DTA measure 2olom_1 Test Date: 2024228:1336 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1649.02 s Mass = 1383.500 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4168 -4.8068 418.5643 423.3711 421.2427 4.0288 -4.8089 418.6315 423.4404 421.2742 5.6259 -4.8068 418.6755 423.4823 421.2784 7.2383 -4.8055 418.7254 423.5308 421.2656 8.8360 -4.8053 418.7842 423.5895 421.2291 10.4335 -4.8039 418.8308 423.6347 421.1776 12.0610 -4.7994 418.8713 423.6707 421.0867 13.6580 -4.7959 418.9296 423.7255 420.9815 15.2541 -4.7922 418.9745 423.7667 420.8698 16.9711 -4.7883 419.0242 423.8125 420.7332 18.6779 -4.7835 419.0581 423.8416 420.5485 20.2744 -4.7808 419.1102 423.8911 420.3592 21.8705 -4.7748 419.1565 423.9313 420.1756 23.4811 -4.7697 419.1909 423.9606 419.9534 25.0780 -4.7612 419.2317 423.9929 419.7442 26.7053 -4.7550 419.2621 424.0171 419.5070 28.3029 -4.7456 419.2921 424.0377 419.2886 29.9005 -4.7379 419.3283 424.0662 419.0525 31.4973 -4.7323 419.3459 424.0782 418.8032 33.1083 -4.7204 419.3807 424.1011 418.5620 34.7209 -4.7070 419.4111 424.1181 418.3320 36.3334 -4.6971 419.4213 424.1184 418.0704 37.9315 -4.6903 419.4543 424.1446 417.8183 39.5311 -4.6792 419.4477 424.1269 417.5697 41.1284 -4.6704 419.4618 424.1322 417.3323 42.7293 -4.6587 419.4818 424.1406 417.0968 44.3581 -4.6475 419.4875 424.1349 416.8329 45.9569 -4.6372 419.5032 424.1404 416.5893 47.5533 -4.6276 419.5050 424.1326 416.3490 49.1648 -4.6156 419.5136 424.1292 416.1046 50.7600 -4.6058 419.5106 424.1164 415.8757 52.3868 -4.5919 419.5017 424.0936 415.6598 53.9834 -4.5834 419.4943 424.0777 415.4403 55.5825 -4.5718 419.5032 424.0750 415.2207 57.1799 -4.5607 419.4870 424.0477 415.0235 58.7906 -4.5479 419.4835 424.0314 414.7988 60.4083 -4.5355 419.4713 424.0068 414.6082 62.0193 -4.5282 419.4537 423.9818 414.4123 63.6156 -4.5183 419.4344 423.9527 414.2198 65.2116 -4.5078 419.4006 423.9084 414.0332 66.8250 -4.4961 419.3941 423.8902 413.8657 68.6191 -4.4814 419.3848 423.8662 413.6420 70.2411 -4.4747 419.3398 423.8145 413.4639 71.8379 -4.4678 419.3076 423.7754 413.3103 73.4499 -4.4602 419.2998 423.7600 413.1211 75.0623 -4.4457 419.2604 423.7061 412.9487 76.6756 -4.4376 419.2165 423.6541 412.7776 78.2753 -4.4352 419.1908 423.6261 412.5911 79.8736 -4.4255 419.1553 423.5807 412.4177 81.4703 -4.4155 419.1266 423.5421 412.2229 83.0985 -4.4112 419.0924 423.5036 412.0527 84.6966 -4.4016 419.0567 423.4583 411.8646 86.3085 -4.3933 418.9890 423.3823 411.6633 87.9056 -4.3901 418.9351 423.3252 411.4759 89.5030 -4.3815 418.8951 423.2765 411.2933 91.1296 -4.3704 418.8486 423.2189 411.1108 92.7273 -4.3615 418.8075 423.1690 410.8954 94.3383 -4.3510 418.7554 423.1064 410.7011 95.9339 -4.3447 418.7111 423.0557 410.5053 97.5301 -4.3326 418.6606 422.9932 410.3093 99.3376 -4.3175 418.6023 422.9197 410.0852 100.9601 -4.3087 418.5290 422.8376 409.8723 102.5573 -4.2981 418.4806 