DTA measure 3olom_1 Test Date: 2024228:1350 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1461.83 s Mass = 1138.500 mg data_number = 1816 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2115 -4.9633 441.2692 446.2326 424.6169 2.0045 -4.9676 441.2501 446.2176 424.6115 2.8265 -4.9776 441.2469 446.2245 424.5673 3.6185 -4.9872 441.0933 446.0805 424.5030 4.4405 -4.9804 441.2342 446.2145 424.5143 5.2328 -4.9899 441.2959 446.2858 424.4287 6.0255 -5.0029 441.1783 446.1812 424.4760 6.8475 -4.9964 441.2966 446.2930 424.4487 7.6395 -5.0097 441.2478 446.2574 424.4342 8.4615 -4.9971 441.3219 446.3190 424.3991 9.2655 -4.9923 441.2088 446.2011 424.2886 10.0658 -5.0139 441.2367 446.2506 424.3393 10.8545 -4.9970 441.2899 446.2869 424.3174 11.6440 -5.0344 441.2354 446.2698 424.2044 12.4628 -5.0215 441.2443 446.2658 424.0264 13.2220 -5.0104 441.3756 446.3859 423.9853 14.0705 -5.0231 441.3645 446.3876 423.9036 14.8590 -5.0257 441.2975 446.3232 423.8791 15.6470 -5.0071 441.1783 446.1855 423.8213 16.4658 -5.0350 441.3264 446.3614 423.5974 17.2550 -5.0322 441.3932 446.4254 423.5519 18.0743 -5.0294 441.4665 446.4959 423.4691 18.8635 -5.0331 441.4412 446.4743 423.3157 19.6610 -5.0297 441.4310 446.4607 423.3138 20.4603 -5.0238 441.4077 446.4315 423.2311 21.2510 -5.0500 441.4834 446.5333 423.0143 22.1015 -5.0304 441.3822 446.4125 422.9545 22.8635 -5.0313 441.4339 446.4653 422.9021 23.6865 -5.0635 441.4151 446.4786 422.7671 24.4785 -5.0742 441.4359 446.5102 422.6451 25.2705 -5.0735 441.2753 446.3488 422.4722 26.1225 -5.0769 441.3284 446.4052 422.3787 26.8845 -5.0553 441.4103 446.4655 422.2313 27.7063 -5.0610 441.3649 446.4259 422.1367 28.4983 -5.0779 441.2980 446.3759 422.0749 29.2898 -5.0615 441.2913 446.3528 422.0163 30.1130 -5.0613 441.2836 446.3449 421.8879 30.9048 -5.0721 441.1801 446.2521 421.6337 31.7268 -5.0507 441.2080 446.2587 421.5527 32.5193 -5.0686 441.2759 446.3445 421.5193 33.3115 -5.0910 441.3771 446.4681 421.4124 34.1338 -5.0933 441.3152 446.4085 421.2377 34.9255 -5.0705 441.2566 446.3271 421.1329 35.7478 -5.0576 441.2328 446.2903 421.0123 36.5408 -5.0923 441.3470 446.4394 421.0040 37.3335 -5.0764 441.3034 446.3798 420.8290 38.1558 -5.0966 441.2973 446.3939 420.7414 38.9175 -5.0886 441.3330 446.4215 420.7534 39.7723 -5.0736 441.3481 446.4218 420.6119 40.5288 -5.0829 441.2926 446.3754 420.4199 41.3803 -5.0714 441.2781 446.3495 420.3081 42.1690 -5.0768 441.1423 446.2191 420.2065 42.9570 -5.0722 441.2335 446.3057 420.0705 43.7758 -5.0568 441.0882 446.1450 420.0404 44.5340 -5.0819 441.1257 446.2076 419.9797 45.3850 -5.0705 441.2111 446.2816 419.7806 46.1438 -5.1022 441.1166 446.2188 419.6579 46.9650 -5.1081 441.0145 446.1227 419.5939 47.7835 -5.1117 