DTA measure 2olom_2 Test Date: 2024228:1415 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1274.66 s Mass = 1138.5000 mg data_number = 1586 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2375 -1.3157 262.6764 263.9921 266.7324 2.0598 -1.3139 262.7665 264.0804 266.7844 2.8215 -1.3145 262.8547 264.1691 266.6630 3.6750 -1.3047 262.9183 264.2230 266.6738 4.4668 -1.2902 262.9965 264.2867 266.6205 5.2585 -1.2845 263.0110 264.2956 266.6774 6.0908 -1.2754 263.0325 264.3079 266.7282 6.8525 -1.2602 263.1138 264.3741 266.7413 7.7048 -1.2622 263.2753 264.5376 266.9083 8.4968 -1.2592 263.3261 264.5853 266.9044 9.2885 -1.2436 263.3189 264.5625 266.9604 10.1115 -1.2503 263.4993 264.7496 267.1674 10.8735 -1.2419 263.5719 264.8138 267.1648 11.7258 -1.2338 263.6561 264.8899 267.1301 12.4878 -1.2290 263.7107 264.9396 267.2422 13.3105 -1.2351 263.7852 265.0202 267.2314 14.1325 -1.2113 263.7839 264.9951 267.2801 14.8938 -1.2072 263.9062 265.1134 267.3282 15.7428 -1.1987 264.0066 265.2053 267.4933 16.5310 -1.1962 264.0417 265.2380 267.6065 17.3190 -1.1955 264.1715 265.3669 267.6809 18.1370 -1.1933 264.2078 265.4011 267.7994 18.8950 -1.1974 264.1900 265.3874 267.8709 19.7435 -1.1708 264.2510 265.4217 267.9210 20.5333 -1.1684 264.4012 265.5696 268.0534 21.3220 -1.1641 264.4882 265.6523 268.0870 22.1405 -1.1572 264.4662 265.6234 268.2237 22.8990 -1.1549 264.5816 265.7365 268.3196 23.7483 -1.1393 264.6760 265.8154 268.3830 24.5375 -1.1365 264.7049 265.8414 268.5953 25.3275 -1.1332 264.8432 265.9763 268.6989 26.1585 -1.1343 264.8450 265.9793 268.7595 26.9298 -1.1073 264.8868 265.9941 268.8297 27.7515 -1.1176 265.0356 266.1531 269.0074 28.5435 -1.1149 265.0271 266.1421 269.1122 29.3655 -1.1137 265.1176 266.2314 269.2200 30.1580 -1.1103 265.2359 266.3462 269.3692 30.9495 -1.0982 265.4001 266.4983 269.6429 31.7715 -1.1004 265.3596 266.4599 269.7041 32.5335 -1.1019 265.4201 266.5220 269.7682 33.3865 -1.1017 265.5321 266.6338 269.9275 34.1785 -1.0975 265.5567 266.6542 269.9793 34.9705 -1.0938 265.6494 266.7432 270.1427 35.7935 -1.0841 265.7420 266.8262 270.3181 36.5865 -1.1089 265.7898 266.8987 270.3695 37.4085 -1.1017 265.8444 266.9461 270.5180 38.2015 -1.1004 265.9107 267.0110 270.6446 38.9943 -1.0992 266.0572 267.1565 270.6867 39.8165 -1.0942 266.0940 267.1882 270.7890 40.6080 -1.0952 266.1336 267.2288 270.9158 41.4305 -1.0952 266.2520 267.3472 271.0590 42.2235 -1.1015 266.2460 267.3476 271.1842 43.0155 -1.0979 266.3644 267.4623 271.2977 43.8378 -1.1000 266.3849 267.4849 271.4554 44.6295 -1.0915 266.4322 267.5237 271.5244 45.4518 -1.0665 266.5844 267.6509 271.6347 46.2438 -1.0696 266.6853 267.7550 271.7648 47.0355 -1.0675 266.7241 267.7917 271.8976 47.8583 -1.0823 