422.7787 409.6694 104.1718 -4.2896 418.4184 422.7080 409.4917 105.7700 -4.2802 418.3527 422.6329 409.2762 107.3810 -4.2717 418.2828 422.5545 409.0809 108.9924 -4.2624 418.2089 422.4713 408.8965 110.5981 -4.2525 418.1429 422.3954 408.6797 112.1946 -4.2435 418.0738 422.3173 408.4927 113.8053 -4.2363 418.0098 422.2461 408.2886 115.4020 -4.2283 417.9385 422.1668 408.1016 117.0026 -4.2170 417.8533 422.0703 407.8845 118.6315 -4.2078 417.7896 421.9974 407.6930 120.2304 -4.2015 417.6957 421.8971 407.5055 121.8281 -4.1926 417.6220 421.8146 407.2974 123.4238 -4.1865 417.5353 421.7218 407.1195 125.0361 -4.1774 417.4691 421.6465 406.9244 126.6490 -4.1684 417.3779 421.5463 406.7265 128.2615 -4.1632 417.2830 421.4462 406.5142 129.8571 -4.1505 417.2159 421.3664 406.3233 131.4526 -4.1423 417.1168 421.2590 406.1129 133.0638 -4.1354 417.0335 421.1689 405.9215 134.6765 -4.1279 416.9497 421.0776 405.7118 136.2894 -4.1192 416.8504 420.9696 405.4943 137.8849 -4.1116 416.7628 420.8743 405.2924 139.4823 -4.1008 416.6696 420.7704 405.1048 141.0814 -4.0952 416.5670 420.6622 404.9055 142.7081 -4.0860 416.4594 420.5454 404.6797 144.3046 -4.0778 416.3644 420.4422 404.4750 145.9154 -4.0685 416.2683 420.3368 404.2815 147.5115 -4.0585 416.1739 420.2325 404.0702 149.1244 -4.0506 416.0736 420.1242 403.8683 150.7226 -4.0439 415.9753 420.0192 403.6736 152.3500 -4.0317 415.8698 419.9016 403.4805 153.9461 -4.0263 415.7652 419.7915 403.2937 155.5420 -4.0202 415.6607 419.6809 403.0987 157.1535 -4.0105 415.5601 419.5707 402.9138 158.7639 -4.0025 415.4472 419.4497 402.7053 160.3746 -3.9934 415.3454 419.3388 402.5226 161.9719 -3.9860 415.2216 419.2075 402.3312 163.5843 -3.9797 415.1195 419.0992 402.1289 165.1825 -3.9728 415.0172 418.9900 401.9437 166.7963 -3.9659 414.8912 418.8571 401.7567 168.4090 -3.9554 414.7570 418.7124 401.5448 170.0069 -3.9485 414.6469 418.5954 401.3486 171.6194 -3.9385 414.5306 418.4691 401.1536 173.2146 -3.9338 414.4160 418.3498 400.9462 174.8403 -3.9248 414.3144 418.2392 400.7395 176.4358 -3.9187 414.1785 418.0972 400.5394 178.0475 -3.9134 414.0645 417.9778 400.3486 179.6450 -3.9053 413.9431 417.8484 400.1288 181.2459 -3.8967 413.8117 417.7084 399.9341 182.8578 -3.8897 413.7011 417.5908 399.7343 184.4698 -3.8814 413.5586 417.4400 399.5220 186.0670 -3.8760 413.4424 417.3184 399.3326 187.6795 -3.8694 413.3212 417.1906 399.1219 189.2780 -3.8628 413.2007 417.0635 398.9326 190.8894 -3.8563 413.0686 416.9249 398.7360 192.4998 -3.8495 412.9350 416.7845 398.5356 194.0955 -3.8421 412.7950 416.6372 398.3277 195.7065 -3.8353 412.6557 416.4910 398.1558 197.3035 -3.8294 412.5307 416.3601 397.9461 198.9141 -3.8196 412.4155 416.2351 397.7381 200.5234 -3.8125 412.2709 416.0834 397.5420 202.1185 -3.8038 412.1278 415.9315 397.3513 203.7149 -3.7991 412.0049 415.8040 397.1619 205.3260 -3.7910 411.8717 415.6626 396.9435 206.9218 -3.7874 411.7366 415.5239 