DTA measure 2proba.dat Test Date: 20231011:1636 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.65 s Mass = 1402.000 mg data_number = 1026 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.2945 -5.5736 430.9133 436.4869 416.6155 3.9084 -5.5844 430.9317 436.5161 416.6150 5.5224 -5.5942 430.9563 436.5505 416.5936 7.1368 -5.6042 430.9861 436.5903 416.5830 8.7358 -5.6096 431.0131 436.6227 416.5141 10.3498 -5.6220 431.0214 436.6434 416.4380 11.9488 -5.6278 431.0571 436.6849 416.3384 13.5776 -5.6357 431.0704 436.7062 416.2390 15.1723 -5.6433 431.0805 436.7238 416.1043 16.7780 -5.6492 431.1132 436.7624 415.9446 18.3695 -5.6557 431.1295 436.7852 415.7773 19.9621 -5.6633 431.1334 436.7967 415.5994 21.5885 -5.6714 431.1548 436.8262 415.4093 23.1839 -5.6761 431.1664 436.8425 415.1955 24.7978 -5.6808 431.1762 436.8570 414.9719 26.3968 -5.6838 431.1790 436.8628 414.7719 27.9958 -5.6894 431.1856 436.8749 414.5569 29.6248 -5.6931 431.1978 436.8909 414.3501 31.2238 -5.6978 431.2057 436.9035 414.1467 32.8376 -5.7041 431.2003 436.9044 413.9301 34.4366 -5.7082 431.1883 436.8964 413.7299 36.0368 -5.7111 431.1897 436.9008 413.5318 37.6673 -5.7167 431.1863 436.9030 413.3152 39.2665 -5.7202 431.1714 436.8916 413.1123 40.8805 -5.7242 431.1629 436.8871 412.9138 42.4793 -5.7252 431.1498 436.8750 412.7220 44.0936 -5.7287 431.1374 436.8661 412.5304 45.7085 -5.7289 431.1316 436.8605 412.3338 47.3174 -5.7308 431.1057 436.8365 412.1461 48.9099 -5.7334 431.0839 436.8173 411.9456 50.5044 -5.7348 431.0622 436.7970 411.7603 52.0984 -5.7369 431.0337 436.7706 411.5858 53.7210 -5.7392 431.0209 436.7601 411.4043 55.3168 -5.7433 430.9767 436.7200 411.2117 56.9304 -5.7507 430.9474 436.6981 411.0146 58.5293 -5.7511 430.9207 436.6717 410.7975 60.1279 -5.7516 430.8790 436.6306 410.5967 61.7435 -5.7536 430.8366 436.5902 410.3959 63.3579 -5.7550 430.8151 436.5701 410.1940 64.9568 -5.7545 430.7706 436.5251 410.0032 66.5708 -5.7568 430.7162 436.4730 409.7824 68.1696 -5.7594 430.6685 436.4279 409.5742 69.7843 -5.7609 430.6262 436.3871 409.3964 71.3988 -5.7606 430.5774 436.3380 409.1910 72.9976 -5.7614 430.5274 436.2888 409.0043 74.6115 -5.7616 430.4961 436.2577 408.7893 76.2110 -5.7622 430.4295 436.1917 408.5947 77.8251 -5.7642 430.3765 436.1407 408.4072 79.4329 -5.7654 430.3149 436.0803 408.2311 81.0246 -5.7671 430.2649 436.0320 408.0396 82.6163 -5.7682 430.1988 435.9670 407.8380 84.2240 -5.7700 430.1325 435.9025 407.6638 85.8196 -5.7685 430.0732 435.8417 407.4633 87.4469 -5.7703 429.9977 435.7680 407.2770 89.0455 -5.7723 429.9213 435.6937 407.0951 90.6445 -5.7727 429.8639 435.6366 406.8770 92.2435 -5.7726 429.7800 435.5526 406.6745 93.8576 -5.7756 429.7262 435.5018 406.4694 95.4725 -5.7743 429.6489 435.4232 406.2582 97.0715 -5.7732 429.5591 435.3323 406.0491 98.6853 -5.7750 429.4858 435.2608 405.8354 100.2843 -5.7771 429.3951 435.1722 405.6247 101.8978 -5.7773 429.3266 435.1039 405.4280 103.5119 -5.7769 429.2393 435.0162 405.2162 105.1116 -5.7788 429.1673 434.9461 405.0074 106.7280 -5.7801 429.0589 434.8390 404.8058 108.3280 -5.7808 428.9651 434.7459 404.5851 109.9273 -5.7806 428.8908 434.6714 404.3798 111.5486 -5.7828 428.7902 434.5731 404.1845 113.1410 -5.7828 428.7077 434.4905 403.9853 114.7473 -5.7828 428.6072 434.3900 403.7837 116.3425 -5.7816 428.5138 434.2954 403.6056 117.9354 -5.7824 428.4086 434.1910 403.4101 119.5639 -5.7815 428.3080 434.0895 403.1965 121.1629 -5.7806 428.2263 434.0069 403.0224 122.7768 -5.7791 428.1038 433.8830 402.8269 124.3756 -5.7804 428.0110 433.7914 402.6388 125.9746 -5.7781 427.9091 433.6872 402.4660 127.5885 -5.7794 427.8095 433.5888 402.2786 129.2026 -5.7792 427.6893 433.4685 402.0690 130.8016 -5.7780 427.5815 433.3595 401.8826 132.4155 -5.7789 427.4611 433.2400 401.6825 134.0145 -5.7804 427.3480 433.1284 401.4924 135.6449 -5.7824 427.2421 433.0244 401.2769 137.2445 -5.7789 427.1369 432.9158 401.0737 138.8583 -5.7779 427.0187 432.7966 400.8741 140.4568 -5.7795 426.9134 432.6929 400.6675 142.0558 -5.7791 426.7910 432.5701 400.4730 143.6824 -5.7775 426.6731 432.4506 400.2717 145.2734 -5.7761 426.5585 432.3346 400.0783 146.8806 -5.7767 426.4321 432.2088 399.8752 148.4724 -5.7750 426.3137 432.0887 399.6832 150.0805 -5.7747 426.1950 431.9697 399.4857 151.6930 -5.7755 426.0410 431.8166 399.2980 153.2929 -5.7760 425.9096 431.6855 399.1120 154.9088 -5.7756 425.7958 431.5715 398.9175 156.5078 -5.7727 425.6687 431.4414 398.7357 158.1068 -5.7738 425.5410 431.3147 398.5533 159.7359 -5.7724 425.4047 431.1770 398.3497 161.3349 -5.7719 425.2685 431.0404 398.1504 162.9486 -5.7745 425.1549 430.9293 397.9377 164.5478 -5.7732 425.0113 430.7844 397.7372 166.1466 -5.7699 424.8769 430.6468 397.5267 167.7756 -5.7721 424.7427 430.5148 397.3044 169.3895 -5.7702 424.5921 430.3623 397.0988 170.9885 -5.7685 424.4665 430.2350 396.8886 172.5875 -5.7691 424.3333 430.1024 396.6710 174.2021 -5.7668 424.1925 429.9593 396.4676 175.8136 -5.7634 424.0452 429.8086 396.2498 177.4199 -5.7612 423.9084 429.6696 396.0281 179.0113 -5.7605 423.7796 429.5401 395.8146 180.6034 -5.7574 423.6210 429.3783 395.6043 182.2114 -5.7552 423.4879 429.2431 395.3966 183.8353 -5.7539 423.3457 429.0996 395.1884 185.4326 -5.7527 423.1972 428.9499 394.9822 187.0315 -5.7503 423.0520 428.8023 394.7713 188.6305 -5.7473 422.8883 428.6356 394.5718 190.2445 -5.7463 422.7499 428.4962 394.3662 191.8584 -5.7444 422.6040 428.3484 394.1816 193.4724 -5.7428 