DTA measure 2pb3 Date: 202443:1330 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1497.34 s Mass = 1410.100 mg data_number = 1862 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2050 -4.3956 417.6004 421.9960 420.8082 2.0578 -4.4003 417.6298 422.0301 420.8465 2.8205 -4.3992 417.6684 422.0676 420.8600 3.6415 -4.4048 417.7303 422.1351 420.8462 4.4325 -4.3973 417.7400 422.1373 420.8587 5.2245 -4.3934 417.7716 422.1650 420.8663 6.0483 -4.3929 417.8038 422.1967 420.8503 6.8105 -4.3924 417.8346 422.2270 420.8197 7.6625 -4.3923 417.8863 422.2786 420.7769 8.4535 -4.3895 417.8969 422.2864 420.7624 9.2443 -4.3883 417.9126 422.3009 420.7458 10.0655 -4.3871 417.9579 422.3449 420.7148 10.8258 -4.3834 417.9951 422.3786 420.6644 11.6773 -4.3816 418.0148 422.3963 420.6142 12.4685 -4.3789 418.0377 422.4167 420.5744 13.2600 -4.3786 418.0652 422.4438 420.5213 14.0815 -4.3759 418.1206 422.4965 420.4685 14.8423 -4.3787 418.1510 422.5297 420.3873 15.6935 -4.3850 418.1710 422.5560 420.3092 16.4855 -4.3857 418.1843 422.5700 420.2305 17.2765 -4.3856 418.2117 422.5973 420.1732 18.0973 -4.3832 418.2438 422.6270 420.0988 18.8640 -4.3810 418.2571 422.6381 420.0264 19.7040 -4.3806 418.2715 422.6521 419.9258 20.4658 -4.3824 418.3065 422.6890 419.8267 21.3180 -4.3866 418.3371 422.7238 419.7214 22.0798 -4.3846 418.3580 422.7426 419.6204 22.9013 -4.3755 418.3843 422.7598 419.5366 23.7230 -4.3707 418.4051 422.7759 419.4334 24.4840 -4.3651 418.4116 422.7767 419.3372 25.3353 -4.3530 418.4486 422.8016 419.2131 26.0968 -4.3465 418.4670 422.8136 419.1098 26.9185 -4.3418 418.5026 422.8444 418.9850 27.7398 -4.3408 418.5321 422.8729 418.8653 28.4990 -4.3366 418.5365 422.8731 418.7607 29.3528 -4.3318 418.5405 422.8724 418.6329 30.1128 -4.3297 418.5677 422.8974 418.4988 30.9335 -4.3256 418.6013 422.9269 418.3852 31.7255 -4.3228 418.6298 422.9527 418.2713 32.5175 -4.3211 418.6449 422.9660 418.1588 33.3695 -4.3187 418.6520 422.9707 418.0268 34.1318 -4.3127 418.6702 422.9830 417.9113 34.9530 -4.3066 418.6929 422.9995 417.7871 35.7445 -4.3016 418.6962 422.9978 417.6436 36.5358 -4.3027 418.7176 423.0203 417.5492 37.3873 -4.2961 418.7215 423.0176 417.4215 38.1510 -4.2914 418.7363 423.0277 417.2971 38.9753 -4.2855 418.7615 423.0470 417.1765 39.7515 -4.2818 418.7948 423.0766 417.0676 40.5780 -4.2792 418.7940 423.0732 416.9251 41.3695 -4.2792 418.7842 423.0634 416.8076 42.1608 -4.2759 418.7872 423.0631 416.6850 42.9825 -4.2734 418.8054 423.0788 416.5652 43.7733 -4.2694 418.8000 423.0694 416.4328 44.5940 -4.2640 418.8024 423.0664 416.3161 45.3850 -4.2612 418.8337 423.0950 416.1951 46.1743 -4.2541 418.8344 423.0885 416.0818 46.9960 -4.2511 418.8372 423.0882 415.9533 47.7575 -4.2473 418.8709 