266.8129 267.8951 272.0423 48.6460 -1.0740 266.8390 267.9130 272.0628 49.4640 -1.0617 266.8962 267.9579 272.1685 50.2533 -1.0591 267.0938 268.1529 272.3115 51.0425 -1.0617 267.0736 268.1353 272.4714 51.8603 -1.0512 267.1370 268.1882 272.6118 52.6480 -1.0683 267.2814 268.3497 272.6228 53.4663 -1.0784 267.3323 268.4107 272.7254 54.2553 -1.0768 267.3986 268.4754 272.8020 55.0453 -1.0659 267.4812 268.5471 273.0013 55.8635 -1.0789 267.4751 268.5541 273.0830 56.6528 -1.0588 267.5853 268.6441 273.1788 57.4725 -1.0610 267.6398 268.7007 273.2409 58.2618 -1.0575 267.8308 268.8882 273.3780 59.0523 -1.0538 267.9305 268.9843 273.5171 59.8745 -1.0539 267.9730 269.0269 273.5933 60.6665 -1.0541 267.9614 269.0155 273.6769 61.4888 -1.0500 268.0825 269.1325 273.7843 62.2810 -1.0417 268.1542 269.1959 274.0036 63.0718 -1.0329 268.2206 269.2535 273.9839 63.8938 -1.0374 268.3222 269.3596 274.0988 64.6855 -1.0152 268.4110 269.4261 274.2291 65.5078 -0.9999 268.4727 269.4726 274.2434 66.3003 -0.9889 268.5586 269.5474 274.4060 67.0925 -1.0042 268.6941 269.6984 274.6052 67.9145 -1.0249 268.6032 269.6281 274.6911 68.7065 -1.0323 268.7614 269.7937 274.7665 69.5288 -1.0334 268.8576 269.8911 274.9183 70.3205 -1.0421 268.9865 270.0286 275.0141 71.1125 -1.0298 269.0598 270.0896 275.1241 71.9353 -1.0306 269.1267 270.1573 275.0965 72.7275 -1.0313 269.2156 270.2469 275.1106 73.5505 -1.0246 269.2937 270.3183 275.3060 74.3435 -1.0329 269.4157 270.4486 275.3172 75.1355 -1.0405 269.4758 270.5163 275.4595 75.9575 -1.0281 269.4693 270.4974 275.5892 76.7495 -1.0205 269.5731 270.5936 275.6431 77.5715 -1.0132 269.6315 270.6447 275.5803 78.3635 -1.0185 269.7424 270.7609 275.7327 79.1548 -1.0117 269.7540 270.7657 275.7386 80.0065 -1.0234 269.9554 270.9787 275.8046 80.7648 -1.0135 269.9605 270.9740 275.7822 81.5843 -1.0126 270.0634 271.0760 275.8934 82.3728 -1.0115 270.1414 271.1529 276.0649 83.1608 -1.0101 270.2726 271.2827 276.2551 83.9790 -0.9997 270.3598 271.3595 276.2815 84.7670 -1.0077 270.4092 271.4169 276.3523 85.5858 -1.0138 270.3620 271.3758 276.4668 86.3743 -1.0031 270.5111 271.5142 276.5114 87.1640 -0.9949 270.5872 271.5821 276.6702 87.9948 -0.9991 270.6708 271.6699 276.7995 88.7540 -0.9909 270.7272 271.7180 276.9313 89.6033 -0.9931 270.7341 271.7273 276.9873 90.3923 -0.9903 270.8189 271.8093 277.0532 91.1835 -0.9824 270.9908 271.9732 277.0599 92.0053 -0.9951 271.1141 272.1092 277.2395 92.7675 -0.9966 271.1547 272.1513 277.3341 93.6195 -0.9838 271.1592 272.1430 277.4673 94.3815 -0.9946 271.2851 272.2797 277.6165 95.2035 -0.9955 271.4309 272.4264 277.7556 96.0253 -0.9984 271.4407 272.4391 277.8815 96.7873 -1.0053 271.5394 272.5447 277.9474 97.6410 -1.0052 271.6343 272.6396 277.9732 