441.1372 446.2488 419.5747 48.5448 -5.1057 441.1814 446.2870 419.4401 49.3985 -5.0907 440.8272 445.9179 419.3552 50.1608 -5.0892 440.9732 446.0624 419.3075 50.9823 -5.1114 441.0474 446.1589 419.2599 51.7713 -5.1000 441.0173 446.1173 419.1103 52.5613 -5.0984 441.0827 446.1810 418.8990 53.4113 -5.0857 441.0270 446.1128 418.9054 54.1725 -5.1265 440.9989 446.1254 418.8278 54.9958 -5.1004 441.1220 446.2223 418.6514 55.7875 -5.1009 441.0294 446.1304 418.5339 56.5795 -5.0900 441.0099 446.1000 418.5097 57.4030 -5.0875 440.8766 445.9641 418.3492 58.1958 -5.0903 440.9218 446.0121 418.3165 59.0175 -5.0706 441.0060 446.0766 418.1511 59.8103 -5.1098 440.9592 446.0690 418.0643 60.6035 -5.1075 440.8214 445.9289 417.9965 61.4255 -5.1026 440.8766 445.9792 417.7986 62.2175 -5.1132 440.9361 446.0493 417.6440 63.0395 -5.0998 440.8172 445.9169 417.6152 63.8315 -5.1262 440.7659 445.8922 417.5460 64.6235 -5.1587 440.8108 445.9695 417.4698 65.4455 -5.1709 440.7379 445.9087 417.4002 66.2375 -5.1620 440.8142 445.9762 417.2334 67.0595 -5.1489 440.7084 445.8573 417.0805 67.8518 -5.1499 440.5495 445.6994 417.0357 68.6450 -5.1689 440.3403 445.5091 416.9067 69.4685 -5.1991 440.4179 445.6169 416.7967 70.2315 -5.1847 440.3300 445.5148 416.6455 71.0840 -5.1850 440.4237 445.6086 416.5365 71.8758 -5.1577 440.3774 445.5350 416.4846 72.6675 -5.1371 440.2472 445.3843 416.4672 73.4910 -5.1426 440.3506 445.4932 416.3777 74.2545 -5.1711 440.2781 445.4492 416.3437 75.0988 -5.1884 440.2624 445.4508 416.1028 75.8870 -5.1776 440.1611 445.3387 415.9919 76.6755 -5.1746 440.3113 445.4859 415.9646 77.4930 -5.1562 440.1719 445.3281 415.9259 78.2510 -5.1114 440.1030 445.2143 415.7122 79.0995 -5.1563 440.1644 445.3207 415.5934 79.8873 -5.1866 440.0640 445.2506 415.4961 80.6750 -5.1729 440.1332 445.3062 415.5382 81.4948 -5.1925 439.9919 445.1845 415.3383 82.2843 -5.2063 439.9671 445.1735 415.2034 83.1030 -5.1638 439.9948 445.1586 415.2433 83.8918 -5.1490 439.9308 445.0799 415.1263 84.6810 -5.1354 439.8646 445.0000 415.0602 85.5025 -5.1567 439.9767 445.1334 414.8621 86.2933 -5.1832 439.8921 445.0753 414.7314 87.1140 -5.1792 439.7481 444.9272 414.6325 87.9038 -5.1742 439.7558 444.9300 414.5871 88.6955 -5.1728 439.8412 445.0140 414.4241 89.5478 -5.1811 439.6835 444.8647 414.3147 90.3095 -5.1691 439.7389 444.9080 414.2060 91.1408 -5.1785 439.6091 444.7876 414.1749 91.9198 -5.1714 439.6649 444.8363 414.0323 92.7418 -5.1759 439.6531 444.8290 413.9223 93.5338 -5.1564 439.4913 444.6478 413.8307 94.3255 -5.1768 439.5659 444.7427 413.6780 95.1480 -5.1729 439.5284 444.7013 413.5452 95.9400 -5.1807 439.4385 444.6193 413.4404 96.7628 -5.1770 439.3825 444.5594 413.4125 97.5550 -5.1942 439.2810 444.4751 413.2969 