DTA measure 1lasssu_olom Date: 2024312:165 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.67 s Mass = 100.000 mg data_number = 1587 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1618 -1.7448 198.4200 200.1648 245.7490 1.9500 -1.7407 198.5996 200.3403 245.7472 2.7390 -1.7377 198.7831 200.5208 245.7372 3.5875 -1.7329 198.9863 200.7192 245.7328 4.3460 -1.7274 199.1388 200.8662 245.7333 5.1648 -1.7242 199.3264 201.0506 245.7464 5.9848 -1.7188 199.5404 201.2593 245.7598 6.7440 -1.7168 199.7144 201.4313 245.7814 7.5925 -1.7140 199.9215 201.6355 245.8027 8.3853 -1.7107 200.0854 201.7961 245.8554 9.1760 -1.7063 200.2559 201.9621 245.9005 9.9943 -1.7036 200.4440 202.1476 245.9267 10.7830 -1.6987 200.6313 202.3300 245.9672 11.6018 -1.6958 200.8247 202.5205 246.0208 12.4203 -1.6929 201.0416 202.7345 246.0831 13.1803 -1.6937 201.1973 202.8910 246.1320 14.0325 -1.6894 201.3800 203.0694 246.1912 14.7910 -1.6878 201.5592 203.2470 246.2888 15.6098 -1.6840 201.7320 203.4160 246.3705 16.4283 -1.6836 201.9132 203.5968 246.4766 17.1873 -1.6818 202.0945 203.7763 246.5528 18.0373 -1.6774 202.2818 203.9591 246.6720 18.8265 -1.6738 202.4658 204.1397 246.7869 19.6163 -1.6720 202.6319 204.3039 246.8501 20.4388 -1.6722 202.8069 204.4791 246.9698 21.2273 -1.6692 202.9837 204.6529 247.1041 22.0460 -1.6708 203.1787 204.8496 247.2303 22.8360 -1.6671 203.3497 205.0168 247.3583 23.6250 -1.6667 203.5132 205.1799 247.4556 24.4740 -1.6642 203.7255 205.3897 247.6014 25.2323 -1.6594 203.8931 205.5525 247.7194 26.0508 -1.6535 204.0742 205.7277 247.8557 26.8695 -1.6489 204.2570 205.9059 248.0434 27.6280 -1.6529 204.4173 206.0701 248.1760 28.4940 -1.6503 204.5868 206.2371 248.2979 29.2535 -1.6496 204.7489 206.3985 248.4366 30.0738 -1.6446 204.9500 206.5946 248.5969 30.8620 -1.6411 205.1196 206.7607 248.7358 31.6510 -1.6414 205.2888 206.9302 248.8780 32.4995 -1.6355 205.4793 207.1148 249.0592 33.2590 -1.6347 205.6461 207.2808 249.2037 34.0788 -1.6336 205.8267 207.4603 249.3744 34.8973 -1.6337 206.0221 207.6557 249.5292 35.6560 -1.6334 206.1775 207.8109 249.6652 36.5045 -1.6321 206.3526 207.9848 249.8285 37.2940 -1.6294 206.5287 208.1580 249.9850 38.0840 -1.6311 206.6942 208.3252 250.1256 38.9108 -1.6299 206.8853 208.5152 250.2854 39.6710 -1.6279 207.0517 208.6796 250.4458 40.5195 -1.6303 207.2155 208.8458 250.6055 41.3080 -1.6308 207.3865 209.0173 250.7376 42.0968 -1.6283 207.5763 209.2046 250.8926 42.9150 -1.6275 207.7542 209.3817 251.0343 43.7033 -1.6263 207.9083 209.5346 251.1810 44.5220 -1.6263 208.0638 209.6901 251.3506 45.3105 -1.6243 208.2445 209.8688 251.4933 46.0990 -1.6230 208.4283 210.0513 251.6161 46.9480 -1.6240 208.6143 210.2382 251.7773 47.7365 -1.6226 208.7859 210.4085 251.9151 48.5263 -1.6225 208.9578 210.5803 252.0432 49.3498 -1.6205 209.1428 210.7633 252.1796 50.1383 -1.6159 209.2940 210.9099 252.3120 50.9570 -1.6221 209.4776 211.0997 252.4491 51.7453 -1.6214 209.6574 211.2788 252.5764 52.5340 -1.6204 209.8224 211.4428 252.6854 53.3835 -1.6201 209.9873 211.6074 252.8032 54.1425 -1.6201 