423.1181 415.8398 48.6098 -4.2454 418.8661 423.1115 415.7034 49.4000 -4.2374 418.8633 423.1007 415.5985 50.1905 -4.2290 418.8715 423.1005 415.4822 51.0120 -4.2239 418.8783 423.1021 415.3606 51.7728 -4.2184 418.8992 423.1175 415.2545 52.6250 -4.2124 418.9044 423.1168 415.1457 53.4160 -4.2050 418.8981 423.1031 415.0521 54.2070 -4.2003 418.8847 423.0849 414.9490 55.0285 -4.1946 418.8903 423.0849 414.8502 55.7895 -4.1916 418.8883 423.0799 414.7387 56.6413 -4.1881 418.8758 423.0638 414.6525 57.4025 -4.1860 418.8922 423.0782 414.5452 58.2238 -4.1811 418.8891 423.0703 414.4509 59.0445 -4.1784 418.8748 423.0532 414.3419 59.8145 -4.1745 418.8784 423.0529 414.2501 60.6318 -4.1698 418.8951 423.0650 414.1512 61.4228 -4.1650 418.8951 423.0601 414.0560 62.2445 -4.1596 418.8997 423.0593 413.9742 63.0043 -4.1536 418.8777 423.0313 413.8846 63.8553 -4.1494 418.8623 423.0118 413.7998 64.6455 -4.1483 418.8571 423.0054 413.6970 65.4368 -4.1449 418.8507 422.9956 413.5962 66.2575 -4.1421 418.8507 422.9928 413.5024 67.0188 -4.1387 418.8480 422.9867 413.4186 67.8703 -4.1316 418.8452 422.9767 413.3326 68.6608 -4.1267 418.8297 422.9564 413.2613 69.4508 -4.1232 418.8267 422.9500 413.1578 70.2720 -4.1180 418.8125 422.9305 413.0819 71.0320 -4.1165 418.7983 422.9148 412.9984 71.8838 -4.1101 418.7771 422.8872 412.9096 72.6450 -4.1080 418.7931 422.9011 412.8306 73.4668 -4.1042 418.7780 422.8823 412.7264 74.2880 -4.0974 418.7675 422.8649 412.6329 75.0480 -4.0953 418.7519 422.8472 412.5589 75.9000 -4.0899 418.7658 422.8557 412.4442 76.6618 -4.0878 418.7201 422.8079 412.3668 77.4835 -4.0858 418.7242 422.8100 412.2806 78.3050 -4.0810 418.7062 422.7872 412.1910 79.0665 -4.0784 418.6933 422.7717 412.0981 79.9185 -4.0747 418.6726 422.7473 412.0060 80.6773 -4.0697 418.6570 422.7267 411.9178 81.5065 -4.0631 418.6566 422.7197 411.8125 82.2675 -4.0609 418.6322 422.6931 411.7449 83.1193 -4.0577 418.6179 422.6756 411.6651 83.9105 -4.0540 418.6022 422.6562 411.5624 84.7013 -4.0494 418.6148 422.6643 411.4726 85.5220 -4.0450 418.5747 422.6197 411.3726 86.3128 -4.0414 418.5433 422.5847 411.2802 87.1345 -4.0423 418.5320 422.5743 411.1880 87.9265 -4.0379 418.5169 422.5548 411.1081 88.7178 -4.0353 418.4986 422.5339 411.0158 89.5395 -4.0300 418.4699 422.4999 410.9159 90.3290 -4.0243 418.4617 422.4860 410.8234 91.1495 -4.0223 418.4334 422.4557 410.7115 91.9405 -4.0194 418.4051 422.4245 410.6252 92.7320 -4.0151 418.3773 422.3924 410.5378 93.5535 -4.0110 418.3668 422.3778 410.4342 94.3455 -4.0057 418.3570 422.3626 410.3330 95.1660 -4.0054 418.3283 422.3337 410.2370 95.9565 -4.0005 418.3044 422.3049 410.1565 96.7475 -3.9948 418.3000 422.2948 410.0560 97.5700 -3.9911 418.2793 422.2705 409.9447 98.3315 -3.9882 418.2505 422.2387 409.8510 99.1838 -3.9857 418.2187 422.2044 409.7372 99.9750 -3.9821 418.1733 422.1554 409.6590 100.7753 -3.9784 418.1737 422.1521 409.5565 101.5600 -3.9756 418.1300 422.1056 409.4634 102.3815 -3.9721 418.1069 422.0790 409.3554 103.2030 -3.9661 418.0929 422.0590 409.2549 103.9635 -3.9634 418.0616 422.0250 409.1771 104.8160 -3.9569 418.0425 421.9994 409.0599 105.5775 -3.9547 418.0171 421.9718 408.9696 106.3995 -3.9508 417.9832 421.9340 408.8506 107.1915 -3.9474 417.9493 421.8966 408.7432 107.9833 -3.9434 417.9306 421.8740 408.6809 108.8353 -3.9400 417.8856 421.8256 408.5692 109.5965 -3.9379 417.8667 421.8046 408.4598 110.4183 -3.9341 417.8426 421.7767 408.3706 111.1850 -3.9298 417.7968 421.7266 408.2722 112.0125 -3.9273 417.7680 421.6953 408.1661 112.8033 -3.9226 417.7296 421.6523 408.0694 113.6245 -3.9174 417.7098 421.6271 407.9781 114.4148 -3.9157 417.6770 421.5927 407.8904 115.2358 -3.9084 417.6574 421.5658 407.7941 116.0255 -3.9071 417.6154 421.5224 407.6877 116.8160 -3.9066 417.5864 421.4930 407.5944 117.6663 -3.8999 417.5519 421.4519 407.4738 118.4268 -3.8967 417.5224 421.4191 407.3813 119.2480 -3.8938 417.4827 421.3765 407.2939 120.0395 -3.8891 417.4343 421.3233 407.1948 120.8305 -3.8855 417.4065 421.2919 407.1028 121.6820 -3.8822 417.3771 421.2592 406.9775 122.4430 -3.8814 417.3243 421.2057 406.8872 123.2643 -3.8738 417.2987 421.1725 406.7844 124.0563 -3.8718 417.2691 421.1409 406.6692 124.8475 -3.8693 417.2192 421.0885 406.5863 125.6720 -3.8629 417.1850 421.0479 406.4690 126.4328 -3.8584 417.1642 421.0225 406.3645 127.2848 -3.8574 417.1226 420.9800 406.2592 128.0760 -3.8544 417.0882 420.9426 406.1654 128.8665 -3.8508 417.0257 420.8765 406.0654 129.6880 -3.8485 417.0047 420.8533 405.9623 130.4478 -3.8446 416.9758 420.8204 405.8666 131.3025 -3.8405 416.9504 420.7909 405.7843 132.0660 -3.8377 416.9193 420.7570 405.6592 132.9183 -3.8312 416.8601 420.6914 405.5384 133.6785 -3.8280 416.8164 420.6444 405.4409 134.5005 -3.8293 416.7777 420.6070 405.3372 135.2915 -3.8237 416.7269 420.5506 405.2400 136.0835 -3.8186 416.6700 420.4886 405.1343 136.9055 -3.8174 416.6573 420.4746 405.0278 137.6965 -3.8133 416.6085 420.4218 404.9351 138.5178 -3.8097 416.5579 420.3677 404.8302 139.3085 -3.8075 416.5150 420.3224 404.7395 140.0998 -3.8018 416.4725 420.2743 404.6450 140.9215 -3.7973 416.4167 420.2140 404.5296 141.7013 -3.7941 416.3804 420.1745 404.4405 142.4890 -3.7907 416.3419 420.1326 404.3417 143.3405 -3.7884 416.3011 420.0895 404.2471 144.1315 -3.7861 416.2691 420.0552 404.1457 144.9233 -3.7828 416.2165 419.9993 404.0364 145.7443 -3.7781 416.1590 419.9370 403.9343 146.5043 -3.7740 416.1086 419.8826 403.8550 147.3560 -3.7698 416.0719 