98.4330 -0.9913 271.7897 272.7810 278.2465 99.2245 -0.9861 271.8556 272.8418 278.4627 100.0485 -0.9982 271.9758 272.9740 278.6525 100.8105 -0.9857 271.9871 272.9728 278.6354 101.6630 -0.9949 272.0711 273.0660 278.6480 102.4253 -0.9889 272.1835 273.1724 278.6726 103.2488 -0.9997 272.3487 273.3484 278.8460 104.0718 -0.9919 272.5192 273.5111 278.9039 104.8345 -0.9902 272.5607 273.5509 279.0147 105.6873 -0.9874 272.6300 273.6174 279.2552 106.4495 -0.9789 272.7235 273.7024 279.3181 107.2718 -0.9808 272.9331 273.9139 279.2446 108.1060 -0.9845 273.0875 274.0719 279.3521 108.8795 -0.9948 273.1204 274.1152 279.3835 109.7015 -0.9961 273.2079 274.2040 279.5749 110.4635 -0.9991 273.4156 274.4147 279.8241 111.3155 -0.9961 273.5128 274.5088 279.9700 112.0770 -0.9918 273.5230 274.5148 279.9692 112.8960 -1.0089 273.5873 274.5962 280.1189 113.7140 -0.9944 273.7647 274.7591 280.3569 114.4720 -0.9923 273.9064 274.8986 280.3493 115.3223 -1.0080 274.0677 275.0756 280.4421 116.0800 -0.9966 274.0575 275.0541 280.6976 116.8988 -0.9998 274.0258 275.0256 280.7057 117.7173 -0.9970 274.1655 275.1625 280.7257 118.4760 -0.9881 274.3461 275.3342 280.8968 119.3258 -1.0029 274.4433 275.4462 281.4724 120.0850 -1.0254 274.4740 275.4993 281.7835 120.9045 -1.0340 274.5844 275.6183 281.8458 121.7233 -1.0259 274.7077 275.7336 281.7794 122.4828 -1.0160 274.8416 275.8576 281.8336 123.3345 -1.0183 274.9172 275.9355 281.9860 124.0963 -1.0104 274.9814 275.9918 281.7887 124.9175 -0.9946 275.0763 276.0709 281.7029 125.7398 -1.0105 275.2348 276.2453 281.8734 126.5015 -1.0241 275.2891 276.3132 282.0791 127.3538 -1.0144 275.4640 276.4784 282.2214 128.1155 -1.0194 275.5846 276.6041 282.1532 128.9375 -1.0165 275.6863 276.7028 282.3897 129.7298 -1.0196 275.7433 276.7628 282.4458 130.5215 -1.0247 275.7992 276.8239 282.5271 131.3735 -1.0253 275.8774 276.9027 282.7709 132.1355 -1.0244 275.8549 276.8792 283.0146 132.9595 -1.0331 275.9247 276.9578 283.0330 133.7515 -1.0219 275.9571 276.9790 283.0152 134.5435 -1.0238 275.9808 277.0046 283.3116 135.3955 -1.0263 276.1662 277.1926 283.3912 136.1580 -1.0351 276.1304 277.1654 283.5046 136.9813 -1.0280 276.2284 277.2564 283.6549 137.7733 -1.0362 276.2090 277.2452 283.6104 138.5670 -1.0252 276.3273 277.3526 283.8648 139.4250 -1.0211 276.4576 277.4787 283.9633 140.1865 -1.0265 276.4696 277.4960 284.0204 141.0088 -1.0389 276.6918 277.7307 284.1206 141.8310 -1.0340 276.8111 277.8451 284.1584 142.5925 -1.0269 276.8274 277.8543 284.2231 143.4453 -1.0330 276.7882 277.8212 284.2868 144.2063 -1.0380 277.0012 278.0391 284.4009 145.0240 -1.0453 277.1039 278.1492 284.5547 145.8423 -1.0361 277.2221 278.2581 284.4265 146.6000 -1.0358 277.1531 278.1888 284.6921 147.4495 -1.0290 