98.3475 -5.1845 439.2770 444.4616 413.1680 99.1995 -5.1620 439.1862 444.3482 413.1053 99.9618 -5.1638 439.2160 444.3797 412.9261 100.7845 -5.1717 439.2490 444.4206 412.8645 101.5765 -5.1629 439.2419 444.4048 412.8448 102.3685 -5.1831 439.0675 444.2506 412.7436 103.2205 -5.1851 439.1569 444.3421 412.5972 103.9830 -5.1934 439.0897 444.2831 412.5605 104.8065 -5.1697 438.9752 444.1449 412.3616 105.5985 -5.1618 438.9605 444.1223 412.3563 106.3895 -5.1860 438.8022 443.9882 412.2011 107.2378 -5.1722 438.6662 443.8384 412.1618 107.9955 -5.1627 438.6876 443.8503 412.0682 108.8138 -5.1707 438.7184 443.8891 411.9079 109.6018 -5.1771 438.6403 443.8174 411.7877 110.3898 -5.1453 438.5300 443.6753 411.7532 111.2380 -5.1402 438.6583 443.7984 411.6452 111.9690 -5.1467 438.5636 443.7102 411.5789 112.8255 -5.1325 438.5431 443.6756 411.4462 113.6153 -5.1254 438.6178 443.7432 411.3851 114.4040 -5.1198 438.6029 443.7227 411.3326 115.2233 -5.1417 438.6161 443.7578 411.2502 116.0120 -5.1611 438.4257 443.5868 411.1271 116.8348 -5.1337 438.3099 443.4436 411.0294 117.6258 -5.1086 438.3415 443.4500 410.9242 118.4173 -5.1189 438.3807 443.4995 410.7800 119.2385 -5.0852 438.2344 443.3196 410.6475 120.0295 -5.0923 438.1697 443.2620 410.4519 120.8515 -5.0770 438.1817 443.2586 410.4120 121.6440 -5.0714 438.0637 443.1351 410.2899 122.4365 -5.0630 437.9862 443.0492 410.1649 123.2585 -5.0581 437.9525 443.0106 410.0706 124.0205 -5.0559 437.9285 442.9845 410.0263 124.8743 -5.0593 437.9115 442.9708 409.8806 125.6665 -5.0692 437.7377 442.8069 409.7779 126.4578 -5.0731 437.6656 442.7387 409.7136 127.2800 -5.0841 437.6391 442.7233 409.5618 128.0415 -5.0740 437.5667 442.6407 409.5272 128.8950 -5.0834 437.6186 442.7019 409.4310 129.6868 -5.0529 437.4864 442.5393 409.3849 130.4785 -5.0392 437.4379 442.4771 409.3073 131.3008 -5.0537 437.3756 442.4293 409.1602 132.0938 -5.0565 437.2987 442.3552 409.0478 132.9178 -5.0362 437.2490 442.2852 408.9465 133.7098 -5.0161 437.1621 442.1782 408.8378 134.5015 -5.0329 437.1087 442.1416 408.7100 135.3238 -5.0590 437.0843 442.1433 408.5242 136.1155 -5.0453 436.9792 442.0246 408.4414 136.9378 -5.0647 436.9204 441.9851 408.3370 137.7295 -5.0476 436.7611 441.8087 408.2666 138.5195 -5.0267 436.7094 441.7360 408.2515 139.3375 -5.0419 436.7238 441.7657 408.0869 140.1250 -5.0372 436.6841 441.7213 407.9856 140.9430 -5.0582 436.5589 441.6170 407.7751 141.7320 -5.0329 436.4495 441.4824 407.6988 142.5320 -5.0371 436.3502 441.3873 407.5510 143.3333 -5.0555 436.2910 441.3465 407.3774 144.1220 -5.0493 436.1286 441.1779 407.1996 144.9413 -5.0513 436.1373 441.1885 407.0402 145.7300 -5.0491 436.0678 441.1169 406.9667 146.5490 -5.0486 435.9880 441.0365 406.7767 147.3373 -5.0575 