419.8417 403.7485 148.1473 -3.7658 416.0343 419.8001 403.6572 148.9378 -3.7619 415.9751 419.7370 403.5501 149.7590 -3.7596 415.9292 419.6888 403.4534 150.5193 -3.7581 415.8847 419.6428 403.3563 151.3708 -3.7558 415.8327 419.5885 403.2394 152.1435 -3.7523 415.7929 419.5452 403.1612 152.9460 -3.7479 415.7260 419.4739 403.0793 153.7678 -3.7447 415.6883 419.4329 402.9687 154.5600 -3.7412 415.6504 419.3916 402.8741 155.3503 -3.7369 415.6004 419.3373 402.7857 156.2013 -3.7306 415.5509 419.2815 402.7036 156.9608 -3.7271 415.5083 419.2354 402.5968 157.7823 -3.7254 415.4569 419.1824 402.4942 158.5735 -3.7219 415.3975 419.1195 402.4112 159.3650 -3.7189 415.3494 419.0683 402.3192 160.2163 -3.7147 415.2934 419.0080 402.2123 160.9768 -3.7108 415.2438 418.9546 402.1017 161.7983 -3.7095 415.2038 418.9132 401.9929 162.5833 -3.7074 415.1444 418.8518 401.9165 163.3935 -3.7044 415.0680 418.7724 401.8053 164.1855 -3.7000 415.0443 418.7443 401.6983 165.0373 -3.6959 414.9841 418.6800 401.5961 165.7985 -3.6921 414.9347 418.6269 401.5079 166.6198 -3.6910 414.8752 418.5662 401.4049 167.4405 -3.6886 414.8262 418.5148 401.3065 168.2010 -3.6854 414.7633 418.4487 401.2115 169.0513 -3.6801 414.7111 418.3912 401.0902 169.8115 -3.6772 414.6727 418.3500 401.0015 170.6330 -3.6716 414.6110 418.2827 400.8963 171.4543 -3.6678 414.5513 418.2192 400.7922 172.2135 -3.6642 414.5066 418.1708 400.7057 173.0248 -3.6618 414.4462 418.1080 400.6207 173.8758 -3.6569 414.3950 418.0519 400.5169 174.6350 -3.6539 414.3513 418.0051 400.4156 175.4565 -3.6502 414.2869 417.9372 400.3020 176.2470 -3.6452 414.2149 417.8601 400.2141 177.0378 -3.6399 414.1575 417.7975 400.1201 177.8898 -3.6401 414.1159 417.7560 400.0065 178.6508 -3.6373 414.0606 417.6980 399.9101 179.4725 -3.6362 414.0041 417.6403 399.8012 180.2640 -3.6307 413.9388 417.5695 399.7134 181.0550 -3.6323 413.8832 417.5156 399.6188 181.8768 -3.6397 413.8076 417.4473 399.5137 182.6575 -3.6377 413.7558 417.3935 399.4276 183.4468 -3.6313 413.7071 417.3384 399.3305 184.2985 -3.6268 413.6343 417.2610 399.2140 185.0605 -3.6158 413.5746 417.1904 399.1269 185.8825 -3.6119 413.5164 417.1284 399.0234 186.7045 -3.6114 413.4740 417.0854 398.9320 187.4655 -3.6100 413.4209 417.0308 398.8465 188.3175 -3.6066 413.3613 416.9679 398.7565 189.0785 -3.6060 413.2902 416.8962 398.6463 189.9003 -3.6022 413.2212 416.8234 398.5652 190.6915 -3.5966 413.1657 416.7624 398.4535 191.4830 -3.5957 413.1203 416.7160 398.3461 192.3345 -3.5907 413.0278 416.6185 398.2369 193.1010 -3.5871 412.9718 416.5589 398.1507 193.8995 -3.5839 412.9220 416.5059 398.0646 194.7213 -3.5798 412.8653 416.4451 397.9576 195.5115 -3.5793 412.8035 416.3827 397.8648 196.3023 -3.5779 412.7322 416.3101 