277.3182 278.3472 284.6892 148.2083 -1.0332 277.4203 278.4534 284.7958 149.0270 -1.0375 277.4664 278.5038 285.0451 149.8453 -1.0335 277.4038 278.4373 285.0486 150.6033 -1.0374 277.5042 278.5417 285.0156 151.4520 -1.0408 277.5874 278.6281 285.0572 152.2405 -1.0481 277.8186 278.8668 285.1236 153.0290 -1.0437 277.7510 278.7947 285.2258 153.8483 -1.0261 277.9240 278.9501 285.4110 154.6370 -1.0473 278.1007 279.1479 285.4652 155.4563 -1.0389 278.0734 279.1123 285.5321 156.2468 -1.0469 278.2091 279.2559 285.6411 157.0375 -1.0599 278.2298 279.2897 285.7687 157.8615 -1.0615 278.3664 279.4278 285.9179 158.6535 -1.0361 278.5319 279.5680 286.0367 159.4938 -1.0503 278.6979 279.7483 286.0502 160.2610 -1.0492 278.7411 279.7903 286.1792 161.0838 -1.0368 278.8109 279.8477 286.1883 161.8758 -1.0406 278.8666 279.9072 286.2734 162.6675 -1.0554 278.9576 280.0130 286.1272 163.5198 -1.0395 279.0273 280.0667 286.2182 164.2815 -1.0508 279.2496 280.3004 286.2423 165.1045 -1.0385 279.2101 280.2485 286.3530 165.8965 -1.0341 279.2274 280.2615 286.3843 166.6885 -1.0197 279.4024 280.4221 286.5520 167.5405 -1.0423 279.4582 280.5004 286.8522 168.3025 -1.0314 279.5235 280.5549 286.9759 169.1245 -1.0385 279.5229 280.5614 287.1257 169.9188 -1.0383 279.6433 280.6816 287.3738 170.7115 -1.0329 279.7198 280.7528 287.4733 171.5635 -1.0325 279.8850 280.9176 287.8068 172.3255 -1.0330 279.9880 281.0210 287.8255 173.1495 -1.0477 280.1098 281.1576 288.0183 173.9415 -1.0514 280.1323 281.1837 288.1675 174.7335 -1.0426 280.2937 281.3363 288.2474 175.5855 -1.0449 280.3084 281.3533 288.4418 176.3473 -1.0403 280.4668 281.5071 288.5769 177.1688 -1.0454 280.6568 281.7023 288.7695 177.9565 -1.0476 280.6917 281.7393 288.9696 178.7448 -1.0482 280.6320 281.6802 289.0640 179.5930 -1.0423 280.5928 281.6351 289.2757 180.3510 -1.0423 280.8191 281.8614 289.5107 181.1718 -1.0545 281.0683 282.1227 289.6750 181.9605 -1.0540 281.2051 282.2591 289.8061 182.7490 -1.0634 281.3505 282.4140 289.8562 183.5993 -1.0496 281.3366 282.3861 289.8989 184.3580 -1.0558 281.3304 282.3862 289.9731 185.1768 -1.0591 281.4297 282.4888 290.0967 185.9953 -1.0681 281.5838 282.6519 290.1100 186.7560 -1.0566 281.5817 282.6383 290.2175 187.6075 -1.0653 281.7385 282.8038 290.3629 188.3690 -1.0628 281.9498 283.0126 290.4088 189.1905 -1.0686 282.0468 283.1154 290.4771 190.0198 -1.0752 282.0322 283.1074 290.4996 190.7885 -1.0832 281.9906 283.0738 290.5721 191.6105 -1.0825 282.1692 283.2517 290.7429 192.3720 -1.0797 282.2053 283.2850 290.8686 193.2278 -1.0992 282.4301 283.5292 290.9486 194.0200 -1.0922 282.5645 283.6568 290.9885 194.8120 -1.0849 282.6771 283.7620 291.0120 195.6343 -1.0838 282.7273 283.8111 291.2221 196.3958 -1.0887 282.8267 