396.7329 208.5490 -3.7792 411.6015 415.3807 396.5234 210.1459 -3.7725 411.4608 415.2333 396.3173 211.7510 -3.7648 411.3026 415.0674 396.1015 213.3513 -3.7608 411.1753 414.9361 395.8948 214.9494 -3.7529 411.0443 414.7971 395.7029 216.5466 -3.7460 410.9115 414.6575 395.4798 218.1734 -3.7411 410.7617 414.5028 395.2690 219.7709 -3.7351 410.6168 414.3520 395.0559 221.3676 -3.7271 410.4732 414.2003 394.8477 222.9785 -3.7197 410.3331 414.0528 394.6510 224.5758 -3.7125 410.1825 413.8950 394.4297 226.1880 -3.7038 410.0448 413.7485 394.2298 227.7996 -3.6975 409.8923 413.5898 394.0383 229.3969 -3.6906 409.7389 413.4294 393.8346 230.9936 -3.6851 409.6039 413.2890 393.6305 232.6005 -3.6762 409.4481 413.1243 393.4182 234.2118 -3.6666 409.3139 412.9805 393.2094 235.8241 -3.6626 409.1512 412.8138 393.0204 237.4358 -3.6571 409.0020 412.6591 392.8256 239.0326 -3.6488 408.8433 412.4920 392.6193 240.6283 -3.6419 408.7157 412.3577 392.4312 242.2384 -3.6356 408.5438 412.1794 392.2322 243.8645 -3.6308 408.3912 412.0220 392.0486 245.4609 -3.6287 408.2387 411.8673 391.8482 247.0570 -3.6192 408.0918 411.7110 391.6495 248.6689 -3.6134 407.9370 411.5504 391.4598 250.2658 -3.6056 407.7784 411.3840 391.2629 251.8724 -3.6027 407.6296 411.2323 391.0742 253.4901 -3.5981 407.4823 411.0804 390.8728 255.1021 -3.5955 407.3182 410.9137 390.6847 256.6993 -3.5888 407.1600 410.7488 390.4811 258.3093 -3.5832 406.9940 410.5772 390.2777 259.9050 -3.5755 406.8322 410.4077 390.0700 261.5321 -3.5703 406.6794 410.2497 389.8588 263.1448 -3.5657 406.5315 410.0972 389.6652 264.7416 -3.5607 406.3603 409.9210 389.4564 266.3383 -3.5524 406.1995 409.7518 389.2537 267.9480 -3.5450 406.0414 409.5864 389.0302 269.5605 -3.5403 405.8971 409.4373 388.8320 271.1740 -3.5329 405.7283 409.2612 388.6045 272.7619 -3.5275 405.5682 409.0957 388.4042 274.3791 -3.5188 405.4028 408.9216 388.1925 275.9750 -3.5137 405.2442 408.7578 387.9838 277.5861 -3.5076 405.0684 408.5760 387.7754 279.1981 -3.5013 404.9005 408.4017 387.5701 280.8101 -3.4959 404.7470 408.2429 387.3488 282.4071 -3.4899 404.5784 408.0683 387.1616 284.0188 -3.4833 404.4328 407.9161 386.9563 285.6165 -3.4770 404.2575 407.7345 386.7388 287.2145 -3.4703 404.0960 407.5663 386.5376 288.8429 -3.4635 403.9367 407.4002 386.3076 290.4401 -3.4561 403.7774 407.2336 386.1189 292.0376 -3.4499 403.5954 407.0453 385.9139 293.6395 -3.4441 403.4235 406.8676 385.7233 295.2563 -3.4416 403.2496 406.6912 385.5026 296.8541 -3.4325 403.0782 406.5106 385.3074 298.4516 -3.4261 402.9234 406.3495 385.1024 300.0784 -3.4197 402.7378 406.1575 384.8946 301.6750 -3.4128 402.5742 405.9871 384.7111 303.2720 -3.4079 402.3915 405.7994 384.4919 304.8696 -3.4012 402.2403 405.6415 384.3060 306.4810 -3.3964 402.0589 405.4553 384.1075 308.0928 -3.3921 401.9074 405.2994 383.9063 309.6893 -3.3871 401.7263 405.1134 383.7259 311.3010 -3.3792 401.5624 404.9416 383.5468 