397.7566 197.1233 -3.5749 412.6708 416.2457 397.6607 197.9143 -3.5701 412.6213 416.1914 397.5743 198.7355 -3.5663 412.5620 416.1283 397.4603 199.5260 -3.5626 412.5064 416.0689 397.3473 200.3163 -3.5584 412.4377 415.9961 397.2616 201.1370 -3.5552 412.3688 415.9240 397.1604 201.8985 -3.5535 412.3121 415.8656 397.0565 202.7508 -3.5497 412.2241 415.7738 396.9462 203.5405 -3.5449 412.1603 415.7052 396.8306 204.3228 -3.5449 412.1009 415.6458 396.7443 205.1445 -3.5430 412.0440 415.5870 396.6478 205.9358 -3.5395 411.9816 415.5211 396.5444 206.7270 -3.5364 411.9145 415.4509 396.4255 207.5785 -3.5314 411.8432 415.3745 396.3184 208.3388 -3.5286 411.7884 415.3170 396.2040 209.1595 -3.5256 411.7212 415.2468 396.1181 209.9500 -3.5226 411.6498 415.1725 396.0122 210.7403 -3.5192 411.5772 415.0964 395.9153 211.5913 -3.5166 411.5023 415.0188 395.8132 212.3508 -3.5137 411.4602 414.9739 395.7247 213.1723 -3.5123 411.3880 414.9003 395.6007 213.9838 -3.5099 411.3020 414.8118 395.4952 214.7745 -3.5048 411.2322 414.7370 395.3961 215.5653 -3.4986 411.1880 414.6866 395.3177 216.3865 -3.5008 411.1336 414.6344 395.1873 217.1475 -3.5080 411.0494 414.5574 395.0849 217.9993 -3.5079 410.9774 414.4853 394.9919 218.7895 -3.4969 410.9131 414.4100 394.8913 219.5810 -3.4913 410.8575 414.3488 394.8000 220.4025 -3.4882 410.7797 414.2679 394.6917 221.1628 -3.4852 410.7156 414.2007 394.6030 222.0143 -3.4794 410.6440 414.1234 394.4948 222.8055 -3.4777 410.5742 414.0518 394.3751 223.6158 -3.4778 410.4976 413.9754 394.2884 224.4060 -3.4764 410.4364 413.9128 394.1986 225.2280 -3.4709 410.3575 413.8284 394.1046 225.9875 -3.4658 410.2947 413.7606 394.0155 226.8388 -3.4635 410.2221 413.6856 393.9225 227.6000 -3.4617 410.1637 413.6254 393.8192 228.4215 -3.4579 410.0900 413.5479 393.7064 229.2430 -3.4572 410.0061 413.4632 393.6068 230.0040 -3.4550 409.9297 413.3847 393.5234 230.8558 -3.4525 409.8670 413.3195 393.4182 231.6460 -3.4514 409.7996 413.2510 393.3186 232.4368 -3.4493 409.7340 413.1833 393.2147 233.2590 -3.4440 409.6567 413.1007 393.1289 234.0578 -3.4414 409.5826 413.0240 393.0333 234.8285 -3.4406 409.5148 412.9554 392.9393 235.6803 -3.4325 409.4466 412.8791 392.8198 236.4415 -3.4306 409.3776 412.8083 392.7522 237.2630 -3.4306 409.2907 412.7213 392.6423 238.0545 -3.4282 409.2108 412.6391 392.5608 238.8453 -3.4250 409.1532 412.5782 392.4525 239.6965 -3.4217 409.0882 412.5099 392.3397 240.4578 -3.4183 409.0169 412.4352 392.2559 241.2795 -3.4240 408.9305 412.3545 392.1306 242.0715 -3.4194 408.8466 412.2660 392.0392 242.8628 -3.4137 408.7648 412.1785 391.9473 243.7145 -3.4102 408.7009 412.1111 391.8313 244.5010 -3.4021 408.6120 412.0141 391.7182 245.2795 -3.3941 408.5433 411.9374 391.6101 