DTA measure 1gyors_olom Date: 2024312:1452 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.00 s Mass = 100.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1973 -1.4640 212.6851 214.1491 246.4325 1.9865 -1.4623 212.7794 214.2416 246.4245 2.8068 -1.4596 212.9103 214.3699 246.4024 3.5953 -1.4553 213.0512 214.5065 246.3704 4.3850 -1.4534 213.1600 214.6134 246.3634 5.2330 -1.4503 213.3002 214.7505 246.3589 5.9915 -1.4495 213.4279 214.8774 246.3512 6.8103 -1.4513 213.5373 214.9886 246.3744 7.6298 -1.4415 213.6778 215.1193 246.3831 8.3880 -1.4396 213.7902 215.2298 246.4264 9.2370 -1.4380 213.9039 215.3419 246.4527 10.0255 -1.4397 214.0375 215.4772 246.4678 10.8150 -1.4390 214.1483 215.5873 246.4950 11.6373 -1.4371 214.2801 215.7172 246.5310 12.4265 -1.4356 214.4210 215.8566 246.5926 13.2470 -1.4334 214.5435 215.9769 246.6434 14.0353 -1.4291 214.6535 216.0826 246.7159 14.8240 -1.4272 214.7869 216.2141 246.7729 15.6735 -1.4274 214.9221 216.3495 246.8542 16.4325 -1.4212 215.0361 216.4574 246.9367 17.2518 -1.4223 215.1429 216.5652 247.0193 18.0713 -1.4203 215.2792 216.6994 247.1466 18.8300 -1.4184 215.3978 216.8162 247.2563 19.6990 -1.4151 215.5105 216.9257 247.3680 20.4640 -1.4142 215.6349 217.0491 247.4710 21.2828 -1.4153 215.7492 217.1645 247.5991 22.0710 -1.4129 215.8619 217.2748 247.7298 22.8600 -1.4125 216.0077 217.4202 247.8698 23.7085 -1.4117 216.1284 217.5400 248.0168 24.4670 -1.4094 216.2460 217.6554 248.1495 25.2858 -1.4090 216.3526 217.7617 248.3129 26.1043 -1.4107 216.4850 217.8957 248.4956 26.8630 -1.4110 216.6070 218.0179 248.6428 27.7115 -1.4129 216.7486 218.1615 248.8233 28.5005 -1.4105 216.8448 218.2553 249.0115 29.2900 -1.4090 216.9776 218.3866 249.1965 30.1085 -1.4096 217.1015 218.5111 249.3582 30.8970 -1.4074 217.2157 218.6231 249.5430 31.7180 -1.4060 217.3240 218.7300 249.7524 32.5065 -1.4063 217.4505 218.8568 249.9132 33.2950 -1.4091 217.5636 218.9727 250.0740 34.1440 -1.4094 217.6965 219.1059 250.2972 34.9023 -1.4104 217.8130 219.2234 250.4961 35.7210 -1.4103 217.9540 219.3643 250.7054 36.5398 -1.4130 218.0697 219.4827 250.8995 37.2980 -1.4117 218.1822 219.5939 251.0557 38.1485 -1.4134 218.3209 219.7343 251.2778 38.9375 -1.4130 218.4313 219.8443 251.4620 39.7270 -1.4145 218.5479 219.9624 251.6418 40.5460 -1.4148 218.7028 220.1176 251.8298 41.3353 -1.4155 218.8041 220.2196 252.0272 42.1538 -1.4157 218.9239 220.3396 252.2186 42.9420 -1.4152 219.0629 220.4781 252.3807 43.7310 -1.4198 219.1837 220.6035 252.5451 44.5805 -1.4227 219.2919 220.7146 252.7355 45.3395 -1.4190 219.4132 220.8322 252.9260 46.1598 -1.4231 219.5380 220.9611 253.0954 46.9790 -1.4266 219.6699 221.0966 253.2431 47.7380 -1.4267 219.7799 221.2066 253.4105 48.5865 -1.4278 219.8959 221.3237 253.5888 49.3760 -1.4294 220.0390 221.4685 253.7494 50.1660 -1.4320 220.1713 221.6032 253.8946 51.0145 -1.4365 220.2883 221.7248 254.0818 51.7730 -1.4380 220.4061 221.8441 254.2167 52.5918 -1.4388 220.5364 221.9752 254.3674 53.4110 -1.4409 220.6566 222.0974 254.5270 54.1700 -1.4405 220.7736 222.2141 254.6648 55.0185 -1.4426 220.9030 222.3457 254.8079 55.8080 -1.4468 221.0236 222.4705 254.9262 56.5978 -1.4473 221.1461 222.5934 255.0666 57.4173 -1.4479 221.2711 222.7189 255.2097 58.2063 -1.4481 221.4090 222.8571 255.3480 59.0260 -1.4444 221.5179 222.9623 255.4662 59.8145 -1.4476 221.6437 223.0913 255.6082 60.6030 -1.4480 221.7741 223.2221 255.7512 61.4528 -1.4514 221.9049 223.3563 255.8937 62.2115 -1.4535 222.0091 223.4626 256.0069 63.0310 -1.4525 222.1511 223.6035 256.1250 63.8503 -1.4532 222.2873 223.7405 256.2485 64.6393 -1.4532 222.4071 223.8603 256.3722 65.4578 -1.4566 222.5349 223.9915 256.5012 66.2463 -1.4562 222.6458 224.1020 256.6249 67.0350 -1.4561 222.7690 224.2251 256.7429 67.8838 -1.4598 222.9075 224.3673 256.8744 68.6420 -1.4622 223.0040 224.4662 256.9854 69.4608 -1.4610 223.1454 224.6064 257.1089 70.2800 -1.4628 223.2695 224.7323 257.2178 71.0390 -1.4725 223.3908 224.8634 257.3351 71.8885 -1.4720 223.5329 225.0049 257.4510 72.6775 -1.4712 223.6501 225.1213 257.5619 73.4680 -1.4715 223.7673 225.2388 257.6640 74.2878 -1.4722 223.8832 225.3554 257.8066 75.0770 -1.4721 224.0020 225.4741 257.9047 75.8968 -1.4724 224.1452 225.6176 258.0108 76.7153 -1.4783 224.2982 225.7765 258.1389 77.4740 -1.4815 224.4100 225.8915 258.2524 78.3225 -1.4810 224.5228 226.0038 258.3346 79.1110 -1.4815 224.6526 226.1342 258.4474 79.9000 -1.4800 224.7849 226.2649 258.5525 80.7183 -1.4828 224.8935 226.3763 258.6660 81.5070 -1.4808 225.0094 226.4902 258.7690 82.3253 -1.4826 225.1581 226.6407 258.8790 83.1138 -1.4817 225.2725 226.7542 258.9621 83.9020 -1.4838 225.4044 226.8882 259.0658 84.7510 -1.4880 225.5254 227.0134 259.1938 85.5093 -1.4882 225.6418 227.1300 259.3064 86.3280 -1.4899 225.7659 227.2559 259.4073 87.1468 -1.4925 225.8854 227.3779 259.5177 87.9050 -1.4933 226.0147 227.5080 259.6219 88.7540 -1.4918 226.1403 227.6321 259.7464 89.5425 -1.4943 226.2687 227.7631 259.8651 90.3310 -1.4953 226.3937 227.8890 259.9608 91.1600 -1.4970 226.5324 228.0294 260.0978 91.9290 -1.4964 226.6435 228.1399 260.2101 92.7778 -1.4972 226.7777 228.2749 260.3359 93.5360 -1.5005 226.8952 228.3958 260.4422 94.3560 -1.5034 227.0251 228.5286 260.5563 95.1440 -1.5037 227.1372 228.6409 260.6703 95.9330 -1.5022 227.2572 228.7594 260.8007 96.7825 -1.5053 227.4175 228.9228 260.9254 97.5410 -1.5041 227.5146 229.0187 261.0178 98.3598 -1.5022 227.6520 229.1542 261.1472 99.1783 -1.5044 227.7720 229.2764 261.2991 99.9370 -1.5078 227.8956 229.4034 261.4006 100.7855 -1.5086 228.0304 229.5391 261.5148 101.5473 -1.5110 228.1391 229.6502 261.6502 102.3708 -1.5148 228.2711 229.7858 261.7967 103.1893 -1.5139 228.3907 229.9047 261.9266 