435.9464 441.0039 406.8401 148.1270 -5.0474 435.9334 440.9808 406.7139 148.9763 -5.0652 435.8728 440.9380 406.5226 149.7360 -5.0606 435.7895 440.8501 406.4217 150.5568 -5.0845 435.6480 440.7324 406.4576 151.3788 -5.0710 435.5905 440.6615 406.3279 152.1405 -5.0672 435.5511 440.6183 406.2686 153.1105 -5.0458 435.5015 440.5473 406.1530 153.9930 -5.0402 435.4608 440.5010 406.0131 154.7545 -5.0555 435.4342 440.4897 405.9554 155.5770 -5.0681 435.3529 440.4210 405.9025 156.3998 -5.0561 435.1162 440.1723 405.7377 157.1615 -5.0385 435.0279 440.0665 405.6278 158.0135 -5.0317 435.0335 440.0651 405.6181 158.7755 -5.0327 434.9136 439.9463 405.5529 159.5975 -5.0211 434.7569 439.7779 405.4645 160.4195 -5.0170 434.6361 439.6531 405.3005 161.1815 -5.0224 434.5789 439.6014 405.1857 162.0350 -5.0370 434.5677 439.6047 405.0329 162.8678 -5.0393 434.3890 439.4284 404.9756 163.8213 -5.0498 434.3564 439.4062 404.9307 164.6135 -5.0390 434.1519 439.1909 404.7803 165.4355 -5.0106 434.1427 439.1533 404.6581 166.2273 -4.9947 434.0881 439.0828 404.7523 167.0488 -5.0080 433.9491 438.9571 404.5548 167.8408 -5.0158 433.9377 438.9536 404.5776 168.6325 -5.0370 433.7639 438.8009 404.4620 169.4850 -5.0109 433.7229 438.7338 404.3642 170.2465 -5.0305 433.6601 438.6906 404.2799 171.0658 -4.9913 433.5642 438.5555 404.0915 171.8530 -5.0121 433.4553 438.4675 403.9656 172.6415 -5.0199 433.3645 438.3845 403.9362 173.4623 -5.0106 433.2702 438.2808 403.7341 174.2508 -5.0032 433.2832 438.2864 403.6622 175.0698 -4.9629 433.1768 438.1397 403.6098 175.8598 -4.9810 433.1120 438.0930 403.4946 176.6518 -4.9880 433.0841 438.0721 403.4415 177.4708 -4.9974 432.9460 437.9434 403.2269 178.2323 -5.0135 432.8792 437.8927 403.1338 179.0845 -4.9901 432.7841 437.7742 403.0904 179.8728 -4.9773 432.7286 437.7059 402.9568 180.6635 -4.9705 432.6512 437.6217 402.8685 181.4858 -4.9666 432.5802 437.5468 402.7801 182.2480 -4.9843 432.5004 437.4847 402.7024 183.1003 -4.9631 432.4631 437.4262 402.4732 183.8603 -4.9735 432.4214 437.3949 402.3804 184.7123 -4.9632 432.3510 437.3142 402.2121 185.4743 -4.9585 432.2763 437.2348 402.2061 186.2978 -4.9610 432.0859 437.0469 402.0496 187.0898 -4.9773 432.1277 437.1050 402.0103 187.8815 -4.9932 432.0398 437.0330 401.9466 188.7373 -5.0001 432.0426 437.0427 401.7973 189.4985 -5.0073 431.8824 436.8896 401.7024 190.3208 -4.9923 431.8638 436.8561 401.6182 191.1155 -4.9690 431.7615 436.7305 401.5225 191.9075 -4.9753 431.6113 436.5866 401.4220 192.7298 -4.9555 431.5503 436.5058 401.2319 193.4938 -4.9635 431.5066 436.4701 401.1049 194.3478 -4.9797 431.3849 436.3646 401.0723 195.1400 -4.9741 431.2850 436.2591 401.0217 195.9325 -4.9695 431.2274 436.1969 400.9120 196.7560 -5.0067 431.1422 