DTA measure 1olom4 Test Date: 2023103:1657 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.25 s Mass = 1144.500 mg data_number = 1575 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3315 -5.4461 210.6255 216.0716 264.7080 2.1235 -5.4363 210.8676 216.3039 264.7460 2.9455 -5.4238 211.1215 216.5453 264.7819 3.7075 -5.4161 211.3626 216.7787 264.8295 4.5595 -5.4100 211.6085 217.0185 264.9050 5.3515 -5.3969 211.8320 217.2289 264.9559 6.1435 -5.3870 212.0618 217.4488 265.0067 6.9343 -5.3733 212.3112 217.6845 265.0454 7.7448 -5.3607 212.5384 217.8990 265.1271 8.5375 -5.3556 212.7837 218.1393 265.1941 9.3895 -5.3492 213.0417 218.3909 265.2892 10.1515 -5.3391 213.2676 218.6067 265.3582 10.9735 -5.3132 213.5066 218.8198 265.4365 11.7655 -5.3053 213.7263 219.0316 265.5358 12.5585 -5.2860 213.9594 219.2454 265.6254 13.3853 -5.2720 214.1796 219.4515 265.7364 14.1470 -5.2607 214.4101 219.6708 265.8458 15.0000 -5.2521 214.6677 219.9197 265.9495 15.7620 -5.2359 214.8892 220.1251 266.0569 16.5840 -5.2222 215.1320 220.3542 266.1712 17.3743 -5.2115 215.3378 220.5493 266.2828 18.1970 -5.1991 215.5937 220.7928 266.3987 18.9585 -5.1866 215.8124 220.9990 266.5183 19.8108 -5.1738 216.0504 221.2241 266.6577 20.6028 -5.1664 216.2604 221.4268 266.8014 21.3945 -5.1539 216.4747 221.6286 266.9317 22.2168 -5.1364 216.7381 221.8745 267.0614 22.9785 -5.1274 216.9453 222.0727 267.2040 23.8305 -5.1172 217.2016 222.3188 267.3351 24.5930 -5.1043 217.3953 222.4996 267.4782 25.4165 -5.0941 217.6349 222.7290 267.6249 26.2085 -5.0787 217.8637 222.9425 267.7448 27.0193 -5.0674 218.0878 223.1553 267.8992 27.8015 -5.0572 218.3053 223.3624 268.0489 28.6535 -5.0510 218.5583 223.6093 268.2019 29.4155 -5.0367 218.7492 223.7860 268.3328 30.2375 -5.0230 218.9789 224.0019 268.4761 31.0295 -5.0114 219.2041 224.2154 268.6120 31.8215 -5.0021 219.4296 224.4317 268.7728 32.6450 -4.9901 219.6702 224.6603 268.9384 33.4065 -4.9790 219.8710 224.8500 269.0691 34.2585 -4.9638 220.1037 225.0675 269.2120 35.0505 -4.9572 220.3122 225.2694 269.3393 35.8418 -4.9457 220.5388 225.4845 269.4642 36.6635 -4.9332 220.7640 225.6971 269.6002 37.4560 -4.9216 220.9863 225.9079 269.7475 38.2500 -4.9103 221.1831 226.0934 269.8845 39.0715 -4.8993 221.4174 226.3166 270.0239 39.8635 -4.8887 221.6417 226.5304 270.1558 40.6548 -4.8816 221.8567 226.7383 270.2779 41.4775 -4.8734 222.0776 226.9510 270.3995 42.2388 -4.8599 222.2713 227.1312 270.5122 43.0908 -4.8489 222.5019 227.3508 270.6370 43.8830 -4.8350 222.7255 227.5605 270.7556 44.6745 -4.8261 222.9354 227.7615 270.8711 45.4968 -4.8156 223.1666 227.9822 270.9843 46.2588 -4.8127 223.3681 228.1809 271.1060 47.1118 -4.8102 223.5961 228.4064 271.2153 47.8988 -4.8085 223.8044 228.6129 271.3208 48.6775 -4.7909 224.0250 228.8159 271.4186 49.4998 -4.7697 224.2311 229.0009 271.5225 50.3215 -4.7595 224.4398 229.1993 271.6276 51.0835 -4.7505 224.6371 229.3875 271.7319 51.9358 -4.7579 224.8888 229.6467 271.8402 52.7008 -4.7625 225.0861 229.8485 271.9318 53.5265 -4.7405 225.2923 230.0327 272.0341 54.3185 -4.7164 