283.9155 291.3604 197.2480 -1.0944 282.9531 284.0476 291.4101 198.0098 -1.0875 283.0937 284.1812 291.4711 198.8328 -1.0862 283.0983 284.1845 291.5672 199.6548 -1.0973 283.1596 284.2570 291.6918 200.4165 -1.0944 283.2366 284.3309 291.6983 201.2688 -1.0928 283.3901 284.4829 291.7306 202.0308 -1.1055 283.3140 284.4195 292.0321 202.8528 -1.0960 283.4328 284.5288 292.0271 203.6748 -1.1025 283.5704 284.6729 292.0914 204.4365 -1.1142 283.7308 284.8451 292.2297 205.2888 -1.1103 283.8948 285.0051 292.2523 206.0510 -1.0996 284.1181 285.2177 292.3976 206.8738 -1.1000 284.1134 285.2135 292.6654 207.6968 -1.1051 284.2167 285.3218 292.6891 208.4585 -1.1127 284.2489 285.3616 292.6970 209.3090 -1.1013 284.5035 285.6048 292.8584 210.0670 -1.1068 284.5349 285.6416 292.9834 210.9008 -1.1129 284.6476 285.7605 292.9835 211.6890 -1.1200 284.8040 285.9241 293.0813 212.4770 -1.1082 284.7240 285.8322 293.1579 213.2958 -1.1147 284.7321 285.8468 293.3521 214.0840 -1.1189 285.1020 286.2209 293.4245 214.9020 -1.1165 285.0744 286.1909 293.5768 215.6905 -1.1184 285.1886 286.3071 293.6178 216.4813 -1.1152 285.2301 286.3454 293.6761 217.3040 -1.1112 285.3298 286.4410 293.8207 218.0940 -1.1304 285.4917 286.6221 293.9837 218.9138 -1.1337 285.5190 286.6527 294.0629 219.7043 -1.1348 285.5901 286.7249 294.1274 220.4955 -1.1264 285.6799 286.8063 294.2884 221.3175 -1.1210 285.8266 286.9477 294.4655 222.1093 -1.1310 285.8854 287.0164 294.5676 222.9305 -1.1490 285.9480 287.0970 294.7053 223.7230 -1.1363 286.0836 287.2199 294.8314 224.5155 -1.1455 286.1052 287.2507 294.8753 225.3378 -1.1558 286.2022 287.3580 294.9626 226.0995 -1.1652 286.0599 287.2251 295.2097 226.9525 -1.1421 286.0680 287.2101 295.2648 227.7445 -1.1526 286.1309 287.2835 295.3842 228.5365 -1.1464 286.1694 287.3158 295.4977 229.3585 -1.1520 286.2067 287.3588 295.5557 230.1205 -1.1545 286.2733 287.4279 295.6438 230.9735 -1.1470 286.4288 287.5758 295.7872 231.7655 -1.1485 286.5028 287.6513 295.8887 232.5575 -1.1613 286.7439 287.9052 295.9932 233.3795 -1.1594 286.8771 288.0365 296.1417 234.1715 -1.1630 286.8615 288.0245 296.2272 234.9928 -1.1534 287.0864 288.2398 296.2556 235.7855 -1.1721 287.3108 288.4829 296.3756 236.5775 -1.1624 287.3557 288.5181 296.4616 237.4000 -1.1482 287.6280 288.7762 296.5490 238.1915 -1.1562 287.5746 288.7308 296.5365 239.0138 -1.1496 287.7210 288.8706 296.6502 239.8060 -1.1624 287.7635 288.9260 296.8755 240.5985 -1.1565 287.6321 288.7886 297.0097 241.4313 -1.1645 287.7621 288.9266 297.1250 242.1940 -1.1618 287.9798 289.1416 297.2012 243.0133 -1.1531 288.0311 289.1842 297.2925 243.8013 -1.1677 288.2116 289.3793 297.3436 244.6200 -1.1621 288.4185 289.5806 297.5116 245.4085 -1.1654 288.5260 289.6914 297.6190 