436.1489 400.8514 197.5195 -5.0095 431.1104 436.1199 400.6477 198.3738 -5.0082 430.9987 436.0068 400.5166 199.1413 -5.0088 430.9079 435.9166 400.4734 199.9650 -5.0009 430.8084 435.8094 400.3657 200.7575 -4.9958 430.8059 435.8018 400.2143 201.5518 -4.9954 430.6942 435.6896 400.1570 202.3775 -4.9637 430.6271 435.5908 400.0379 203.1695 -4.9444 430.5620 435.5065 399.9638 203.9963 -4.9360 430.4275 435.3635 399.8513 204.7668 -4.9200 430.4264 435.3464 399.6926 205.5848 -4.9156 430.3416 435.2572 399.5437 206.3748 -4.9212 430.2100 435.1312 399.4685 207.1650 -4.9222 430.0830 435.0052 399.4208 207.9873 -4.9214 430.0645 434.9858 399.3332 208.7470 -4.9249 429.9427 434.8676 399.2120 209.5955 -4.9252 429.8910 434.8162 399.0929 210.3868 -4.9145 429.8054 434.7199 398.9142 211.1783 -4.9169 429.6546 434.5715 398.9520 212.0018 -4.9216 429.6537 434.5753 398.8299 212.7653 -4.9121 429.6038 434.5159 398.7393 213.5885 -4.9334 429.5392 434.4725 398.6415 214.3815 -4.9230 429.4323 434.3553 398.4854 215.2065 -4.8994 429.3200 434.2193 398.4238 215.9985 -4.9124 429.3550 434.2674 398.2968 216.7905 -4.9281 429.2177 434.1458 398.2366 217.6125 -4.9350 429.1479 434.0828 398.0694 218.3758 -4.9462 429.1015 434.0478 397.9642 219.2298 -4.9210 428.8870 433.8080 397.8605 219.9915 -4.9037 428.7793 433.6830 397.7588 220.8143 -4.9089 428.7290 433.6379 397.6077 221.6138 -4.9106 428.7294 433.6401 397.5869 222.4075 -4.8928 428.6333 433.5261 397.4409 223.2328 -4.8845 428.5174 433.4019 397.3375 223.9955 -4.8955 428.4634 433.3590 397.3163 224.8470 -4.8920 428.2834 433.1754 397.0776 225.6413 -4.8933 428.1519 433.0452 397.0178 226.4355 -4.8953 428.1185 433.0138 396.8921 227.2578 -4.8948 428.0277 432.9225 396.8253 228.0208 -4.8989 427.9804 432.8793 396.7250 228.8843 -4.9111 427.9682 432.8792 396.6454 229.6478 -4.8920 427.7966 432.6885 396.5320 230.4755 -4.8828 427.7456 432.6284 396.3940 231.2678 -4.8858 427.7021 432.5880 396.2224 232.0595 -4.8786 427.5589 432.4375 396.1623 232.8825 -4.8845 427.4581 432.3426 396.1084 233.6465 -4.8700 427.3982 432.2683 395.9821 234.4988 -4.8668 427.3087 432.1755 395.9149 235.2928 -4.8776 427.3180 432.1956 395.9236 236.0840 -4.8567 427.1494 432.0061 395.7387 236.9070 -4.8740 427.0379 431.9119 395.5693 237.6675 -4.8775 427.0532 431.9308 395.4657 238.4885 -4.9012 426.9346 431.8358 395.4527 239.4910 -4.8629 426.7619 431.6248 395.2791 240.3410 -4.8616 426.6763 431.5379 395.1028 241.0993 -4.8510 426.6118 431.4628 394.9921 241.9180 -4.8588 426.5245 431.3833 394.9147 242.7365 -4.8344 426.3446 431.1790 394.8182 243.4950 -4.8479 426.2642 431.1121 394.7688 244.3448 -4.8377 426.2387 431.0763 394.6033 245.1333 -4.8303 426.1380 430.9684 394.5373 245.9233 -4.8180 426.0739 430.8919 394.3975 