225.5076 230.2239 272.1249 55.1105 -4.6987 225.7119 230.4106 272.2237 55.9325 -4.6870 225.9316 230.6186 272.3389 56.6945 -4.6765 226.1346 230.8111 272.4286 57.5488 -4.6650 226.3608 231.0258 272.5446 58.3328 -4.6563 226.5531 231.2093 272.6336 59.1255 -4.6465 226.7541 231.4006 272.7257 59.9175 -4.6374 226.9531 231.5905 272.8173 60.7695 -4.6219 227.1792 231.8011 272.9215 61.5315 -4.6285 227.3809 232.0094 273.0129 62.3530 -4.6129 227.5906 232.2035 273.1058 63.1445 -4.5969 227.8087 232.4056 273.2005 63.9363 -4.5992 228.0176 232.6167 273.2794 64.7885 -4.5840 228.2244 232.8083 273.3757 65.5228 -4.5642 228.4214 232.9856 273.4460 66.3773 -4.5495 228.6323 233.1818 273.5530 67.1693 -4.5392 228.8220 233.3612 273.6467 67.9770 -4.5299 229.0350 233.5649 273.7337 68.7568 -4.5222 229.2354 233.7576 273.8292 69.5800 -4.5089 229.4332 233.9420 273.9040 70.3420 -4.4991 229.6180 234.1172 273.9793 71.1938 -4.4884 229.8384 234.3268 274.0818 71.9860 -4.4781 230.0288 234.5069 274.1793 72.7775 -4.4699 230.2389 234.7088 274.2601 73.5998 -4.4602 230.4406 234.9008 274.3495 74.3615 -4.4504 230.6286 235.0790 274.4489 75.2138 -4.4416 230.8392 235.2808 274.5534 75.9760 -4.4345 231.0356 235.4701 274.6424 76.7978 -4.4192 231.2371 235.6563 274.7442 77.6265 -4.4084 231.4281 235.8364 274.8371 78.4250 -4.3976 231.6240 236.0216 274.9386 79.1795 -4.3894 231.8236 236.2130 275.0385 80.0315 -4.3797 232.0405 236.4202 275.1467 80.7938 -4.3701 232.2227 236.5928 275.2403 81.6155 -4.3623 232.4098 236.7722 275.3565 82.4075 -4.3511 232.6037 236.9548 275.4547 83.1988 -4.3412 232.8019 237.1431 275.5565 84.0505 -4.3298 233.0149 237.3448 275.6838 84.8125 -4.3215 233.2030 237.5245 275.7722 85.6345 -4.3106 233.3942 237.7049 275.8746 86.4265 -4.3020 233.5850 237.8870 275.9931 87.2178 -4.2868 233.7767 238.0635 276.1024 88.0395 -4.2163 233.9769 238.1932 276.2160 88.8533 -4.2552 234.1724 238.4276 276.3273 89.6305 -4.2615 234.3712 238.6327 276.4341 90.4523 -4.2560 234.5706 238.8266 276.5507 91.2445 -4.2457 234.7485 238.9942 276.6391 92.0363 -4.2382 234.9309 239.1691 276.7538 92.8583 -4.2298 235.1451 239.3749 276.8700 93.6203 -4.2200 235.3117 239.5318 276.9885 94.4720 -4.2068 235.5305 239.7373 277.1011 95.2640 -4.1960 235.7083 239.9043 277.2045 96.0555 -4.1883 235.8993 240.0875 277.3298 96.8780 -4.1823 236.0778 240.2601 277.4451 97.6398 -4.1768 236.2641 240.4409 277.5449 98.4918 -4.1652 236.4625 240.6277 277.6613 99.2905 -4.1552 236.6562 240.8114 277.7800 100.0528 -4.1470 236.8355 240.9824 277.8888 100.8748 -4.1368 237.0135 241.1504 278.0073 101.6968 -4.1295 237.2067 241.3362 278.1253 102.4575 -4.1227 237.3743 241.4970 278.2259 103.3095 -4.1139 237.5848 241.6988 278.3512 104.0715 -4.1062 237.7549 241.8611 278.4564 104.8938 -4.0985 237.9592 242.0577 278.5933 105.6855 -4.0886 238.1414 242.2301 278.7061 106.4775 -4.0806 238.3222 242.4029 278.8161 107.3295 -4.0731 238.5135 242.5866 278.9508 108.0915 -4.0644 238.6795 242.7440 279.0624 108.9310 -4.0560 238.8718 242.9278 279.1795 109.7155 -4.0479 239.0535 243.1014 279.2994 110.5075 -4.0368 239.2479 