.0960 266.4240 277.4522 100.4485 -1.3279 265.1331 266.4610 277.5715 101.2100 -1.3304 265.1691 266.4996 277.6786 102.0615 -1.3361 265.2051 266.5412 277.8021 102.8535 -1.3380 265.2390 266.5770 277.9197 103.6448 -1.3390 265.2938 266.6328 278.0357 104.4665 -1.3429 265.3238 266.6667 278.1608 105.2285 -1.3538 265.3592 266.7131 278.2685 106.0803 -1.3581 265.4010 266.7591 278.3999 106.8418 -1.3656 265.4365 266.8021 278.4833 107.6638 -1.3641 265.4610 266.8251 278.6345 108.4845 -1.3655 265.5012 266.8668 278.7559 109.2458 -1.3707 265.5510 266.9217 278.8915 110.0975 -1.3737 265.5926 266.9663 279.0407 110.8585 -1.3723 265.6337 267.0059 279.1521 111.6785 -1.3789 265.6635 267.0424 279.2689 112.4700 -1.3838 265.6923 267.0762 279.4081 113.2608 -1.3786 265.7336 267.1122 279.5138 114.1130 -1.3746 265.7862 267.1608 279.6619 114.8730 -1.3791 265.8200 267.1991 279.7944 115.6938 -1.3772 265.8499 267.2270 279.9306 116.4850 -1.3783 265.8975 267.2758 280.0613 117.2765 -1.3823 265.9351 267.3174 280.2087 118.1290 -1.3851 265.9992 267.3843 280.3257 118.8898 -1.3887 266.0595 267.4482 280.4676 119.7118 -1.3956 266.0939 267.4895 280.5976 120.5030 -1.4040 266.1306 267.5347 280.7376 121.3833 -1.4084 266.1710 267.5794 280.8761 122.1430 -1.4051 266.2363 267.6415 281.0140 122.9933 -1.4044 266.2803 267.6847 281.1472 123.7535 -1.4020 266.3162 267.7182 281.2871 124.5755 -1.4051 266.3658 267.7709 281.4294 125.3970 -1.4070 266.4010 267.8080 281.5447 126.1570 -1.4087 266.4476 267.8563 281.6716 127.0085 -1.4093 266.4946 267.9039 281.8029 127.7698 -1.4116 266.5598 267.9714 281.9309 128.5908 -1.4147 266.5861 268.0008 282.0652 129.4115 -1.4169 266.6185 268.0355 282.2045 130.1733 -1.4201 266.6541 268.0742 282.3348 131.0243 -1.4228 266.7157 268.1385 282.4797 131.8135 -1.4239 266.7696 268.1935 282.6203 132.6038 -1.4254 266.8372 268.2626 282.7675 133.4240 -1.4268 266.8868 268.3136 282.8891 134.1850 -1.4296 266.9364 268.3659 282.9983 135.1220 -1.4319 266.9730 268.4048 283.1532 136.0303 -1.4342 267.0541 268.4884 283.3092 136.8198 -1.4379 267.1179 268.5558 283.4278 137.6403 -1.4410 267.1671 268.6081 283.5607 138.4323 -1.4433 267.2122 268.6555 283.6773 139.2225 -1.4465 267.2454 268.6920 283.8084 140.0440 -1.4489 267.3021 268.7510 283.9542 140.8335 -1.4508 267.3473 268.7980 284.0870 141.6540 -1.4493 267.4104 268.8597 284.2184 142.4440 -1.4522 267.4617 268.9139 284.3458 143.2348 -1.4558 267.4991 268.9549 284.4615 144.0578 -1.4589 267.5681 269.0269 284.6048 144.8493 -1.4602 267.6210 269.0812 284.7105 145.8435 -1.4637 267.6929 269.1566 284.8666 146.6655 -1.4687 267.7407 269.2094 285.0064 147.4565 -1.4722 267.8084 269.2806 285.1358 148.2483 -1.4765 267.8667 269.3432 285.2526 149.0698 -1.4776 267.9156 269.3932 285.4034 149.8598 -1.4782 267.9526 269.4308 285.5217 150.6813 -1.4856 268.0074 269.4930 285.6420 151.4705 -1.4823 268.0788 269.5611 285.7677 152.2603 -1.4788 268.1551 269.6339 285.8899 153.0815 -1.4835 268.1998 