422.4625 428.2053 393.9692 195.0711 -5.7422 422.3147 428.0569 393.7669 196.6698 -5.7398 422.1587 427.8985 393.5795 198.2838 -5.7359 422.0135 427.7493 393.3817 199.8979 -5.7338 421.8492 427.5829 393.1832 201.4969 -5.7315 421.7073 427.4388 392.9985 203.1106 -5.7313 421.5515 427.2828 392.8011 204.7096 -5.7284 421.3941 427.1226 392.6077 206.3086 -5.7262 421.2403 426.9665 392.4033 207.9340 -5.7213 421.0906 426.8119 392.2120 209.5251 -5.7217 420.9303 426.6520 392.0380 211.1174 -5.7196 420.7804 426.5000 391.8550 212.7246 -5.7181 420.6188 426.3368 391.6635 214.3183 -5.7174 420.4526 426.1700 391.4642 215.9294 -5.7149 420.3059 426.0209 391.2701 217.5426 -5.7107 420.1324 425.8431 391.0661 219.1416 -5.7084 419.9750 425.6834 390.8653 220.7406 -5.7047 419.8117 425.5164 390.6521 222.3395 -5.6984 419.6643 425.3627 390.4465 223.9536 -5.6921 419.5032 425.1953 390.2446 225.5675 -5.6867 419.3293 425.0160 390.0339 227.1815 -5.6839 419.1789 424.8628 389.8406 228.7805 -5.6819 419.0047 424.6866 389.6337 230.3803 -5.6801 418.8295 424.5096 389.4312 231.9804 -5.6764 418.6785 424.3550 389.2183 233.6094 -5.6720 418.5266 424.1986 389.0290 235.2081 -5.6708 418.3374 424.0082 388.8149 236.8228 -5.6679 418.1585 423.8264 388.6080 238.4218 -5.6650 418.0042 423.6691 388.4075 240.0161 -5.6606 417.8407 423.5013 388.2054 241.6373 -5.6583 417.6759 423.3342 388.0049 243.2295 -5.6539 417.5087 423.1626 387.8010 244.8366 -5.6495 417.3219 422.9714 387.6203 246.4286 -5.6467 417.1576 422.8043 387.4168 248.0376 -5.6451 417.0045 422.6496 387.2080 249.6499 -5.6427 416.8379 422.4807 387.0018 251.2489 -5.6399 416.6576 422.2975 386.8006 252.8628 -5.6326 416.4828 422.1154 386.6017 254.4618 -5.6318 416.3075 421.9393 386.4148 256.0606 -5.6320 416.1441 421.7761 386.2134 257.6898 -5.6285 415.9683 421.5968 386.0039 259.2888 -5.6230 415.7913 421.4143 385.8144 260.9026 -5.6196 415.6224 421.2420 385.5784 262.5016 -5.6119 415.4483 421.0602 385.3647 264.1155 -5.6100 415.2732 420.8832 385.1525 265.7295 -5.6042 415.1263 420.7305 384.9319 267.3435 -5.6033 414.9366 420.5400 384.6959 268.9425 -5.5988 414.7576 420.3564 384.4741 270.5415 -5.5928 414.5917 420.1845 384.2421 272.1538 -5.5902 414.3959 419.9861 384.0156 273.7605 -5.5842 414.2231 419.8074 383.8036 275.3665 -5.5828 414.0456 419.6283 383.5763 276.9585 -5.5784 413.8722 419.4506 383.3497 278.5665 -5.5762 413.6855 419.2616 383.1445 280.1600 -5.5748 413.5225 419.0973 382.9267 281.7875 -5.5709 413.3277 418.8985 382.7079 283.3869 -5.5676 413.1595 418.7271 382.4857 284.9865 -5.5664 412.9768 418.5433 382.2660 286.5999 -5.5589 412.7958 418.3547 382.0468 288.1993 -5.5524 412.6227 418.1752 381.8384 289.8280 -5.5467 412.4358 417.9825 381.6037 291.4268 -5.5445 412.2519 417.7964 