246.1015 -3.3908 408.4849 411.8757 391.5217 246.8935 -3.3879 408.4211 411.8090 391.4211 247.6840 -3.3824 408.3405 411.7229 391.3125 248.5348 -3.3798 408.2568 411.6366 391.2077 249.2963 -3.3789 408.1955 411.5744 391.1217 250.1170 -3.3754 408.1145 411.4899 391.0024 250.9070 -3.3711 408.0448 411.4159 390.9026 251.6973 -3.3701 407.9637 411.3338 390.7836 252.5490 -3.3641 407.8923 411.2564 390.6845 253.3108 -3.3605 407.8105 411.1710 390.5827 254.1318 -3.3565 407.7338 411.0903 390.4541 254.9420 -3.3519 407.6507 411.0026 390.3682 255.7330 -3.3513 407.5829 410.9342 390.2666 256.5243 -3.3475 407.5161 410.8636 390.1632 257.3450 -3.3459 407.4423 410.7882 390.0576 258.1058 -3.3442 407.3651 410.7093 389.9585 258.9575 -3.3409 407.2899 410.6309 389.8418 259.7465 -3.3371 407.2253 410.5625 389.7273 260.5370 -3.3350 407.1310 410.4660 389.6272 261.3585 -3.3327 407.0515 410.3842 389.5250 262.1198 -3.3334 406.9669 410.3003 389.4379 262.9713 -3.3324 406.9025 410.2348 389.3176 263.7615 -3.3283 406.8215 410.1498 389.2156 264.5728 -3.3236 406.7370 410.0606 389.0983 265.3640 -3.3199 406.6642 409.9841 389.0009 266.1555 -3.3176 406.5905 409.9081 388.8953 266.9463 -3.3182 406.5005 409.8187 388.8072 267.7975 -3.3143 406.4442 409.7585 388.6895 268.5593 -3.3110 406.3560 409.6670 388.5992 269.3798 -3.3138 406.2710 409.5848 388.5099 270.2005 -3.3186 406.2000 409.5187 388.3937 270.9608 -3.3132 406.1127 409.4260 388.3055 271.8123 -3.3068 406.0391 409.3459 388.1960 272.5725 -3.3022 405.9669 409.2692 388.1010 273.3943 -3.2991 405.8712 409.1703 387.9942 274.1865 -3.2899 405.8065 409.0964 387.8958 275.0163 -3.2849 405.7237 409.0086 387.7833 275.7848 -3.2822 405.6347 408.9170 387.6918 276.6070 -3.2810 405.5501 408.8311 387.6048 277.3970 -3.2775 405.4915 408.7690 387.4798 278.2183 -3.2733 405.4171 408.6904 387.3781 279.0100 -3.2731 405.3340 408.6071 387.2937 279.8005 -3.2748 405.2673 408.5421 387.1922 280.6215 -3.2741 405.1820 408.4561 387.0855 281.3815 -3.2731 405.0962 408.3693 386.9965 282.2335 -3.2705 405.0052 408.2757 386.8948 282.9948 -3.2674 404.9344 408.2018 386.8280 283.8173 -3.2643 404.8465 408.1108 386.7128 284.6388 -3.2629 404.7566 408.0194 386.5964 285.5508 -3.2605 404.6686 407.9291 386.4929 286.4533 -3.2604 404.5843 407.8447 386.3775 287.2143 -3.2568 404.5221 407.7788 386.2947 288.0350 -3.2534 404.4379 407.6913 386.1949 288.8265 -3.2528 404.3633 407.6161 386.0961 289.6180 -3.2503 404.2951 407.5454 385.9964 290.4695 -3.2458 404.2004 407.4462 385.8978 291.2315 -3.2388 404.1169 407.3556 385.8161 292.0533 -3.2335 404.0235 407.2570 385.7077 292.8445 -3.2292 403.9354 407.1646 385.5977 293.6353 -3.2264 403.8536 407.0800 385.5074 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