103.9480 -1.5146 228.5198 230.0344 262.0419 104.7965 -1.5141 228.6502 230.1643 262.1978 105.5850 -1.5133 228.7757 230.2890 262.3251 106.3758 -1.5169 228.8939 230.4107 262.4548 107.1953 -1.5201 229.0232 230.5433 262.5740 107.9548 -1.5231 229.1536 230.6767 262.6933 108.8040 -1.5245 229.2665 230.7910 262.8494 109.5930 -1.5272 229.3938 230.9211 262.9964 110.3820 -1.5302 229.5290 231.0592 263.1302 111.2008 -1.5315 229.6594 231.1909 263.2756 112.0195 -1.5311 229.7998 231.3309 263.4254 112.8080 -1.5348 229.9176 231.4524 263.5662 113.6570 -1.5343 230.0326 231.5669 263.7289 114.4153 -1.5344 230.1467 231.6810 263.8717 115.2340 -1.5391 230.2816 231.8207 263.9877 116.0528 -1.5420 230.4168 231.9587 264.1297 116.8110 -1.5420 230.5262 232.0682 264.2808 117.6595 -1.5436 230.6488 232.1925 264.4351 118.4483 -1.5453 230.7807 232.3260 264.5672 119.2370 -1.5463 230.9191 232.4654 264.7181 120.0553 -1.5465 231.0490 232.5955 264.8613 120.8440 -1.5484 231.1650 232.7134 264.9925 121.6628 -1.5543 231.2789 232.8332 265.1444 122.4813 -1.5537 231.4257 232.9794 265.2896 123.2400 -1.5546 231.5455 233.1001 265.4513 124.0885 -1.5615 231.6736 233.2351 265.6021 124.8773 -1.5625 231.7703 233.3328 265.7233 125.6660 -1.5628 231.9017 233.4644 265.8412 126.4843 -1.5647 232.0391 233.6037 266.0105 127.2730 -1.5649 232.1886 233.7535 266.1575 128.0918 -1.5654 232.3108 233.8762 266.3034 128.8800 -1.5659 232.4095 233.9754 266.4524 129.6690 -1.5704 232.5409 234.1113 266.5838 130.5175 -1.5721 232.6656 234.2377 266.7382 131.2760 -1.5727 232.8020 234.3747 266.8672 132.0948 -1.5746 232.9171 234.4917 267.0089 132.9148 -1.5795 233.0501 234.6296 267.1463 133.6740 -1.5771 233.1715 234.7486 267.2755 134.5220 -1.5806 233.3353 234.9159 267.4167 135.3105 -1.5855 233.4483 235.0338 267.5466 136.0990 -1.5844 233.5703 235.1547 267.6887 136.9178 -1.5893 233.6899 235.2792 267.8156 137.7065 -1.5919 233.8241 235.4160 267.9311 138.5260 -1.5944 233.9483 235.5427 268.0893 139.3145 -1.5935 234.0793 235.6728 268.2140 140.1030 -1.5948 234.1956 235.7905 268.3393 140.9530 -1.5993 234.3313 235.9307 268.4612 141.7113 -1.6005 234.4593 236.0598 268.5591 142.5298 -1.5991 234.5756 236.1747 268.6730 143.3485 -1.6011 234.7053 236.3064 268.7869 144.1375 -1.6054 234.8327 236.4382 268.9055 144.9578 -1.6086 234.9731 236.5817 269.0496 145.7470 -1.6100 235.0767 236.6867 269.1679 146.5390 -1.6130 235.2132 236.8262 269.2724 147.3875 -1.6134 235.3593 236.9727 269.4045 148.1460 -1.6133 235.4776 237.0909 269.5014 148.9648 -1.6143 235.5885 237.2028 269.6251 149.7833 -1.6155 235.7144 237.3299 269.7423 150.5420 -1.6173 235.8455 237.4628 269.8538 151.3905 -1.6186 235.9875 237.6062 269.9500 152.1800 -1.6205 236.1104 237.7309 270.0919 152.9700 -1.6227 236.2258 237.8485 270.2239 153.7883 -1.6208 236.3633 237.9841 270.3400 154.5770 -1.6224 236.5003 238.1227 270.4484 155.3968 -1.6252 