210.1609 211.7810 252.9364 54.9628 -1.6184 210.3403 211.9586 253.0780 55.7828 -1.6172 210.4869 212.1041 253.1679 56.5430 -1.6178 210.6488 212.2666 253.2745 57.3915 -1.6157 210.8354 212.4512 253.3876 58.1800 -1.6128 211.0018 212.6145 253.5022 58.9690 -1.6106 211.1816 212.7922 253.5969 59.7873 -1.6104 211.3831 212.9935 253.7225 60.5760 -1.6102 211.5311 213.1412 253.8180 61.3965 -1.6069 211.6718 213.2787 253.9028 62.1880 -1.6092 211.8375 213.4466 254.0049 62.9770 -1.6117 212.0226 213.6343 254.0981 63.8255 -1.6110 212.2051 213.8161 254.2213 64.5840 -1.6103 212.3710 213.9813 254.2980 65.4028 -1.6084 212.5441 214.1526 254.3882 66.1938 -1.6090 212.6942 214.3032 254.4660 66.9840 -1.6089 212.8476 214.4565 254.5480 67.8345 -1.6076 213.0294 214.6370 254.6414 68.5930 -1.6078 213.1835 214.7913 254.7081 69.4110 -1.6100 213.3585 214.9685 254.7970 70.2300 -1.6057 213.5194 215.1252 254.8965 71.0183 -1.6046 213.6679 215.2725 254.9513 71.8370 -1.6058 213.8476 215.4534 255.0335 72.6258 -1.6049 214.0151 215.6200 255.1168 73.4160 -1.6010 214.1943 215.7954 255.1906 74.2650 -1.6099 214.3471 215.9570 255.2697 75.0248 -1.6059 214.5118 216.1176 255.3757 75.8460 -1.6084 214.6677 216.2762 255.4449 76.6355 -1.6053 214.8322 216.4375 255.5372 77.4248 -1.6072 215.0072 216.6144 255.6084 78.2738 -1.6072 215.1757 216.7829 255.7105 79.0323 -1.6071 215.3321 216.9392 255.7910 79.8508 -1.6050 215.4977 217.1028 255.8915 80.6693 -1.6011 215.6571 217.2581 255.9792 81.4280 -1.6023 215.7979 217.4002 256.0523 82.2770 -1.6052 215.9892 217.5944 256.1406 83.0670 -1.6064 216.1485 217.7549 256.2365 83.8565 -1.6006 216.3072 217.9078 256.3092 84.6788 -1.5995 216.4615 218.0610 256.3977 85.4380 -1.5980 216.6170 218.2150 256.5022 86.2865 -1.5975 216.7904 218.3879 256.6088 87.0750 -1.5979 216.9453 218.5432 256.7060 87.8640 -1.5942 217.1026 218.6967 256.8124 88.6823 -1.5923 217.2674 218.8597 256.8933 89.4423 -1.5913 217.4153 219.0066 256.9818 90.2985 -1.5918 217.5779 219.1697 257.1032 91.0870 -1.5920 217.7518 219.3438 257.1920 91.8763 -1.5856 217.9209 219.5064 257.2849 92.6960 -1.5854 218.0738 219.6591 257.3931 93.4853 -1.5848 218.2289 219.8137 257.5006 94.3048 -1.5847 218.3967 219.9814 257.6097 95.0930 -1.5927 218.5557 220.1485 257.7163 95.8813 -1.6031 218.7013 220.3045 257.8159 96.7300 -1.6041 218.8541 220.4582 257.9193 97.5188 -1.5934 219.0252 220.6185 258.0237 98.3070 -1.5855 219.1833 220.7688 258.1728 99.1268 -1.5840 219.3340 220.9179 258.2594 99.9185 -1.5905 219.5053 221.0958 258.3721 100.7480 -1.5986 219.6859 221.2845 258.4862 101.5365 -1.6077 219.8334 221.4411 258.6015 102.3250 -1.6224 219.9652 221.5876 258.7038 103.1740 -1.6100 220.1204 221.7304 258.8188 103.9323 -1.6022 220.2724 221.8747 258.9249 104.7508 -1.5997 220.4330 222.0327 259.0321 105.5693 -1.5998 220.5960 222.1957 259.1409 106.3580 -1.6008 220.7389 222.3397 259.2554 107.1768 -1.6034 220.9086 222.5120 259.3513 107.9650 -1.6037 221.0692 222.6728 259.4784 108.7545 -1.6000 221.2056 222.8055 259.6015 109.6035 -1.5992 221.3528 222.9520 259.7088 110.3620 -1.6006 221.5424 223.1430 