243.2846 279.4199 111.3008 -4.0303 239.4229 243.4531 279.5435 112.1245 -4.0222 239.6086 243.6308 279.6560 112.8865 -4.0141 239.7739 243.7880 279.7664 113.7385 -4.0051 239.9595 243.9645 279.8806 114.5305 -3.9966 240.1597 244.1563 280.0336 115.3225 -3.9921 240.3465 244.3386 280.1561 116.1445 -3.9855 240.5252 244.5107 280.2580 116.9065 -3.9739 240.6973 244.6712 280.3748 117.7585 -3.9636 240.8961 244.8597 280.5042 118.5203 -3.9573 241.0640 245.0214 280.6066 119.3735 -3.9480 241.2498 245.1978 280.7332 120.1358 -3.9395 241.4267 245.3662 280.8413 120.9583 -3.9335 241.6052 245.5387 280.9551 121.7198 -3.9266 241.7763 245.7029 281.0527 122.5718 -3.9177 241.9655 245.8832 281.1699 123.3640 -3.9108 242.1452 246.0560 281.2885 124.1555 -3.9036 242.3113 246.2150 281.3823 124.9780 -3.8949 242.4900 246.3849 281.4979 125.7395 -3.8887 242.6667 246.5554 281.6265 126.5915 -3.8813 242.8470 246.7283 281.7316 127.3525 -3.8745 243.0325 246.9071 281.8252 128.1748 -3.8671 243.1966 247.0637 281.9182 128.9965 -3.8599 243.3874 247.2473 282.0234 129.8105 -3.8518 243.5671 247.4188 282.1301 130.5575 -3.8444 243.7287 247.5730 282.2302 131.4118 -3.8395 243.9178 247.7573 282.3527 132.1735 -3.8331 244.0719 247.9050 282.4291 132.9958 -3.8267 244.2574 248.0842 282.5505 133.8175 -3.8196 244.4348 248.2545 282.6448 134.5795 -3.8127 244.6148 248.4275 282.7422 135.4315 -3.8054 244.7873 248.5926 282.8596 136.1935 -3.7985 244.9576 248.7561 282.9425 137.0155 -3.7862 245.1373 248.9235 283.0466 137.8075 -3.7813 245.3014 249.0827 283.1510 138.5995 -3.7753 245.4629 249.2382 283.2394 139.4553 -3.7642 245.6571 249.4213 283.3514 140.2478 -3.7568 245.8309 249.5877 283.4646 141.0095 -3.7498 245.9962 249.7459 283.5565 141.8315 -3.7372 246.1713 249.9085 283.6541 142.6235 -3.7330 246.3263 250.0593 283.7567 143.4155 -3.7331 246.5022 250.2353 283.8583 144.2373 -3.7272 246.6721 250.3993 283.9580 145.0293 -3.7221 246.8521 250.5742 284.0601 145.8510 -3.7153 247.0179 250.7332 284.1582 146.6435 -3.7121 247.1819 250.8940 284.2527 147.4345 -3.7033 247.3568 251.0601 284.3381 148.2573 -3.6968 247.5154 251.2122 284.4530 149.0183 -3.6897 247.6773 251.3669 284.5581 149.8860 -3.6845 247.8767 251.5611 284.6489 150.6688 -3.6820 248.0350 251.7170 284.7304 151.4608 -3.6724 248.1995 251.8719 284.8190 152.2525 -3.6655 248.3570 252.0226 284.9257 153.0750 -3.6622 248.5443 252.2065 285.0360 153.8368 -3.6534 248.6922 252.3456 285.1201 154.6888 -3.6503 248.8630 252.5134 285.2334 155.4505 -3.6417 249.0119 252.6536 285.3519 156.2730 -3.6379 249.1950 252.8330 285.4558 157.0945 -3.6312 249.3645 252.9957 285.5620 157.8565 -3.6230 249.5150 253.1381 285.6474 158.7085 -3.6215 249.6896 253.3111 285.7777 159.4708 -3.6095 249.8543 253.4638 285.8810 160.3878 -3.6031 250.0524 253.6554 285.9896 161.3028 -3.5952 250.2415 253.8367 286.1104 162.0645 -3.5943 250.3864 253.9807 286.2116 162.9165 -3.5859 250.5614 254.1473 286.3317 163.6785 -3.5780 250.7217 254.2997 286.4436 164.5005 -3.5696 250.8962 254.4658 286.5602 165.3225 -3.5656 251.0590 254.6246 286.6777 166.0845 -3.5587 251.1903 