246.7430 -4.8289 425.9583 430.7871 394.3074 247.5035 -4.8619 425.8328 430.6947 394.1800 248.3570 -4.8522 425.7924 430.6446 394.0215 249.1485 -4.8572 425.7105 430.5677 393.9877 249.9405 -4.8513 425.6268 430.4781 393.8680 250.7635 -4.8398 425.5704 430.4102 393.8820 251.5265 -4.8232 425.5003 430.3235 393.7334 252.3788 -4.8133 425.3596 430.1730 393.6011 253.1705 -4.8360 425.2635 430.0994 393.4115 253.9625 -4.8340 425.2252 430.0592 393.3631 254.7850 -4.8172 425.0391 429.8563 393.3338 255.5550 -4.8294 425.0660 429.8953 393.2448 256.4065 -4.8236 424.9763 429.7999 393.0966 257.1685 -4.8034 424.8843 429.6877 393.0421 257.9905 -4.8070 424.6991 429.5061 392.9329 258.8125 -4.8225 424.6842 429.5067 392.7826 259.5745 -4.8203 424.6310 429.4513 392.7294 260.4273 -4.7996 424.4859 429.2854 392.5218 261.1895 -4.8352 424.3375 429.1727 392.3814 262.0115 -4.7961 424.3015 429.0976 392.3488 262.8335 -4.7884 424.2379 429.0263 392.2605 263.5953 -4.7913 424.1488 428.9400 392.1771 264.4485 -4.7855 424.0357 428.8212 392.0536 265.2108 -4.7877 423.8972 428.6849 391.9225 266.0328 -4.8059 423.8018 428.6076 391.8071 266.8548 -4.7926 423.7474 428.5399 391.7748 267.6150 -4.7838 423.6418 428.4256 391.7971 268.4615 -4.8005 423.5606 428.3611 391.6267 269.2203 -4.7934 423.5675 428.3609 391.4822 270.0385 -4.7963 423.4418 428.2381 391.3376 270.8568 -4.7742 423.3410 428.1152 391.2821 271.6155 -4.7672 423.2205 427.9878 391.2665 272.4643 -4.7757 423.1337 427.9095 391.0820 273.2228 -4.7811 423.0652 427.8463 391.0119 274.0428 -4.7760 422.9627 427.7387 390.8575 274.8608 -4.7618 422.8534 427.6151 390.7149 275.6308 -4.7392 422.6729 427.4121 390.6056 276.4623 -4.7429 422.6230 427.3659 390.4963 277.2203 -4.7701 422.5874 427.3575 390.4340 278.0690 -4.7511 422.5450 427.2961 390.3025 278.8580 -4.7552 422.4225 427.1776 390.1905 279.6495 -4.7459 422.3643 427.1102 390.0795 280.4713 -4.7401 422.2083 426.9484 389.8788 281.2328 -4.7513 422.0987 426.8500 389.8810 282.0850 -4.7377 422.0393 426.7770 389.7704 282.8468 -4.7317 421.9287 426.6604 389.7295 283.6688 -4.7349 421.7729 426.5078 389.6001 284.4908 -4.7427 421.6714 426.4141 389.4745 285.2525 -4.7236 421.6196 426.3433 389.2728 286.1060 -4.7203 421.6006 426.3208 389.2797 286.8675 -4.7315 421.5364 426.2679 389.0953 287.6898 -4.7372 421.3650 426.1023 389.0651 288.4823 -4.7178 421.3366 426.0544 388.8949 289.2745 -4.7300 421.2913 426.0213 388.7064 290.1268 -4.7179 421.1169 425.8348 388.6171 290.8888 -4.7263 421.0753 425.8017 388.6155 291.7115 -4.7076 420.9736 425.6811 388.4645 292.5038 -4.7041 420.8380 425.5421 388.3623 293.2955 -4.7068 420.8017 425.5084 388.3405 294.1478 -4.7054 420.7687 425.4741 388.1429 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