259.8202 111.1848 -1.6042 221.6910 223.2952 259.9562 111.9730 -1.6048 221.8164 223.4211 260.0658 112.7620 -1.5981 221.9652 223.5633 260.1737 113.6105 -1.5975 222.1541 223.7516 260.2933 114.3703 -1.5957 222.2959 223.8916 260.4163 115.1898 -1.5951 222.4526 224.0477 260.5266 116.0093 -1.5983 222.6131 224.2115 260.6510 116.7685 -1.5994 222.7590 224.3584 260.7671 117.6175 -1.6027 222.9141 224.5168 260.8816 118.4070 -1.6026 223.0618 224.6644 260.9968 119.1965 -1.6036 223.2149 224.8185 261.1008 120.0153 -1.6009 223.3747 224.9756 261.2313 120.8058 -1.6023 223.5225 225.1248 261.3514 121.6345 -1.6036 223.6831 225.2867 261.4655 122.4285 -1.6044 223.8493 225.4537 261.5789 123.2178 -1.6014 223.9850 225.5864 261.6899 124.0405 -1.6020 224.1167 225.7187 261.8238 124.8010 -1.6041 224.2617 225.8658 261.9322 125.6520 -1.6057 224.4495 226.0553 262.0616 126.4413 -1.6095 224.5851 226.1946 262.1838 127.2310 -1.6165 224.7295 226.3460 262.2935 128.0495 -1.6156 224.8948 226.5105 262.3929 128.8385 -1.6183 225.0441 226.6625 262.5191 129.6588 -1.6183 225.1874 226.8058 262.6353 130.4480 -1.6140 225.3423 226.9563 262.7466 131.2370 -1.6145 225.4896 227.1040 262.8614 132.0865 -1.6084 225.6597 227.2680 262.9790 132.8450 -1.5938 225.7904 227.3842 263.0885 133.6640 -1.5807 225.9494 227.5302 263.2022 134.4838 -1.5836 226.1096 227.6932 263.3167 135.2430 -1.5870 226.2479 227.8349 263.4261 136.0915 -1.5891 226.3779 227.9670 263.5337 136.8805 -1.5882 226.5323 228.1205 263.6592 137.6700 -1.5911 226.6809 228.2719 263.7635 138.4890 -1.5900 226.8207 228.4107 263.8778 139.2780 -1.5931 226.9836 228.5768 263.9824 140.0968 -1.5943 227.1411 228.7354 264.1027 140.8953 -1.5946 227.2929 228.8876 264.1857 141.6910 -1.5960 227.4422 229.0381 264.2933 142.5093 -1.5949 227.6063 229.2011 264.4068 143.2980 -1.5916 227.7212 229.3128 264.5025 144.1168 -1.5955 227.8769 229.4724 264.6205 144.9070 -1.5969 228.0313 229.6282 264.7277 145.6970 -1.5972 228.1826 229.7798 264.8120 146.5455 -1.5972 228.3243 229.9215 264.8882 147.3035 -1.5992 228.4685 230.0677 264.9893 148.1220 -1.5947 228.6018 230.1964 265.0921 148.9408 -1.5973 228.7711 230.3684 265.1968 149.6990 -1.6060 228.9046 230.5105 265.3086 150.5488 -1.5994 229.0697 230.6691 265.4165 151.3375 -1.5958 229.1950 230.7907 265.5104 152.1273 -1.5993 229.3470 230.9463 265.6027 152.9508 -1.6022 229.5063 231.1084 265.7040 153.7393 -1.6046 229.6380 231.2426 265.7904 154.5580 -1.5997 229.7774 231.3771 265.8831 155.3463 -1.5994 229.9296 231.5289 265.9816 156.1350 -1.6020 230.0744 231.6763 266.0809 156.9838 -1.6037 230.2221 231.8258 266.1822 157.7420 -1.6063 230.3918 231.9981 266.2885 158.5608 -1.6051 230.5199 232.1250 266.3931 159.3793 -1.6062 230.6708 232.2770 266.4814 160.1380 -1.6119 230.7853 232.3972 266.5665 160.9865 -1.6267 230.9328 232.5595 266.6585 161.7750 -1.6305 231.0870 232.7175 266.7603 162.5640 -1.6191 231.2247 232.8438 266.8647 163.3823 -1.6254 231.3843 233.0097 266.9567 164.1710 -1.6233 231.5252 233.1486 267.0322 164.9898 -1.6245 231.6546 233.2791 267.1340 165.7828 -1.6262 231.8014 