DTA measure 1proba.dat Test Date: 20231011:166 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.59 s Mass = 1402.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1985 -1.9814 271.3774 273.3587 260.5934 2.0510 -1.9824 271.3917 273.3741 260.6082 2.8128 -1.9819 271.3858 273.3677 260.6122 3.6348 -1.9827 271.3852 273.3680 260.6189 4.4570 -1.9812 271.3863 273.3675 260.6363 5.2185 -1.9809 271.3768 273.3577 260.6370 6.0718 -1.9822 271.3934 273.3756 260.6396 6.8358 -1.9816 271.3917 273.3733 260.6649 7.6575 -1.9805 271.3811 273.3616 260.7092 8.4798 -1.9788 271.3918 273.3706 260.7093 9.2415 -1.9801 271.3952 273.3753 260.7155 10.0938 -1.9798 271.3841 273.3639 260.7465 10.8555 -1.9810 271.3799 273.3609 260.7906 11.6775 -1.9836 271.3727 273.3562 260.8403 12.4995 -1.9822 271.3901 273.3722 260.8788 13.2615 -1.9820 271.3866 273.3686 260.8983 14.1135 -1.9842 271.3801 273.3642 260.9443 14.8755 -1.9859 271.3842 273.3700 261.0059 15.6975 -1.9848 271.3835 273.3683 261.0786 16.5205 -1.9847 271.3728 273.3575 261.1452 17.2835 -1.9856 271.3863 273.3718 261.2157 18.1360 -1.9865 271.3853 273.3718 261.2955 18.8985 -1.9860 271.3922 273.3782 261.3812 19.7205 -1.9814 271.3889 273.3703 261.4569 20.5423 -1.9831 271.3788 273.3620 261.5508 21.3035 -1.9839 271.3791 273.3630 261.6410 22.1565 -1.9832 271.3841 273.3673 261.7502 22.9188 -1.9841 271.4007 273.3848 261.8793 23.7405 -1.9820 271.4018 273.3839 261.9567 24.5593 -1.9832 271.4033 273.3865 262.0633 25.3175 -1.9857 271.4108 273.3965 262.1731 26.1655 -1.9842 271.4094 273.3936 262.2957 26.9235 -1.9831 271.4090 273.3921 262.3978 27.7435 -1.9844 271.4033 273.3877 262.5291 28.5615 -1.9861 271.4072 273.3933 262.6614 29.3198 -1.9880 271.4038 273.3918 262.7752 30.1685 -1.9886 271.4173 273.4059 262.9155 30.9578 -1.9900 271.4118 273.4018 263.0582 31.7473 -1.9917 271.4305 273.4223 263.1872 32.5685 -1.9952 271.4374 273.4326 263.3234 33.3300 -1.9970 271.4423 273.4392 263.4565 34.1820 -2.0009 271.4454 273.4463 263.5862 34.9740 -2.0020 271.4217 273.4237 263.7344 35.7660 -2.0033 271.4349 273.4382 263.8438 36.5898 -2.0036 271.4376 273.4412 263.9920 37.3548 -2.0063 271.4460 273.4523 264.1317 38.2070 -2.0058 271.4806 273.4864 264.2799 38.9690 -2.0076 271.4855 273.4931 264.4060 39.7908 -2.0094 271.4948 273.5042 264.5499 40.6130 -2.0152 271.4798 273.4950 264.7051 41.3745 -2.0157 271.4794 273.4950 264.8261 42.2270 -2.0177 271.4960 273.5137 264.9695 42.9888 -2.0166 271.5018 273.5185 265.0863 43.8108 -2.0176 271.5182 273.5357 265.2496 44.6330 -2.0197 271.5112 273.5309 265.3782 45.3945 -2.0216 271.5279 273.5495 265.4995 46.2468 -2.0221 271.5301 273.5522 265.6453 47.0085 -2.0228 271.5483 273.5711 265.7786 47.8308 -2.0252 271.5480 273.5732 265.9104 48.6528 -2.0256 271.5737 273.5993 266.0503 49.4145 -2.0279 271.5845 273.6124 266.1647 50.2665 -2.0296 271.5994 273.6290 266.3137 51.0585 -2.0311 271.5982 273.6293 266.4567 51.8505 -2.0329 271.6259 273.6588 266.6000 52.6725 -2.0352 271.6458 273.6810 266.7290 53.4345 -2.0353 271.6414 273.6767 266.8488 54.2865 -2.0370 271.6507 273.6877 266.9973 55.0785 -2.0420 271.6770 273.7190 267.1265 55.8698 -2.0432 271.6822 273.7254 267.2422 56.6865 -2.0437 271.6929 273.7366 267.3731 57.4458 -2.0428 271.7060 273.7487 267.4967 58.2940 -2.0467 271.7320 273.7788 267.6289 59.0820 -2.0497 271.7469 273.7966 267.7784 59.8718 -2.0513 271.7651 273.8163 267.8926 60.6910 -2.0515 271.7819 273.8334 268.0178 61.4500 -2.0539 271.7925 273.8464 268.1413 62.2985 -2.0538 271.8188 273.8726 268.2816 63.0873 -2.0581 271.8326 273.8906 268.4033 63.8785 -2.0591 271.8486 273.9077 268.5064 64.6988 -2.0595 271.8594 273.9189 268.6356 65.4605 -2.0624 271.8882 273.9506 268.7567 66.3118 -2.0636 271.9136 273.9772 268.8735 67.0735 -2.0661 271.9174 273.9835 268.9819 67.8955 -2.0649 271.9311 273.9960 269.1026 68.7180 -2.0663 271.9633 274.0296 269.2304 69.4805 -2.0709 271.9909 274.0618 269.3341 70.3325 -2.0702 272.0091 274.0793 269.4667 71.0948 -2.0703 272.0360 274.1063 269.5703 71.9175 -2.0684 272.0320 274.1005 269.6905 72.7100 -2.0696 272.0609 274.1305 269.8198 73.5045 -2.0720 272.0985 274.1705 269.9411 74.3565 -2.0714 272.1237 274.1951 270.0506 75.1185 -2.0721 272.1469 274.2191 270.1573 75.9403 -2.0727 272.1863 274.2590 270.2734 76.7325 -2.0746 272.1993 274.2739 270.4019 77.5238 -2.0758 272.2294 274.3051 270.4995 78.3463 -2.0752 272.2511 274.3263 270.6238 79.1388 -2.0766 272.2668 274.3434 270.7506 79.9608 -2.0790 272.3105 274.3895 270.8673 80.7530 -2.0823 272.3328 274.4151 270.9735 81.5445 -2.0829 272.3644 274.4473 271.1081 82.3670 -2.0820 272.4000 274.4820 271.2151 83.1588 -2.0838 272.4294 274.5132 271.3535 83.9815 -2.0839 272.4586 274.5426 271.5052 84.7738 -2.0841 272.4837 274.5678 271.6193 85.5655 -2.0841 272.5252 274.6093 271.7371 86.3878 -2.0834 272.5460 274.6294 271.8636 87.1795 -2.0844 272.5681 274.6525 271.9700 88.0018 -2.0829 272.6019 274.6849 272.1099 88.7903 -2.0794 272.6383 274.7177 272.2385 89.5790 -2.0786 272.6782 274.7569 272.3631 90.3975 -2.0807 272.6967 274.7774 272.5020 91.1560 -2.0807 272.7145 274.7952 272.6266 92.0040 -2.0804 272.7611 274.8414 272.7540 92.7920 -2.0818 272.7893 274.8711 272.8676 93.5818 -2.0815 272.8330 274.9144 273.0001 94.4013 -2.0816 272.8608 274.9424 273.1205 95.1608 -2.0822 272.8941 274.9763 273.2299 96.0118 -2.0802 272.9403 275.0205 273.3781 96.8020 -2.0802 272.9799 275.0601 273.4945 97.5925 -2.0799 273.0105 275.0904 273.6199 98.4145 -2.0788 273.0274 275.1062 273.7350 99.1765 -2.0809 273.0769 275.1578 273.8403 100.0290 -2.0825 273.1189 275.2014 273.9814 100.7905 -2.0844 273.1601 275.2446 274.0785 101.6128 -2.0856 273.1897 275.2752 274.2098 102.4345 -2.0843 273.2437 275.3280 274.3314 103.1965 -2.0877 273.2872 275.3749 274.4445 