381.4034 293.0409 -5.5390 412.0719 417.6109 381.1941 294.6398 -5.5357 411.9014 417.4371 380.9780 296.2538 -5.5306 411.7053 417.2359 380.7708 297.8678 -5.5295 411.5092 417.0387 380.5672 299.4819 -5.5241 411.3296 416.8538 380.3525 301.0816 -5.5233 411.1514 416.6747 380.1594 302.6805 -5.5191 410.9595 416.4787 379.9507 304.3084 -5.5152 410.7763 416.2915 379.7403 305.9010 -5.5097 410.5867 416.0965 379.5338 307.5073 -5.5036 410.4120 415.9156 379.3272 309.0994 -5.5024 410.2379 415.7404 379.1408 310.7071 -5.4948 410.0337 415.5286 378.9317 312.3179 -5.4927 409.8375 415.3303 378.7395 313.9155 -5.4875 409.6613 415.1488 378.5463 315.5295 -5.4836 409.4841 414.9677 378.3366 317.1285 -5.4817 409.2984 414.7800 378.1442 318.7275 -5.4802 409.1003 414.5805 377.9503 320.3565 -5.4773 408.9216 414.3989 377.7422 321.9555 -5.4758 408.7402 414.2160 377.5504 323.5695 -5.4724 408.5300 414.0023 377.3513 325.1685 -5.4688 408.3492 413.8181 377.1600 326.7674 -5.4627 408.1580 413.6207 376.9832 328.3861 -5.4589 407.9805 413.4394 376.7765 329.9999 -5.4559 407.7874 413.2433 376.5814 331.5991 -5.4541 407.5990 413.0530 376.4173 333.2148 -5.4472 407.4108 412.8580 376.2102 334.8143 -5.4420 407.2222 412.6642 376.0517 336.4268 -5.4362 407.0440 412.4802 375.8436 338.0333 -5.4303 406.8448 412.2750 375.6797 339.6241 -5.4256 406.6518 412.0774 375.4812 341.2306 -5.4202 406.4600 411.8801 375.2941 342.8238 -5.4180 406.2749 411.6929 375.1024 344.4339 -5.4167 406.0896 411.5063 374.9008 346.0479 -5.4177 405.9034 411.3211 374.6831 347.6475 -5.4146 405.7211 411.1357 374.4873 349.2468 -5.4087 405.5283 410.9370 374.2699 350.8458 -5.4012 405.3212 410.7224 374.0594 352.4596 -5.3926 405.1362 410.5288 373.8460 354.0738 -5.3863 404.9507 410.3369 373.6343 355.6876 -5.3799 404.7530 410.1329 373.4281 357.2869 -5.3782 404.5694 409.9476 373.2289 358.8865 -5.3777 404.3873 409.7650 373.0081 360.5005 -5.3713 404.1906 409.5619 372.7912 362.1145 -5.3656 403.9980 409.3636 372.5943 363.7135 -5.3612 403.8081 409.1693 372.3808 365.3275 -5.3577 403.6211 408.9788 372.1855 366.9263 -5.3568 403.4239 408.7807 371.9902 368.5230 -5.3527 403.2374 408.5901 371.7609 370.1444 -5.3463 403.0309 408.3772 371.5569 371.7359 -5.3442 402.8441 408.1884 371.3578 373.3431 -5.3391 402.6630 408.0021 371.1333 374.9356 -5.3409 402.4570 407.7980 370.9444 376.5314 -5.3396 402.2657 407.6053 370.7387 378.1585 -5.3350 402.0855 407.4205 370.5378 379.7574 -5.3316 401.8972 407.2287 370.3252 381.3564 -5.3271 401.6994 407.0265 370.1314 382.9698 -5.3214 401.5115 406.8328 369.9271 384.5690 -5.3179 401.3163 406.6342 369.7401 386.1843 -5.3109 401.1102 406.4210 369.5141 387.7989 -5.3063 400.9113 406.2175 369.3162 389.3978 -5.3001 400.7234 406.0235 369.1157 