233.4276 267.2429 166.5720 -1.6310 231.9563 233.5873 267.3162 167.4205 -1.6308 232.0947 233.7255 267.4350 168.1790 -1.6340 232.2166 233.8506 267.5441 168.9978 -1.6239 232.3758 233.9996 267.6439 169.8163 -1.6138 232.5255 234.1393 267.7458 170.5755 -1.6145 232.6633 234.2778 267.8560 171.4265 -1.6167 232.8253 234.4420 267.9782 172.2150 -1.6138 232.9551 234.5689 268.0680 173.0040 -1.6153 233.1065 234.7218 268.1491 173.8220 -1.6150 233.2371 234.8521 268.2715 174.6103 -1.6134 233.3830 234.9964 268.3786 175.4298 -1.6249 233.5252 235.1501 268.4973 176.2185 -1.6277 233.6685 235.2963 268.6205 177.0070 -1.6220 233.7805 235.4025 268.7144 177.8560 -1.6209 233.9367 235.5575 268.8423 178.6143 -1.6201 234.0987 235.7188 268.9420 179.4330 -1.6279 234.2500 235.8779 269.0528 180.2518 -1.6293 234.3802 236.0095 269.1691 181.0100 -1.6259 234.5023 236.1282 269.2618 181.8615 -1.6244 234.6364 236.2608 269.4040 182.6505 -1.6189 234.7822 236.4011 269.5138 183.4400 -1.6179 234.9299 236.5478 269.6174 184.2898 -1.6234 235.0695 236.6929 269.7524 185.0780 -1.6259 235.2115 236.8374 269.8428 185.8673 -1.6279 235.3435 236.9714 269.9579 186.6863 -1.6235 235.4914 237.1149 270.0820 187.4750 -1.6235 235.6305 237.2540 270.1790 188.2943 -1.6235 235.7546 237.3780 270.2932 189.0830 -1.6230 235.8936 237.5167 270.4148 189.8720 -1.6228 236.0136 237.6364 270.5093 190.7205 -1.6258 236.1796 237.8054 270.6236 191.4790 -1.6307 236.3378 237.9684 270.7491 192.3183 -1.6312 236.4733 238.1046 270.8361 193.1070 -1.6324 236.6162 238.2485 270.9582 193.8968 -1.6303 236.7343 238.3646 271.0844 194.7168 -1.6312 236.8741 238.5053 271.1898 195.5060 -1.6341 237.0058 238.6399 271.3118 196.3248 -1.6365 237.1700 238.8065 271.4123 197.1130 -1.6350 237.2941 238.9291 271.5504 197.9018 -1.6402 237.4441 239.0843 271.6650 198.7500 -1.6391 237.5949 239.2340 271.7864 199.5093 -1.6409 237.7051 239.3460 271.8876 200.3283 -1.6389 237.8550 239.4939 272.0157 201.1480 -1.6406 237.9760 239.6166 272.1308 201.9095 -1.6449 238.1158 239.7607 272.2315 202.7453 -1.6423 238.2681 239.9104 272.3617 203.5365 -1.6423 238.3929 240.0352 272.4836 204.3590 -1.6443 238.5577 240.2021 272.5842 205.1475 -1.6416 238.6771 240.3188 272.6837 205.9360 -1.6410 238.7881 240.4290 272.7901 206.7555 -1.6419 238.9445 240.5863 272.9186 207.5443 -1.6412 239.0838 240.7250 273.0417 208.3635 -1.6435 239.2089 240.8524 273.1449 209.1523 -1.6446 239.3524 240.9970 273.2502 209.9410 -1.6405 239.4888 241.1293 273.3650 210.7895 -1.6455 239.6353 241.2808 273.4873 211.5488 -1.6456 239.7618 241.4075 273.5828 212.3680 -1.6450 239.8997 241.5447 273.6914 213.1923 -1.6488 240.0462 241.6951 273.7915 213.9510 -1.6501 240.1698 241.8199 273.8886 214.7995 -1.6527 240.3206 241.9733 273.9890 215.5880 -1.6504 240.4633 242.1137 274.0798 216.3770 -1.6517 240.5846 242.2362 274.1733 217.1953 -1.6584 240.7158 242.3742 274.2864 217.9840 -1.6690 240.8469 242.5160 274.3921 218.8028 -1.6624 240.9864 242.6488 274.4943 219.5945 -1.6611 241.1332 242.7943 274.5849 220.3850 -1.6616 241.2564 242.9180 274.6909 221.2335 -1.6604 241.3942 