269.6833 286.0037 153.8735 -1.4891 268.2437 269.7327 286.1400 154.6955 -1.4887 268.3068 269.7955 286.2688 155.4858 -1.4876 268.3749 269.8626 286.3836 156.2763 -1.4865 268.4336 269.9201 286.4875 157.0975 -1.4894 268.4968 269.9861 286.6107 157.8873 -1.4929 268.5428 270.0357 286.7418 158.7080 -1.4964 268.5974 270.0937 286.8752 159.4985 -1.5038 268.6635 270.1672 286.9868 160.2903 -1.5092 268.7315 270.2407 287.0937 161.1115 -1.5122 268.8027 270.3149 287.2303 161.8725 -1.5093 268.8565 270.3658 287.3255 162.7230 -1.5075 268.9173 270.4248 287.4668 163.5133 -1.5087 268.9653 270.4740 287.5934 164.3035 -1.5113 269.0172 270.5285 287.7026 165.1253 -1.5124 269.0857 270.5981 287.8474 165.8840 -1.5123 269.1535 270.6658 287.9597 166.7348 -1.5167 269.2162 270.7329 288.0773 167.5243 -1.5193 269.2602 270.7794 288.2034 168.3143 -1.5218 269.3416 270.8633 288.3277 169.1360 -1.5268 269.4186 270.9453 288.4384 169.8965 -1.5373 269.4742 271.0115 288.5636 170.7488 -1.5310 269.5390 271.0700 288.7102 171.5390 -1.5385 269.6041 271.1426 288.8315 172.3293 -1.5510 269.6601 271.2111 288.9626 173.1498 -1.5520 269.7185 271.2705 289.0833 173.9098 -1.5439 269.7939 271.3378 289.2007 174.7613 -1.5467 269.8609 271.4076 289.3441 175.5218 -1.5500 269.9223 271.4722 289.4650 176.3740 -1.5530 269.9782 271.5312 289.5941 177.1348 -1.5600 270.0349 271.5950 289.7199 177.9558 -1.5608 270.1156 271.6764 289.8498 178.7465 -1.5631 270.1760 271.7391 289.9709 179.5373 -1.5667 270.2514 271.8181 290.0815 180.3883 -1.5624 270.3331 271.8954 290.2480 181.1480 -1.5603 270.3955 271.9558 290.3535 181.9690 -1.5640 270.4245 271.9885 290.4807 182.7595 -1.5636 270.5240 272.0875 290.6032 183.5513 -1.5613 270.5975 272.1588 290.7326 184.4018 -1.5645 270.6600 272.2245 290.8505 185.1625 -1.5674 270.7297 272.2971 290.9747 185.9845 -1.5677 270.8135 272.3812 291.1162 186.7748 -1.5651 270.8638 272.4289 291.2367 187.5665 -1.5697 270.9412 272.5109 291.3645 188.3883 -1.5763 271.0099 272.5862 291.5028 189.1783 -1.5881 271.0733 272.6613 291.6199 189.9980 -1.5925 271.1457 272.7382 291.7481 190.7888 -1.5914 271.2206 272.8120 291.8640 191.5780 -1.5866 271.2797 272.8663 291.9916 192.4290 -1.5879 271.3551 272.9431 292.1176 193.1898 -1.5905 271.4275 273.0181 292.2515 194.0113 -1.5913 271.5044 273.0957 292.3794 194.8028 -1.5936 271.5854 273.1790 292.5062 195.5920 -1.5948 271.6631 273.2579 292.6244 196.5433 -1.5961 271.7383 273.3344 292.7749 197.4063 -1.5989 271.8015 273.4004 292.9269 198.2270 -1.6015 271.8831 273.4846 293.0567 199.0165 -1.6029 271.9590 273.5618 293.2032 199.8070 -1.6056 272.0224 273.6280 293.3443 200.6573 -1.6101 272.1000 273.7102 293.4803 201.4175 -1.6126 272.1657 273.7783 293.6272 202.2390 -1.6127 272.2469 273.8596 293.7736 203.0305 -1.6141 272.3383 273.9523 293.8889 203.8218 -1.6187 272.4094 274.0280 294.0279 204.6733 -1.6228 272.4898 274.1126 294.1767 205.4345 -1.6243 272.5538 274.1780 294.3169 206.2560 -1.6257 272.6372 274.2629 