104.0485 -2.0887 273.3082 275.3969 274.5927 104.8105 -2.0887 273.3490 275.4378 274.7164 105.6325 -2.0857 273.3925 275.4782 274.8369 106.4545 -2.0849 273.4433 275.5282 274.9592 107.2165 -2.0861 273.4750 275.5611 275.0995 108.0685 -2.0850 273.5284 275.6134 275.2350 108.8305 -2.0826 273.5746 275.6573 275.3550 109.6525 -2.0859 273.6210 275.7069 275.4859 110.4748 -2.0861 273.6493 275.7354 275.6389 111.2375 -2.0831 273.6936 275.7767 275.7594 112.0895 -2.0809 273.7378 275.8187 275.9085 112.8515 -2.0827 273.7714 275.8541 276.0374 113.6733 -2.0847 273.8175 275.9022 276.1757 114.4955 -2.0825 273.8670 275.9495 276.3041 115.2573 -2.0819 273.9114 275.9932 276.4425 116.1090 -2.0817 273.9479 276.0295 276.5941 116.9010 -2.0841 274.0090 276.0931 276.7177 117.6925 -2.0842 274.0532 276.1374 276.8425 118.5150 -2.0810 274.1002 276.1812 276.9826 119.2765 -2.0818 274.1350 276.2168 277.1095 120.1280 -2.0814 274.2053 276.2868 277.2596 120.8863 -2.0838 274.2471 276.3309 277.3959 121.7043 -2.0844 274.2924 276.3769 277.5163 122.5228 -2.0825 274.3373 276.4198 277.6556 123.2810 -2.0802 274.4033 276.4834 277.7903 124.1303 -2.0804 274.4616 276.5420 277.9433 124.9185 -2.0811 274.5020 276.5831 278.0746 125.7073 -2.0787 274.5444 276.6231 278.2041 126.5258 -2.0807 274.5967 276.6774 278.3470 127.2860 -2.0780 274.6434 276.7214 278.4786 128.1380 -2.0764 274.6890 276.7654 278.6010 128.9290 -2.0745 274.7495 276.8240 278.7298 129.7205 -2.0845 274.8042 276.8887 278.8682 130.5430 -2.0747 274.8635 276.9381 279.0117 131.3048 -2.0701 274.9084 276.9785 279.1197 132.1570 -2.0720 274.9757 277.0478 279.2486 132.9490 -2.0715 275.0259 277.0974 279.4021 133.7405 -2.0707 275.0754 277.1461 279.5249 134.5630 -2.0728 275.1361 277.2089 279.6322 135.3245 -2.0735 275.2125 277.2860 279.7617 136.1770 -2.0731 275.2516 277.3247 279.8974 136.9690 -2.0725 275.3136 277.3861 280.0186 137.7605 -2.0698 275.3756 277.4453 280.1499 138.5830 -2.0677 275.4221 277.4898 280.2750 139.3445 -2.0674 275.4771 277.5445 280.3981 140.1970 -2.0668 275.5509 277.6177 280.5303 140.9888 -2.0656 275.6032 277.6688 280.6597 141.7815 -2.0645 275.6693 277.7338 280.7863 142.6038 -2.0656 275.7177 277.7833 280.9050 143.3655 -2.0615 275.7596 277.8212 281.0183 144.2183 -2.0594 275.8286 277.8880 281.1666 145.0105 -2.0595 275.9072 277.9667 281.2855 145.8025 -2.0609 275.9544 278.0153 281.3938 146.6245 -2.0597 276.0338 278.0935 281.5162 147.4165 -2.0615 276.0999 278.1614 281.6533 148.2393 -2.0586 276.1625 278.2211 281.7717 149.0315 -2.0575 276.2112 278.2687 281.9184 149.8235 -2.0563 276.2827 278.3390 282.0076 150.6455 -2.0544 276.3492 278.4036 282.1134 151.4375 -2.0530 276.4160 278.4690 282.2352 152.2595 -2.0510 276.4731 278.5241 282.3540 153.0505 -2.0498 276.5371 278.5869 282.4638 153.8388 -2.0480 276.5986 278.6466 282.5830 154.6570 -2.0478 276.6740 278.7218 282.7053 155.4448 -2.0470 276.7283 278.7753 282.8170 156.2638 -2.0427 276.8032 278.8459 282.9435 157.0528 -2.0438 276.8829 278.9267 283.0506 157.8420 -2.0427 276.9444 278.9872 283.1649 158.6608 -2.0432 277.0039 279.0471 283.2990 159.4508 -2.0411 277.0588 279.0999 283.4130 160.2703 -2.0388 277.1343 279.1731 283.5509 161.0605 -2.0390 277.2079 279.2469 283.6692 161.8525 -2.0401 277.2587 279.2989 283.7857 162.7045 -2.0380 277.3457 279.3836 283.9194 163.4665 -2.0379 277.4220 279.4599 284.0561 164.2885 -2.0391 277.4800 279.5191 284.1845 165.0805 -2.0379 277.5456 279.5836 284.3278 165.8725 -2.0339 277.6195 279.6534 284.4550 166.7245 -2.0335 277.7017 279.7352 284.5877 167.4865 -2.0342 277.7785 279.8127 284.7131 168.3085 -2.0330 277.8581 279.8911 284.8555 169.1005 -2.0323 277.9033 279.9355 284.9851 169.8920 -2.0286 277.9899 280.0185 285.1201 170.7445 -2.0260 278.0663 280.0923 285.2507 171.5060 -2.0264 278.1297 280.1561 285.3688 172.3283 -2.0279 278.2262 280.2541 285.5181 173.1200 -2.0258 278.2956 280.3213 285.6430 173.9115 -2.0230 278.3694 280.3924 285.7862 174.7645 -2.0233 278.4288 280.4521 285.9249 175.5268 -2.0206 278.5043 280.5248 286.0515 176.3488 -2.0172 278.5792 280.5964 286.1792 177.1410 -2.0166 278.6542 280.6708 286.3076 177.9325 -2.0161 278.7182 280.7342 286.4283 178.7848 -2.0125 278.8227 280.8352 286.5775 179.5465 -2.0118 278.8798 280.8916 286.7043 180.3688 -2.0092 278.9583 280.9675 286.8308 181.1908 -2.0006 279.0401 281.0407 286.9657 181.9525 -2.0029 279.1201 281.1230 287.0808 182.8048 -2.0028 279.2077 281.2105 287.2370 183.5665 -2.0066 279.2904 281.2970 287.3573 184.3885 -2.0062 279.3510 281.3572 287.4879 185.2090 -2.0040 279.4347 281.4387 287.6055 185.9670 -2.0034 279.5005 281.5039 287.7207 186.8150 -2.0021 279.5863 281.5884 287.8588 187.5733 -2.0027 279.6639 281.6666 287.9716 188.3928 -2.0011 279.7270 281.7281 288.1070 189.1810 -2.0005 279.8094 281.8099 288.2257 189.9690 -1.9994 279.9104 281.9098 288.3497 190.8175 -1.9990 280.0056 282.0046 288.4850 191.5763 -1.9984 280.0697 282.0681 288.5896 192.3968 -1.9983 280.1499 282.1483 288.7158 193.1883 -1.9979 280.2226 282.2205 288.8407 193.9795 -1.9963 280.2915 282.2878 288.9613 194.8020 -1.9962 280.3811 282.3773 289.0890 195.5935 -1.9948 280.4742 282.4690 289.2152 196.4158 -1.9929 280.5561 282.5491 289.3458 197.2075 -1.9952 280.6184 282.6135 289.4652 197.9995 -1.9938 280.7134 282.7072 289.5846 198.8215 -1.9923 280.8193 282.8116 289.7053 199.5835 -1.9909 280.8867 282.8776 289.8211 200.4355 -1.9902 280.9722 282.9624 289.9608 201.2275 -1.9886 281.0473 283.0358 290.0596 202.0195 -1.9870 281.1396 283.1266 290.1841 202.8415 -1.9842 281.2266 283.2107 290.2875 203.6035 -1.9858 281.3050 283.2908 290.4092 204.4555 -1.9834 281.4053 283.3887 290.5503 205.2175 -1.9798 281.5019 283.4817 290.6709 206.0395 -1.9791 281.5751 283.5542 290.8155 206.8618 -1.9776 281.6677 