254.7490 286.7772 166.9365 -3.5533 251.3767 254.9301 286.8995 167.6985 -3.5498 251.5447 255.0945 287.0178 168.5205 -3.5429 251.7065 255.2494 287.1317 169.3125 -3.5346 251.8723 255.4069 287.2465 170.1045 -3.5294 252.0234 255.5528 287.3711 170.9565 -3.5233 252.1984 255.7217 287.4821 171.7185 -3.5221 252.3482 255.8703 287.6108 172.5400 -3.5204 252.5191 256.0396 287.7361 173.3323 -3.5097 252.6766 256.1864 287.8346 174.1233 -3.5034 252.8302 256.3336 287.9526 174.9450 -3.4973 252.9901 256.4874 288.0727 175.7070 -3.4925 253.1373 256.6298 288.1950 176.5588 -3.4838 253.3047 256.7886 288.3147 177.3508 -3.4772 253.4745 256.9517 288.4378 178.1428 -3.4804 253.6370 257.1174 288.5567 178.9650 -3.4824 253.8018 257.2842 288.6776 179.7255 -3.4885 253.9644 257.4530 288.7914 180.6283 -3.4641 254.1370 257.6012 288.9279 181.5418 -3.4582 254.3039 257.7621 289.0560 182.3638 -3.3722 254.4699 257.8422 289.1606 183.1855 -3.4119 254.6333 258.0452 289.2791 183.9483 -3.4267 254.7838 258.2105 289.3844 184.8015 -3.4297 254.9517 258.3814 289.4934 185.5635 -3.4271 255.0992 258.5262 289.6018 186.3855 -3.4192 255.2669 258.6860 289.7001 187.1775 -3.4165 255.4104 258.8269 289.8152 187.9695 -3.4137 255.5657 258.9795 289.9236 188.7925 -3.4270 255.7256 259.1526 290.0304 189.5855 -3.4248 255.8866 259.3114 290.1106 190.4075 -3.4355 256.0495 259.4849 290.2227 191.1720 -3.4098 256.1897 259.5995 290.3223 191.9965 -3.3893 256.3511 259.7404 290.4330 192.8185 -3.3818 256.5059 259.8876 290.5472 193.5833 -3.3790 256.6640 260.0429 290.6234 194.4385 -3.3730 256.8283 260.2013 290.7340 195.2005 -3.3693 256.9684 260.3377 290.8233 196.0225 -3.3685 257.1303 260.4988 290.9317 196.8145 -3.3599 257.2693 260.6292 291.0303 197.6065 -3.3703 257.4250 260.7952 291.1311 198.4283 -3.3626 257.6022 260.9648 291.2318 199.2203 -3.3434 257.7374 261.0808 291.3304 200.0418 -3.3335 257.9053 261.2388 291.4281 200.8355 -3.3286 258.0522 261.3808 291.5181 201.8350 -3.3257 258.2379 261.5636 291.6221 202.6565 -3.3204 258.3844 261.7048 291.7210 203.4478 -3.3158 258.5480 261.8639 291.8294 204.2395 -3.3096 258.7085 262.0180 291.9091 205.0670 -3.3059 258.8754 262.1813 292.0116 205.8288 -3.2987 259.0072 262.3060 292.0902 206.6810 -3.2925 259.1579 262.4504 292.1942 207.4435 -3.2877 259.3018 262.5895 292.2794 208.2658 -3.2829 259.4484 262.7313 292.4006 209.0575 -3.2785 259.6025 262.8811 292.4893 209.8495 -3.2738 259.7640 263.0378 292.5740 210.7015 -3.2706 259.9172 263.1878 292.6895 211.4638 -3.2590 260.0669 263.3259 292.7895 212.2878 -3.2590 260.2210 263.4800 292.8865 213.0795 -3.2584 260.3674 263.6258 292.9853 213.8715 -3.2560 260.5246 263.7806 293.0835 214.6943 -3.2512 260.6674 263.9187 293.1981 215.4565 -3.2467 260.8069 264.0536 293.2970 216.3085 -3.2428 260.9703 264.2130 293.4215 217.0705 -3.2393 261.1266 264.3659 293.5131 217.8925 -3.2358 261.2591 264.4949 293.6079 218.7145 -3.2285 261.4052 264.6338 293.7260 219.4765 -3.2234 261.5459 264.7693 293.8291 220.3285 -3.2199 261.7122 264.9320 293.9693 221.0908 -3.2153 261.8472 265.0626 294.0417 222.0550 -3.2107 262.0393 