236.6230 238.2482 270.5736 156.1855 -1.6281 236.7661 238.3942 270.7047 156.9750 -1.6297 236.8797 238.5095 270.8329 157.8253 -1.6324 237.0102 238.6426 270.9546 158.5840 -1.6346 237.1315 238.7660 271.0750 159.4028 -1.6366 237.2824 238.9190 271.2099 160.2218 -1.6422 237.3980 239.0401 271.3376 160.9803 -1.6434 237.5177 239.1611 271.4483 161.8290 -1.6435 237.6565 239.3000 271.5958 162.6543 -1.6477 237.7927 239.4404 271.7244 163.6155 -1.6526 237.9468 239.5994 271.8823 164.4040 -1.6575 238.0652 239.7227 271.9906 165.2538 -1.6610 238.1992 239.8602 272.1269 166.0123 -1.6638 238.3224 239.9862 272.2568 166.8310 -1.6689 238.4521 240.1210 272.3817 167.6510 -1.6708 238.5691 240.2399 272.5211 168.4100 -1.6714 238.6908 240.3622 272.6496 169.2588 -1.6703 238.8436 240.5140 272.7915 170.0480 -1.6717 238.9665 240.6383 272.9286 170.8380 -1.6739 239.0835 240.7574 273.0416 171.6563 -1.6740 239.2197 240.8937 273.1834 172.4455 -1.6719 239.3433 241.0152 273.3131 173.2658 -1.6761 239.4748 241.1509 273.4495 174.0545 -1.6801 239.5956 241.2758 273.5747 174.8440 -1.6813 239.7259 241.4072 273.6963 175.6945 -1.6844 239.8608 241.5452 273.8305 176.4530 -1.6819 240.0012 241.6831 273.9570 177.2718 -1.6865 240.1219 241.8084 274.0908 178.0910 -1.6874 240.2466 241.9341 274.2370 178.8500 -1.6877 240.3714 242.0592 274.3610 179.6985 -1.6834 240.4953 242.1787 274.5146 180.4875 -1.6785 240.6361 242.3146 274.6322 181.2770 -1.6820 240.7779 242.4599 274.7441 182.1255 -1.6853 240.8874 242.5726 274.8854 182.8840 -1.6879 241.0150 242.7029 275.0019 183.7220 -1.6922 241.1451 242.8373 275.1553 184.5100 -1.6917 241.2886 242.9803 275.2767 185.2985 -1.6931 241.4122 243.1053 275.4063 186.1170 -1.6929 241.5367 243.2296 275.5485 186.9055 -1.6952 241.6622 243.3573 275.6768 187.7260 -1.6996 241.7849 243.4844 275.8143 188.5148 -1.7002 241.9122 243.6124 275.9403 189.3040 -1.7032 242.0398 243.7430 276.0711 190.1545 -1.7051 242.1635 243.8686 276.1929 190.9138 -1.7045 242.3141 244.0186 276.3244 191.7350 -1.7099 242.4575 244.1674 276.4671 192.5545 -1.7080 242.5776 244.2855 276.6094 193.3130 -1.7119 242.6793 244.3912 276.7225 194.1718 -1.7126 242.8381 244.5506 276.8612 194.9313 -1.7136 242.9634 244.6769 276.9905 195.7498 -1.7165 243.0909 244.8073 277.1240 196.5690 -1.7161 243.2184 244.9345 277.2776 197.3280 -1.7188 243.3430 245.0618 277.3911 198.1778 -1.7207 243.4807 245.2013 277.5372 198.9670 -1.7237 243.6132 245.3369 277.6798 199.7570 -1.7276 243.7448 245.4724 277.8284 200.5760 -1.7266 243.8641 245.5907 277.9556 201.3653 -1.7298 244.0009 245.7307 278.1087 202.1848 -1.7309 244.1417 245.8726 278.2593 202.9733 -1.7340 244.2507 245.9848 278.3846 203.7630 -1.7370 244.3880 246.1250 278.5305 204.6123 -1.7373 244.5186 246.2559 278.6944 205.3710 -1.7394 244.6506 246.3900 278.8319 206.1898 -1.7414 244.7900 246.5314 278.9802 207.0098 -1.7440 244.9233 