283.6453 290.9487 207.6245 -1.9773 281.7542 283.7314 291.0739 208.4765 -1.9766 281.8554 283.8320 291.2212 209.2380 -1.9759 281.9386 283.9145 291.3183 210.0600 -1.9802 282.0243 284.0045 291.4629 210.8523 -1.9785 282.1062 284.0847 291.5932 211.6435 -1.9749 282.1779 284.1527 291.7392 212.4960 -1.9740 282.2856 284.2596 291.8781 213.2578 -1.9748 282.3672 284.3420 292.0008 214.0798 -1.9736 282.4587 284.4322 292.1507 214.8720 -1.9823 282.5477 284.5301 292.2974 215.6645 -1.9766 282.6433 284.6199 292.4366 216.5170 -1.9738 282.7311 284.7049 292.5847 217.2760 -1.9722 282.8133 284.7855 292.7071 218.0950 -1.9685 282.9188 284.8873 292.8570 218.8835 -1.9681 282.9919 284.9600 292.9814 219.6720 -1.9659 283.0797 285.0456 293.1113 220.5213 -1.9650 283.1594 285.1244 293.2642 221.2808 -1.9658 283.2399 285.2057 293.3825 222.1000 -1.9645 283.3502 285.3147 293.5191 222.8883 -1.9633 283.4479 285.4112 293.6826 223.6775 -1.9631 283.5373 285.5003 293.8177 224.5283 -1.9625 283.6307 285.5932 293.9635 225.2890 -1.9646 283.7425 285.7071 294.0882 226.1090 -1.9628 283.8455 285.8083 294.2054 226.9010 -1.9636 283.9275 285.8911 294.3528 227.6925 -1.9643 284.0107 285.9750 294.4813 228.5150 -1.9626 284.1070 286.0696 294.6065 229.3068 -1.9621 284.2314 286.1935 294.7422 230.1288 -1.9619 284.3016 286.2635 294.8740 230.9210 -1.9606 284.3877 286.3483 295.0093 231.7125 -1.9617 284.5033 286.4649 295.1467 232.5350 -1.9580 284.5935 286.5515 295.2837 233.3268 -1.9594 284.6933 286.6528 295.4219 234.1488 -1.9604 284.7793 286.7397 295.5613 234.9408 -1.9628 284.8660 286.8288 295.6708 235.7325 -1.9626 284.9593 286.9219 295.8066 236.5548 -1.9615 285.0579 287.0193 295.9241 237.3165 -1.9622 285.1360 287.0982 296.0377 238.1688 -1.9605 285.2368 287.1972 296.1868 238.9605 -1.9597 285.3419 287.3016 296.3064 239.7525 -1.9627 285.4456 287.4084 296.4362 240.5745 -1.9620 285.5423 287.5043 296.5598 241.3365 -1.9620 285.6368 287.5988 296.6951 242.1885 -1.9639 285.7546 287.7185 296.8449 242.9805 -1.9606 285.8490 287.8095 296.9673 243.7725 -1.9617 285.9372 287.8989 297.0714 244.5945 -1.9586 286.0349 287.9935 297.2068 245.3565 -1.9594 286.1195 288.0790 297.3389 246.2085 -1.9588 286.2510 288.2098 297.4630 247.0005 -1.9568 286.3429 288.2998 297.5868 247.7925 -1.9576 286.4313 288.3888 297.7226 248.6143 -1.9589 286.5322 288.4912 297.8531 249.4025 -1.9572 286.6209 288.5782 297.9965 250.2205 -1.9570 286.7382 288.6953 298.1211 251.0090 -1.9582 286.8399 288.7981 298.2348 251.7975 -1.9574 286.9420 288.8994 298.3527 252.6160 -1.9558 287.0455 289.0013 298.4897 253.4038 -1.9549 287.1513 289.1062 298.6084 254.2228 -1.9556 287.2641 289.2197 298.7403 255.0120 -1.9577 287.3535 289.3112 298.8446 255.8010 -1.9580 287.4454 289.4034 298.9680 256.6508 -1.9551 287.5757 289.5308 299.0937 257.4125 -1.9573 287.6700 289.6272 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