265.2500 294.1820 222.9235 -3.2053 262.1969 265.4022 294.3055 223.6855 -3.2024 262.3337 265.5361 294.4222 224.5383 -3.1975 262.4850 265.6825 294.5329 225.3005 -3.1959 262.6244 265.8203 294.6284 226.1220 -3.1897 262.7783 265.9680 294.7551 226.9443 -3.1870 262.9219 266.1089 294.8625 227.7060 -3.1830 263.0721 266.2552 294.9801 228.5580 -3.1779 263.2253 266.4032 295.0907 229.3198 -3.1765 263.3370 266.5135 295.1936 230.1418 -3.1502 263.4985 266.6486 295.3242 230.9340 -3.1491 263.6652 266.8143 295.4307 231.7255 -3.1574 263.7979 266.9553 295.5457 232.5478 -3.1505 263.9443 267.0949 295.6520 233.3095 -3.1503 264.0865 267.2368 295.7649 234.1618 -3.1500 264.2394 267.3894 295.8819 234.9538 -3.1456 264.3936 267.5391 296.0027 235.7448 -3.1441 264.5220 267.6661 296.1184 236.5718 -3.1418 264.6658 267.8076 296.2356 237.3335 -3.1401 264.8180 267.9581 296.3537 238.1855 -3.1342 264.9734 268.1075 296.4690 238.9475 -3.1327 265.1063 268.2389 296.5726 239.7695 -3.1284 265.2541 268.3825 296.6868 240.5615 -3.1234 265.3925 268.5159 296.8194 241.3535 -3.1204 265.5385 268.6589 296.9225 242.3008 -3.1169 265.7026 268.8195 297.0502 243.1595 -3.1137 265.8610 268.9747 297.1682 243.9818 -3.1087 266.0021 269.1107 297.2899 244.7743 -3.1053 266.1403 269.2456 297.4031 245.5685 -3.1015 266.2836 269.3851 297.5129 246.4205 -3.0984 266.4400 269.5383 297.6281 247.1825 -3.0975 266.5693 269.6669 297.7321 248.0045 -3.0956 266.7231 269.8187 297.8377 248.7965 -3.0938 266.8672 269.9611 297.9470 249.5885 -3.0904 266.9987 270.0890 298.0439 250.4105 -3.0850 267.1404 270.2254 298.1545 251.2025 -3.0817 267.2919 270.3736 298.2499 252.0233 -3.0804 267.4467 270.5271 298.3403 252.8153 -3.0762 267.5887 270.6648 298.4497 253.6073 -3.0727 267.7147 270.7874 298.5381 254.4293 -3.0698 267.8533 270.9230 298.6418 255.1908 -3.0674 268.0041 271.0714 298.7396 256.0430 -3.0674 268.1431 271.2105 298.8385 256.8350 -3.0569 268.2801 271.3369 298.9467 257.6268 -3.0437 268.4241 271.4678 299.0305 258.4488 -3.0404 268.5641 271.6045 299.1356 259.2108 -3.0465 268.6928 271.7393 299.2344 260.0628 -3.0468 268.8490 271.8958 299.3422 260.8548 -3.0449 269.0162 272.0611 299.4283 261.6465 -3.0429 269.1534 272.1964 299.5278 262.5175 -3.0395 269.2889 272.3284 299.6227 263.4248 -3.0362 269.4261 272.4623 299.7314 264.2765 -3.0323 269.5638 272.5961 299.8328 265.0693 -3.0284 269.7236 272.7521 299.9173 265.8605 -3.0259 269.8618 272.8877 300.0089 266.6828 -3.0269 270.0040 273.0309 300.1132 267.4445 -3.0227 270.1396 273.1623 300.2182 268.2988 -3.0203 270.2889 273.3092 300.3144 269.0605 -3.0150 270.4150 273.4300 300.4160 269.8825 -3.0102 270.5586 273.5688 300.5227 270.7045 -3.0089 270.7083 273.7171 300.6204 271.4665 -3.0072 270.8293 273.8365 300.7275 272.3185 -3.0068 270.9851 273.9918 300.8307 273.0830 -3.0029 271.1100 274.1129 300.9164 273.9055 -2.9967 271.2476 274.2443 301.0312 274.7025 -2.9959 271.3696 274.3655 301.1350 275.4968 -2.9921 271.5166 274.5087 301.2486 276.3233 -2.9909 271.6634 274.6542 301.3388 277.0880 -2.9864 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