246.6674 279.1225 207.7690 -1.7447 245.0447 246.7894 279.2555 208.6175 -1.7463 245.1817 246.9281 279.4080 209.4060 -1.7482 245.2904 247.0386 279.5507 210.1948 -1.7504 245.4191 247.1694 279.6953 211.0140 -1.7521 245.5618 247.3139 279.8426 211.8028 -1.7547 245.6887 247.4434 280.0030 212.6220 -1.7580 245.8356 247.5936 280.1533 213.4108 -1.7617 245.9611 247.7228 280.2637 214.1990 -1.7630 246.0779 247.8409 280.3963 215.0488 -1.7684 246.2338 248.0022 280.5393 215.8075 -1.7709 246.3557 248.1266 280.6681 216.6280 -1.7736 246.4810 248.2546 280.8206 217.4468 -1.7799 246.6245 248.4044 280.9638 218.2050 -1.7826 246.7614 248.5440 281.1052 219.0553 -1.7819 246.8909 248.6728 281.2217 219.8448 -1.7855 247.0057 248.7913 281.3616 220.6340 -1.7860 247.1264 248.9124 281.4732 221.4565 -1.7899 247.2561 249.0460 281.6095 222.2453 -1.7920 247.3946 249.1866 281.7500 223.0638 -1.7964 247.5404 249.3367 281.8830 223.8520 -1.7997 247.6589 249.4586 281.9972 224.6410 -1.8011 247.7989 249.6000 282.1330 225.4895 -1.8016 247.9343 249.7359 282.2681 226.2483 -1.8020 248.0408 249.8428 282.3751 227.0678 -1.8079 248.1593 249.9672 282.5063 227.8878 -1.8129 248.3094 250.1223 282.6156 228.6470 -1.8141 248.4432 250.2573 282.7526 229.4965 -1.8160 248.5967 250.4127 282.8850 230.2855 -1.8174 248.7259 250.5432 283.0067 231.0750 -1.8199 248.8483 250.6682 283.1102 231.8953 -1.8225 248.9922 250.8147 283.2446 232.6855 -1.8239 249.0919 250.9159 283.3636 233.5068 -1.8240 249.2210 251.0450 283.4874 234.3013 -1.8266 249.3665 251.1931 283.6133 235.1133 -1.8321 249.5081 251.3402 283.7339 235.9023 -1.8341 249.6257 251.4598 283.8392 236.6920 -1.8300 249.7416 251.5716 283.9520 237.5418 -1.8343 249.8928 251.7271 284.0813 238.3010 -1.8382 250.0347 251.8729 284.1933 239.1220 -1.8411 250.1490 251.9901 284.3130 239.9420 -1.8408 250.2734 252.1142 284.4331 240.7010 -1.8461 250.4161 252.2622 284.5632 241.5518 -1.8486 250.5545 252.4031 284.7047 242.3408 -1.8468 250.6972 252.5441 284.8330 243.1300 -1.8502 250.8271 252.6773 284.9437 243.9790 -1.8505 250.9501 252.8006 285.0797 244.7373 -1.8526 251.0918 252.9444 285.1829 245.5590 -1.8552 251.2468 253.1020 285.3313 246.3775 -1.8546 251.3576 253.2122 285.4363 247.1360 -1.8577 251.4712 253.3289 285.5685 247.9848 -1.8585 251.6176 253.4761 285.7084 248.7733 -1.8559 251.7459 253.6017 285.8233 249.5620 -1.8591 251.8606 253.7197 285.9499 250.3803 -1.8612 252.0188 253.8800 286.1124 251.1690 -1.8661 252.1471 254.0132 286.2451 251.9878 -1.8697 252.2785 254.1482 286.3426 252.7760 -1.8708 252.4136 254.2844 286.5072 253.5650 -1.8722 252.5402 254.4124 286.6372 254.4135 -1.8742 252.6886 254.5629 286.7613 255.1720 -1.8798 252.8157 254.6955 286.8977 255.9908 -1.8832 252.9466 254.8298 287.0337 256.8093 -1.8829 253.0763 254.9591 287.1882 257.5680 -1.8818 253.2080 255.0898 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