246.1973 -1.1612 288.6414 289.8026 297.7261 247.0170 -1.1625 288.6778 289.8403 297.8005 247.8065 -1.1779 288.8677 290.0456 297.8978 248.6250 -1.1721 289.0300 290.2022 297.9896 249.4138 -1.1723 289.0854 290.2577 298.1554 250.2055 -1.1894 289.2913 290.4806 298.2163 251.0548 -1.1894 289.4235 290.6129 298.3020 251.8140 -1.1847 289.5756 290.7602 298.3457 252.6370 -1.1883 289.6855 290.8737 298.4658 253.4290 -1.1936 289.7184 290.9120 298.5893 254.2205 -1.1957 289.9940 291.1897 298.7496 255.0728 -1.2029 290.0769 291.2797 298.7877 255.8350 -1.1962 290.1361 291.3324 298.8551 256.6578 -1.1971 290.2791 291.4762 299.0067 257.4498 -1.2079 290.4105 291.6183 299.0875 258.2415 -1.2020 290.3798 291.5818 299.3504 259.0640 -1.1965 290.4713 291.6679 299.4765 259.8555 -1.1991 290.6500 291.8491 299.4587 260.6778 -1.2011 290.7653 291.9664 299.5420 261.4778 -1.2019 290.7796 291.9815 299.6374 262.2895 -1.1938 291.0061 292.1999 299.8351 263.0818 -1.2021 291.1608 292.3630 299.8582 263.8735 -1.2136 291.1853 292.3989 300.0241 264.6955 -1.2015 291.2904 292.4919 300.1427 265.4875 -1.2015 291.4725 292.6739 300.1882 266.3095 -1.2170 291.5442 292.7611 300.3667 267.1020 -1.2185 291.7165 292.9350 300.4348 267.8945 -1.2182 291.8551 293.0734 300.4612 268.7165 -1.2186 291.9293 293.1479 300.5800 269.5085 -1.2158 291.9612 293.1770 300.8155 270.3305 -1.2272 292.1359 293.3631 300.7830 271.1228 -1.2248 292.2460 293.4708 300.8882 271.9155 -1.2204 292.3630 293.5834 300.9967 272.7373 -1.2167 292.5027 293.7193 301.0330 273.5260 -1.2182 292.6104 293.8285 301.1723 274.3438 -1.2288 292.6294 293.8582 301.3425 275.1320 -1.2456 292.7930 294.0386 301.4298 275.9220 -1.2476 292.8675 294.1151 301.5860 276.7400 -1.2493 293.0333 294.2826 301.6822 277.4980 -1.2376 293.0232 294.2608 301.7304 278.3488 -1.2337 293.1289 294.3626 301.8770 279.1370 -1.2484 293.1842 294.4326 301.9838 279.9263 -1.2611 293.3902 294.6513 302.0899 280.7453 -1.2526 293.4394 294.6919 302.2098 281.5340 -1.2535 293.6072 294.8607 302.2598 282.3718 -1.2644 293.7807 295.0450 302.2982 283.1370 -1.2638 293.8843 295.1482 302.5072 283.9575 -1.2593 293.9708 295.2301 302.6177 284.7490 -1.2542 293.9942 295.2484 302.7146 285.5403 -1.2475 294.1256 295.3732 302.8747 286.3615 -1.2515 294.2050 295.4565 302.9310 287.1235 -1.2482 294.3779 295.6261 302.9754 287.9775 -1.2510 294.5231 295.7741 303.0840 288.7695 -1.2618 294.6366 295.8984 303.2445 289.5615 -1.2620 294.7288 295.9908 303.3177 290.3843 -1.2561 294.7772 296.0333 303.3123 291.1465 -1.2631 294.8062 296.0693 303.5384 291.9980 -1.2611 294.9877 296.2488 303.5902 292.7600 -1.2756 295.1112 296.3868 303.7108 293.5818 -1.2703 295.2480 296.5183 303.8698 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