294.4729 207.0465 -1.6283 272.7068 274.3351 294.6046 207.8370 -1.6316 272.7744 274.4060 294.7527 208.6873 -1.6364 272.8663 274.5027 294.9053 209.4468 -1.6382 272.9360 274.5742 295.0341 210.2680 -1.6382 273.0119 274.6501 295.1778 211.0885 -1.6388 273.1070 274.7458 295.3313 211.8483 -1.6428 273.1690 274.8118 295.4643 212.6990 -1.6462 273.2706 274.9169 295.6033 213.4898 -1.6481 273.3434 274.9915 295.7438 214.2803 -1.6468 273.4073 275.0542 295.8812 215.1013 -1.6505 273.5020 275.1525 296.0299 215.8618 -1.6542 273.5844 275.2386 296.1879 216.7128 -1.6549 273.6546 275.3094 296.3256 217.4738 -1.6584 273.7384 275.3968 296.4663 218.2950 -1.6628 273.8145 275.4773 296.5876 219.1150 -1.6662 273.8876 275.5538 296.7312 219.8765 -1.6668 273.9558 275.6226 296.8670 220.7280 -1.6687 274.0635 275.7322 297.0180 221.5168 -1.6723 274.1406 275.8128 297.1462 222.3075 -1.6734 274.2105 275.8839 297.2535 223.1300 -1.6735 274.2968 275.9703 297.3810 223.8915 -1.6768 274.3721 276.0489 297.5116 224.7433 -1.6838 274.4538 276.1377 297.6408 225.5045 -1.6869 274.5322 276.2190 297.7641 226.3248 -1.6954 274.6266 276.3220 297.8969 227.2393 -1.6946 274.7326 276.4271 298.0417 228.1248 -1.6917 274.8168 276.5085 298.1585 228.9453 -1.6934 274.9083 276.6017 298.2886 229.7365 -1.6941 274.9810 276.6751 298.4009 230.5278 -1.6972 275.0672 276.7644 298.5029 231.3495 -1.7014 275.1439 276.8453 298.6323 232.1403 -1.7032 275.2322 276.9354 298.7442 232.9613 -1.7038 275.3129 277.0166 298.8632 233.7525 -1.7081 275.4079 277.1160 298.9844 234.5435 -1.7112 275.4798 277.1910 299.0901 235.3943 -1.7110 275.5847 277.2957 299.2245 236.1545 -1.7131 275.6575 277.3706 299.3295 236.9758 -1.7152 275.7391 277.4543 299.4425 237.7660 -1.7184 275.8278 277.5462 299.5472 238.5570 -1.7216 275.9095 277.6312 299.6674 239.4085 -1.7217 276.0072 277.7288 299.7952 240.1695 -1.7268 276.1010 277.8278 299.9113 240.9900 -1.7284 276.2034 277.9318 300.0278 241.7798 -1.7331 276.2668 277.9999 300.1483 242.5698 -1.7420 276.3541 278.0961 300.2731 243.4218 -1.7431 276.4441 278.1872 300.4086 244.1828 -1.7378 276.5357 278.2736 300.5030 245.0043 -1.7378 276.6288 278.3666 300.6279 245.7960 -1.7422 276.6972 278.4394 300.7552 246.6770 -1.7567 276.7902 278.5469 300.8752 247.4673 -1.7585 276.8848 278.6432 301.0066 248.2883 -1.7603 276.9665 278.7268 301.1466 249.0785 -1.7648 277.0709 278.8357 301.2509 249.8690 -1.7659 277.1590 278.9248 301.3720 250.6898 -1.7694 277.2436 279.0131 301.5119 251.4498 -1.7719 277.3474 279.1193 301.6191 252.3005 -1.7734 277.4287 279.2021 301.7596 253.0895 -1.7748 277.5076 279.2824 301.8643 253.8795 -1.7717 277.6142 279.3859 302.0093 254.7005 -1.7668 277.7059 279.4726 302.1421 255.4903 -1.7670 277.7902 279.5572 302.2531 256.3108 -1.7682 277.8769 279.6451 302.3881 257.1015 -1.7729 277.9571 279.7300 302.5148 257.9278 -1.7762 278.0436 279.8199 302.6380 258.6935 -1.7794 278.1500 279.9294 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