391.0121 -5.2994 400.5375 405.8369 368.9064 392.6116 -5.2940 400.3624 405.6564 368.7083 394.2256 -5.2902 400.1589 405.4491 368.5164 395.8406 -5.2837 399.9629 405.2466 368.3175 397.4395 -5.2807 399.7706 405.0513 368.1100 399.0548 -5.2794 399.5797 404.8591 367.8963 400.6549 -5.2744 399.3745 404.6489 367.6844 402.2490 -5.2661 399.1778 404.4439 367.4838 403.8708 -5.2607 398.9908 404.2515 367.2656 405.4639 -5.2563 398.8021 404.0584 367.0467 407.0580 -5.2499 398.6171 403.8670 366.8366 408.6661 -5.2420 398.4061 403.6480 366.6047 410.2635 -5.2367 398.2024 403.4391 366.3990 411.8775 -5.2311 398.0121 403.2433 366.1799 413.4915 -5.2285 397.8253 403.0538 365.9680 415.0905 -5.2252 397.6364 402.8617 365.7604 416.6895 -5.2187 397.4271 402.6458 365.5399 418.3035 -5.2134 397.2290 402.4424 365.3331 419.9175 -5.2092 397.0365 402.2457 365.1064 421.5163 -5.2024 396.8356 402.0381 364.9018 423.1304 -5.1948 396.6468 401.8415 364.6796 424.7288 -5.1898 396.4545 401.6443 364.4698 426.3278 -5.1866 396.2544 401.4410 364.2676 427.9576 -5.1809 396.0549 401.2358 364.0401 429.5569 -5.1755 395.8705 401.0460 363.8439 431.1710 -5.1717 395.6506 400.8223 363.6343 432.7703 -5.1685 395.4579 400.6263 363.4453 434.3788 -5.1612 395.2645 400.4257 363.2259 435.9851 -5.1591 395.0769 400.2360 363.0265 437.5914 -5.1540 394.8781 400.0320 362.8217 439.1834 -5.1497 394.6762 399.8259 362.6049 440.7791 -5.1448 394.4806 399.6254 362.4195 442.3763 -5.1376 394.2953 399.4328 362.2039 444.0056 -5.1314 394.0837 399.2150 361.9985 445.6048 -5.1282 393.8710 398.9992 361.8103 447.2036 -5.1242 393.6864 398.8106 361.6194 448.8026 -5.1205 393.4810 398.6015 361.4061 450.4166 -5.1154 393.2774 398.3928 361.2014 452.0156 -5.1108 393.0900 398.2008 361.0008 453.6304 -5.1080 392.8797 397.9877 360.8092 455.2445 -5.1016 392.6971 397.7987 360.6090 456.8435 -5.0981 392.5077 397.6058 360.3986 458.4425 -5.0918 392.3059 397.3977 360.2114 460.0564 -5.0866 392.0828 397.1695 360.0129 461.6700 -5.0807 391.9186 396.9993 359.8143 463.2843 -5.0765 391.7100 396.7865 359.6257 464.8843 -5.0697 391.5025 396.5722 359.4327 466.4771 -5.0639 391.3014 396.3653 359.2477 468.0685 -5.0583 391.1024 396.1607 359.0568 469.6904 -5.0535 390.8981 395.9516 358.8724 471.2839 -5.0494 390.7075 395.7569 358.6612 472.8920 -5.0469 390.5102 395.5572 358.4553 474.4884 -5.0423 390.3034 395.3457 358.2465 476.0870 -5.0368 390.1251 395.1620 358.0400 477.7161 -5.0314 389.9013 394.9327 357.8330 479.3151 -5.0263 389.7069 394.7331 357.6218 480.9138 -5.0196 389.5264 394.5460 357.4138 482.5278 -5.0127 389.3263 394.3390 357.1962 484.1268 -5.0076 389.1208 394.1284 356.9923 485.7409 -5.0015 388.9350 393.9365 356.7721 487.3998 -4.9962 388.7229 393.7192 356.5511 488.9986 -4.9930 388.5316 393.5246 356.3468 490.5976 -4.9901 388.3147 393.3049 356.1483 492.2266 -4.9855 388.1212 393.1066 355.9347 493.8255 -4.9817 387.9298 392.9115 355.7354 495.4245 -4.9765 387.7298 392.7063 355.5224 497.0375 -4.9701 387.5205 392.4907 355.3194 498.6299 -4.9659 387.3212 392.2871 355.1151 500.2510 -4.9580 387.1200 392.0780 354.8952 501.8424 -4.9565 386.9266 391.8832 354.7005 503.4358 -4.9502 386.7332 391.6834 354.5005 505.0448 -4.9443 386.5240 391.4683 354.2945 506.6405 -4.9448 386.3254 391.2702 354.0852 508.2695 -4.9379 386.1346 391.0725 353.8766 509.8685 -4.9363 385.9249 390.8613 353.6897 511.4675 -4.9327 385.7152 390.6478 353.4878 513.0665 -4.9285 385.5255 390.4541 353.2948 514.6655 -4.9221 385.3187 390.2408 353.1018 516.2944 -4.9149 385.1197 390.0346 352.8866 517.8933 -4.9121 384.9222 389.8343 352.6986 519.4928 -4.9053 384.7256 389.6309 352.5151 521.1068 -4.8978 384.5183 389.4161 352.3166 522.7058 -4.8902 384.3333 389.2235 352.1413 524.3198 -4.8868 384.1361 389.0230 351.9409 525.9346 -4.8828 383.9264 388.8092 351.7397 527.5336 -4.8765 383.7033 388.5798 351.5420 529.1480 -4.8736 383.5056 388.3792 351.3294 530.7443 -4.8726 383.3225 388.1951 351.1393 532.3375 -4.8678 383.1340 388.0018 350.9238 533.9599 -4.8648 382.9198 387.7846 350.7108 535.5526 -4.8595 382.7141 387.5736 350.4883 537.1479 -4.8580 382.5260 387.3840 350.2789 538.7599 -4.8505 382.3231 387.1736 350.0606 540.3584 -4.8432 382.1340 386.9772 349.8527 541.9716 -4.8412 381.9342 386.7754 349.6349 543.5706 -4.8306 381.7204 386.5510 349.4088 545.1845 -4.8260 381.5502 386.3762 349.1849 546.7835 -4.8202 381.3428 386.1630 348.9733 548.3825 -4.8136 381.1335 385.9471 348.7716 550.0115 -4.8087 380.9284 385.7371 348.5516 551.6105 -4.8074 380.7376 385.5450 348.3390 553.2245 -4.8005 380.5310 385.3316 348.1184 554.8235 -4.7966 380.3174 385.1141 347.9079 556.4301 -4.7941 380.1199 384.9141 347.7007 558.0299 -4.7898 379.9256 384.7155 347.4922 559.6590 -4.7868 379.7437 384.5306 347.2800 561.2578 -4.7797 379.5360 384.3157 347.0767 562.8534 -4.7747 379.3327 384.1074 346.8587 564.4596 -4.7698 379.1289 383.8988 346.6585 566.0511 -4.7639 378.9345 383.6984 346.4350 567.6740 -4.7581 378.7155 383.4735 346.2253 569.2680 -4.7499 378.5233 383.2732 346.0343 570.8645 -4.7444 378.3243 383.0686 345.8283 572.4771 -4.7394 378.1107 382.8501 345.6265 574.0758 -4.7343 377.8991 382.6335 345.4059 575.6899 -4.7287 377.7079 382.4366 345.2130 577.3039 -4.7245 377.4985 382.2230 345.0040 578.9028 -4.7215 377.3003 382.0218 344.7961 580.5016 -4.7199 377.1137 381.8336 344.6044 582.1006 -4.7147 376.9151 381.6298 344.3909 583.7296 -4.7096 376.7068 381.4164 344.2002 585.3439 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