312.8978 -3.3734 401.3938 404.7672 383.3371 314.5023 -3.3677 401.2176 404.5853 383.1285 316.0983 -3.3618 401.0460 404.4078 382.9385 317.7083 -3.3545 400.8605 404.2150 382.7509 319.3339 -3.3487 400.6943 404.0430 382.5383 320.9311 -3.3417 400.4990 403.8406 382.3386 322.5276 -3.3380 400.3386 403.6766 382.1326 324.1173 -3.3341 400.1752 403.5093 381.9254 325.7453 -3.3271 400.0155 403.3425 381.7135 327.3423 -3.3201 399.8332 403.1533 381.5084 328.9535 -3.3150 399.6465 402.9615 381.2908 330.5493 -3.3133 399.4808 402.7941 381.0813 332.1610 -3.3055 399.3076 402.6131 380.8827 333.7640 -3.3007 399.1237 402.4245 380.6718 335.3764 -3.2924 398.9433 402.2358 380.4698 336.9736 -3.2863 398.7744 402.0607 380.2594 338.5901 -3.2795 398.6087 401.8883 380.0560 340.2025 -3.2758 398.4305 401.7063 379.8636 341.7998 -3.2669 398.2570 401.5239 379.6497 343.3976 -3.2613 398.0703 401.3316 379.4268 345.0138 -3.2562 397.8866 401.1429 379.2401 346.6204 -3.2493 397.7212 400.9705 379.0475 348.2320 -3.2463 397.5340 400.7803 378.8368 349.8286 -3.2364 397.3594 400.5959 378.6332 351.4561 -3.2312 397.1923 400.4235 378.4426 353.0523 -3.2244 396.9996 400.2240 378.2517 354.6295 -3.2208 396.8313 400.0522 378.0560 356.2690 -3.2155 396.6460 399.8615 377.8400 357.8716 -3.2077 396.4642 399.6719 377.6521 359.4843 -3.2020 396.2794 399.4813 377.4577 361.0811 -3.1965 396.0963 399.2927 377.2490 362.6920 -3.1934 395.9186 399.1120 377.0691 364.2983 -3.1896 395.7402 398.9298 376.8433 365.8985 -3.1832 395.5657 398.7489 376.6422 367.4971 -3.1765 395.3812 398.5577 376.4254 369.1234 -3.1731 395.1904 398.3635 376.2171 370.7346 -3.1669 395.0170 398.1839 376.0049 372.3304 -3.1590 394.8463 398.0053 375.7818 373.9249 -3.1543 394.6623 397.8166 375.5712 375.5365 -3.1515 394.4799 397.6314 375.3556 377.1488 -3.1457 394.3050 397.4507 375.1205 378.7608 -3.1420 394.1078 397.2498 374.9107 380.3571 -3.1374 393.9290 397.0664 374.7148 381.9685 -3.1303 393.7416 396.8719 374.5007 383.5664 -3.1233 393.5555 396.6787 374.2794 385.1793 -3.1209 393.3854 396.5063 374.0619 386.7736 -3.1131 393.1814 396.2945 373.8516 388.3865 -3.1095 393.0072 396.1168 373.6406 389.9971 -3.1040 392.8344 395.9384 373.4305 391.5938 -3.0973 392.6442 395.7414 373.2169 393.1904 -3.0914 392.4495 395.5409 373.0152 394.8031 -3.0869 392.2612 395.3481 372.7994 396.4038 -3.0816 392.0803 395.1620 372.6020 398.0163 -3.0738 391.9006 394.9744 372.3968 399.6141 -3.0682 391.7197 394.7879 372.1779 401.2106 -3.0612 391.5236 394.5848 371.9678 402.8374 -3.0548 391.3256 394.3805 371.7634 404.4344 -3.0490 391.1650 394.2141 371.5717 406.0224 -3.0453 390.9725 394.0178 371.3580 407.6373 -3.0420 390.7700 393.8121 371.1333 409.2498 -3.0342 390.5802 393.6144 370.9281 410.8468 -3.0309 390.3997 393.4306 370.7303 412.4560 -3.0264 390.2175 393.2439 370.5230 414.0523 -3.0191 390.0402 393.0592 370.3271 415.6681 -3.0144 389.8477 392.8621 370.1371 