243.0546 274.7711 221.9920 -1.6659 241.5382 243.2041 274.8696 222.8108 -1.6682 241.6722 243.3404 274.9737 223.6293 -1.6644 241.7981 243.4625 275.0560 224.3883 -1.6638 241.9372 243.6010 275.1470 225.2433 -1.6637 242.0586 243.7223 275.2326 226.0025 -1.6668 242.1866 243.8533 275.3394 226.8220 -1.6710 242.3270 243.9980 275.4252 227.6408 -1.6682 242.4444 244.1126 275.5206 228.3990 -1.6653 242.5751 244.2404 275.6047 229.2498 -1.6678 242.7334 244.4012 275.6982 230.0385 -1.6675 242.8613 244.5288 275.7905 230.8270 -1.6657 242.9931 244.6589 275.8762 231.6458 -1.6662 243.1291 244.7953 275.9877 232.4343 -1.6671 243.2506 244.9177 276.0821 233.2760 -1.6694 243.4005 245.0699 276.1976 234.0390 -1.6672 243.5331 245.2003 276.3006 234.8590 -1.6665 243.6524 245.3188 276.3977 235.6798 -1.6666 243.7943 245.4608 276.5018 236.4400 -1.6685 243.9194 245.5879 276.6152 237.2885 -1.6719 244.0666 245.7384 276.7105 238.0785 -1.6708 244.1859 245.8568 276.8180 238.8690 -1.6751 244.3164 245.9915 276.9119 239.6875 -1.6699 244.4555 246.1254 277.0037 240.4760 -1.6731 244.5813 246.2543 277.1276 241.2948 -1.6827 244.7350 246.4177 277.2296 242.0833 -1.6796 244.8639 246.5435 277.3207 242.8730 -1.6752 244.9868 246.6620 277.4389 243.7280 -1.6773 245.1215 246.7988 277.5527 244.4885 -1.6820 245.2365 246.9185 277.6517 245.3098 -1.6810 245.3702 247.0511 277.7600 246.0990 -1.6798 245.5200 247.1998 277.8552 246.8900 -1.6825 245.6508 247.3334 277.9688 247.7083 -1.6872 245.7725 247.4597 278.0766 248.4970 -1.6866 245.8921 247.5787 278.1840 249.3158 -1.6847 246.0301 247.7148 278.3060 250.1065 -1.6859 246.1483 247.8342 278.4249 250.8970 -1.6899 246.2791 247.9690 278.5315 251.7470 -1.6921 246.4200 248.1121 278.6333 252.5053 -1.6949 246.5371 248.2321 278.7223 253.3253 -1.6929 246.6518 248.3447 278.8489 254.1448 -1.6906 246.8066 248.4972 278.9622 254.9033 -1.6956 246.9411 248.6367 279.0858 255.7530 -1.6963 247.0765 248.7728 279.1667 256.5413 -1.6948 247.2000 248.8948 279.2862 257.3303 -1.7011 247.3333 249.0344 279.3834 258.1495 -1.7004 247.4477 249.1481 279.4816 258.9385 -1.7000 247.5823 249.2823 279.5891 259.7578 -1.6995 247.7167 249.4162 279.7071 260.5463 -1.7037 247.8482 249.5519 279.8175 261.3350 -1.7080 247.9766 249.6846 279.9185 262.1863 -1.7123 248.1146 249.8269 280.0526 262.9450 -1.7063 248.2228 249.9290 280.1492 263.7638 -1.7051 248.3623 250.0673 280.2616 264.5823 -1.7099 248.4956 250.2054 280.3512 265.3710 -1.7165 248.6148 250.3313 280.4611 266.1898 -1.7146 248.7509 250.4655 280.5936 266.9780 -1.7186 248.8725 250.5911 280.6966 267.7670 -1.7225 249.0100 250.7325 280.8249 268.6155 -1.7154 249.1328 250.8482 280.9261 269.3740 -1.7180 249.2482 250.9662 281.0279 270.1940 -1.7215 249.4011 251.1226 281.1357 271.0163 -1.7158 249.5520 251.2678 281.2495 271.7760 -1.7159 249.6664 251.3824 281.3529 272.6275 -1.7198 249.7910 251.5108 281.4677 273.3860 -1.7242 249.8878 251.6120 281.5663 274.2048 -1.7199 250.0251 251.7450 281.6774 275.0243 -1.7231 250.1626 251.8857 281.7771 275.7828 -1.7254 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