417.2621 -3.0103 389.6631 392.6734 369.9336 418.8736 -3.0047 389.4764 392.4810 369.7252 420.4710 -3.0010 389.2668 392.2678 369.5081 422.0825 -2.9945 389.0957 392.0902 369.3383 423.6923 -2.9905 388.8956 391.8861 369.1199 425.2866 -2.9850 388.7029 391.6879 368.9228 426.8829 -2.9794 388.5220 391.5014 368.7307 428.4929 -2.9745 388.3396 391.3141 368.5454 430.1039 -2.9683 388.1526 391.1209 368.3301 431.7146 -2.9636 387.9538 390.9174 368.1368 433.3109 -2.9593 387.7709 390.7303 367.9602 434.9065 -2.9554 387.5893 390.5447 367.7706 436.5215 -2.9529 387.3954 390.3483 367.5685 438.1373 -2.9442 387.2042 390.1484 367.3589 439.7324 -2.9415 387.0107 389.9522 367.1688 441.3439 -2.9405 386.8243 389.7649 366.9654 442.9429 -2.9353 386.6293 389.5646 366.7536 444.5380 -2.9326 386.4568 389.3894 366.5565 446.1488 -2.9256 386.2584 389.1840 366.3499 447.7605 -2.9188 386.0520 388.9708 366.1602 449.3570 -2.9155 385.8766 388.7921 365.9503 450.9671 -2.9107 385.6968 388.6075 365.7438 452.5633 -2.9057 385.5018 388.4074 365.5328 454.1730 -2.9017 385.3247 388.2265 365.3341 455.7820 -2.8984 385.1078 388.0062 365.1180 457.3930 -2.8932 384.9327 387.8259 364.9183 458.9890 -2.8872 384.7229 387.6100 364.6996 460.5863 -2.8831 384.5365 387.4195 364.4896 462.2121 -2.8762 384.3586 387.2348 364.2863 463.8069 -2.8693 384.1579 387.0272 364.0932 465.4180 -2.8632 383.9818 386.8450 363.8773 467.0816 -2.8614 383.7689 386.6303 363.6756 468.8236 -2.8552 383.5755 386.4307 363.4617 470.4351 -2.8506 383.3779 386.2284 363.2509 472.0309 -2.8447 383.1890 386.0337 363.0562 473.6410 -2.8412 382.9984 385.8396 362.8475 475.2374 -2.8334 382.8044 385.6379 362.6600 476.8476 -2.8266 382.6050 385.4316 362.4493 478.4574 -2.8248 382.4238 385.2485 362.2444 480.0545 -2.8200 382.2317 385.0518 362.0506 481.6641 -2.8142 382.0408 384.8550 361.8563 483.2604 -2.8102 381.8661 384.6763 361.6653 484.8879 -2.8051 381.6648 384.4699 361.4618 486.4845 -2.7991 381.4706 384.2696 361.2577 488.0961 -2.7938 381.2763 384.0701 361.0491 489.6916 -2.7907 381.0670 383.8578 360.8509 491.2859 -2.7840 380.8935 383.6775 360.6428 492.9111 -2.7830 380.7028 383.4858 360.4358 494.5218 -2.7776 380.5070 383.2845 360.2213 496.1175 -2.7708 380.3208 383.0915 360.0207 497.7904 -2.7691 380.1201 382.8892 359.7996 499.5266 -2.7634 379.9195 382.6829 359.5651 501.1385 -2.7598 379.7236 382.4834 359.3476 502.7489 -2.7525 379.5088 382.2613 359.1480 504.3430 -2.7474 379.3280 382.0754 358.9338 505.9389 -2.7396 379.1463 381.8859 358.7210 507.5474 -2.7332 378.9517 381.6848 358.5061 509.1593 -2.7278 378.7543 381.4820 358.2903 510.7704 -2.7231 378.5778 381.3009 358.0821 512.3648 -2.7189 378.3905 381.1093 357.8703 513.9773 -2.7165 378.1796 380.8961 357.6515 515.5736 -2.7123 378.0001 380.7124 357.4329 517.2011 -2.7081 377.7989 380.5070 357.2380 518.7965 -2.6996 377.6032 380.3028 357.0265 520.3920 -2.6948 377.4118 380.1065 356.8080 522.0031 -2.6910 377.2184 379.9095 356.6084 523.6128 -2.6864 377.0151 379.7015 356.3825 525.2218 -2.6831 376.8151 379.4982 356.1855 526.8189 -2.6802 376.6226 379.3027 355.9863 528.5078 -2.6750 376.4251 379.1000 355.7692 530.2310 -2.6697 376.2263 378.8960 355.5354 531.8270 -2.6638 376.0371 378.7009 355.3184 533.4545 -2.6587 375.8425 378.5011 355.1162 535.0504 -2.6537 375.6410 378.2948 354.9157 536.6598 -2.6484 375.4520 378.1004 354.7231 538.2560 -2.6450 375.2612 377.9063 354.5099 539.8648 -2.6401 375.0602 377.7003 354.2983 541.4748 -2.6363 374.8573 377.4936 354.0889 543.0739 -2.6317 374.6666 377.2983 353.9103 544.6848 -2.6306 374.4835 377.1140 353.7118 546.2808 -2.6238 374.2910 376.9148 353.4940 547.8916 -2.6178 374.1037 376.7215 353.2841 549.5040 -2.6157 373.8856 376.5013 353.0915 551.1010 -2.6101 373.6964 376.3065 352.8843 552.7100 -2.6023 373.5052 376.1075 352.6638 554.3071 -2.5991 373.2951 375.8941 352.4709 555.9189 -2.5961 373.1141 375.7102 352.2624 557.5283 -2.5929 372.9202 375.5131 352.0670 559.1240 -2.5899 372.7377 375.3275 351.8819 560.7339 -2.5829 372.5206 375.1035 351.6725 562.3288 -2.5787 372.3296 374.9083 351.4679 563.9408 -2.5749 372.1365 374.7114 351.2666 565.5508 -2.5702 371.9426 374.5128 351.0740 567.1456 -2.5665 371.7394 374.3059 350.8896 568.7543 -2.5601 371.5562 374.1163 350.6858 570.3529 -2.5540 371.3586 373.9126 350.4782 571.9489 -2.5499 371.1664 373.7163 350.2768 573.5759 -2.5443 370.9596 373.5039 350.0648 575.1723 -2.5421 370.7781 373.3202 349.8478 576.7810 -2.5354 370.5718 373.1073 349.6544 578.3770 -2.5314 370.3874 372.9188 349.4501 579.9729 -2.5268 370.1802 372.7071 349.2366 581.5996 -2.5244 369.9868 372.5112 349.0275 583.1958 -2.5216 369.7905 372.3121 348.8289 584.7936 -2.5183 369.5989 372.1172 348.6114 586.3915 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297.4953 986.6026 -1.4737 320.1561 321.6298 297.3012 988.2005 -1.4707 319.9594 321.4301 297.0820 989.9735 -1.4678 319.7335 321.2013 296.8576 991.6181 -1.4598 319.5423 321.0020 296.6462 993.2288 -1.4542 319.3653 320.8195 296.4344 994.8245 -1.4530 319.1471 320.6001 296.2468 996.4329 -1.4493 318.9557 320.4050 296.0436 998.0555 -1.4473 318.7514 320.1987 295.8483 999.6519 -1.4438 318.5589 320.0027 295.6389 1001.2504 -1.4393 318.3472 319.7864 295.4408 1002.8453 -1.4362 318.1454 319.5817 295.2417 1004.4538 -1.4322 317.9507 319.3828 295.0236 1006.0795 -1.4284 317.7580 319.1864 294.8172 1007.6759 -1.4239 317.5562 318.9801 294.6132 1009.2708 -1.4237 317.3464 318.7701 294.4345 1010.8809 -1.4199 317.1597 318.5795 294.2260 1012.4903 -1.4142 316.9627 318.3768 294.0221 1014.0993 -1.4139 316.7626 318.1765 293.8356 1015.6950 -1.4096 316.5650 317.9746 293.6362 1017.3041 -1.4068 316.3646 317.7714 293.4488 1018.8994 -1.4017 316.1652 317.5669 293.2357 1020.5091 -1.3973 315.9696 317.3669 293.0222 1022.1184 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