DTA measure 33gyors Test Date: 2024220:1555 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.29 s Mass = 1.000 mg data_number = 1023 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4706 -4.2671 407.0375 411.3047 410.0947 4.0826 -4.2669 407.1510 411.4179 410.1151 5.6958 -4.2696 407.1517 411.4213 410.1779 7.2930 -4.2581 407.1751 411.4332 410.0992 8.9515 -4.2673 407.2032 411.4705 410.1282 10.7038 -4.2603 407.2902 411.5505 410.0528 12.3016 -4.2582 407.3251 411.5833 410.0317 13.9131 -4.2405 407.3344 411.5749 409.8884 15.5265 -4.2408 407.4221 411.6629 409.7835 17.1238 -4.2437 407.5045 411.7482 409.6526 18.7215 -4.2307 407.5610 411.7917 409.5204 20.3201 -4.2345 407.6132 411.8477 409.3243 21.9489 -4.2274 407.6327 411.8602 409.1174 23.5479 -4.2361 407.7198 411.9558 408.9810 25.1595 -4.2169 407.6927 411.9096 408.7403 26.7570 -4.2241 407.6643 411.8884 408.5317 28.3536 -4.2134 407.8505 412.0639 408.2832 29.9803 -4.2117 407.8938 412.1056 408.0130 31.5780 -4.2010 407.9028 412.1038 407.9037 33.1776 -4.1915 407.8806 412.0721 407.5917 34.7924 -4.1894 407.9128 412.1022 407.2856 36.3898 -4.1799 407.9683 412.1481 407.0428 37.9878 -4.1717 407.9444 412.1161 406.7930 39.6149 -4.1728 407.9610 412.1339 406.5503 41.2126 -4.1533 408.0386 412.1919 406.3515 42.8106 -4.1511 407.9533 412.1044 406.1044 44.4080 -4.1369 408.1259 412.2629 405.8178 46.0198 -4.1224 408.0820 412.2044 405.5710 47.6319 -4.1174 408.0518 412.1692 405.3312 49.2440 -4.1279 407.9641 412.0919 405.1159 50.8400 -4.0973 408.0190 412.1163 404.9018 52.4388 -4.0949 408.0907 412.1855 404.6236 54.0515 -4.0994 408.0735 412.1729 404.4306 55.6626 -4.0650 408.0593 412.1243 404.2304 57.2593 -4.0656 408.1288 412.1945 403.9653 58.8706 -4.0467 408.0375 412.0843 403.7392 60.5723 -4.0400 408.0331 412.0731 403.4582 62.2721 -4.0283 408.0600 412.0883 403.3582 63.9148 -4.0274 408.1385 412.1659 403.1542 65.5570 -4.0278 408.0610 412.0888 402.9936 67.1688 -4.0134 407.9809 411.9943 402.7880 68.7810 -4.0044 407.9639 411.9682 402.6047 70.3824 -4.0057 407.9124 411.9181 402.4572 71.9761 -3.9693 407.9062 411.8756 402.2987 73.5895 -3.9521 407.9028 411.8549 402.1290 75.1878 -3.9518 407.8947 411.8464 401.9277 76.8014 -3.9450 407.8159 411.7609 401.8160 78.4133 -3.9462 407.8228 411.7690 401.6295 80.0105 -3.9189 407.8099 411.7289 401.3993 81.6136 -3.9171 407.7153 411.6324 401.2225 83.2210 -3.9082 407.6435 411.5517 400.9805 84.8338 -3.9048 407.6182 411.5230 400.8866 86.4316 -3.8834 407.6300 411.5134 400.6680 88.0283 -3.8731 407.6200 411.4931 400.5082 89.6403 -3.8658 407.5863 411.4521 400.3375 91.2760 -3.8549 407.5361 411.3911 400.1407 92.8521 -3.8363 407.4721 411.3084 399.9472 94.4476 -3.8356 407.4093 411.2449 399.6606 96.0748 -3.8340 407.3471 411.1811 399.4855 97.6725 -3.8340 407.3686 411.2026 399.3069 99.2844 -3.8187 407.2907 411.1094 399.1211 100.9064 -3.8165 407.2612 411.0777 398.9351 102.6781 -3.8008 407.2091 411.0099 398.6994 104.3041 -3.7947 407.0828 410.8775 398.5521 105.9025 -3.7886 407.0565 410.8451 398.3321 107.5000 -3.7873 406.9752 410.7625 398.0968 109.1124 -3.7731 406.9157 410.6888 398.0033 110.7091 -3.7740 406.8761 410.6501 397.6869 112.5049 -3.7538 406.8057 410.5595 397.5904 114.1351 -3.7598 406.6376 410.3974 397.3358 115.7328 -3.7396 406.6870 410.4266 397.1112 117.3451 -3.7382 406.6416 410.3798 396.9412 118.9578 -3.7295 406.5594 410.2888 396.7280 120.5563 -3.7292 406.4417 410.1709 396.5323 122.1538 -3.7311 406.2763 410.0074 396.2898 123.7501 -3.7172 406.2848 410.0019 396.0964 125.3779 -3.7069 406.1506 409.8575 395.8672 126.9754 -3.6932 406.0908 409.7840 395.6032 128.5736 -3.6837 406.0817 409.7654 395.4724 130.1868 -3.6870 405.9497 409.6367 395.2962 131.7846 -3.6800 405.8688 409.5488 395.0885 133.3818 -3.6668 405.7894 409.4562 394.9397 135.0095 -3.6546 405.7324 409.3870 394.6989 136.6070 -3.6508 405.5584 409.2092 394.4577 138.2044 -3.6432 405.5778 409.2210 394.2772 139.8159 -3.6442 405.4250 409.0692 394.0757 141.4128 -3.6360 405.3759 409.0119 393.8611 143.2050 -3.6300 405.2722 408.9022 393.6631 144.8243 -3.6223 405.1351 408.7574 393.4367 146.4368 -3.6204 405.0946 408.7150 393.2251 148.0346 -3.6103 404.9962 408.6065 393.1253 149.6476 -3.5885 404.8344 408.4230 392.9143 151.2596 -3.5752 404.7690 408.3442 392.7258 152.8580 -3.5771 404.6274 408.2045 392.5323 154.4596 -3.5599 404.5683 408.1282 392.3095 156.0594 -3.5654 404.4347 408.0001 392.0691 157.6710 -3.5444 404.3238 407.8682 391.9205 159.2821 -3.5336 404.2229 407.7564 391.7391 160.8803 -3.5165 404.1260 407.6425 391.5559 162.4784 -3.5191 404.0096 407.5287 391.3058 164.0898 -3.5176 403.8626 407.3801 391.1625 165.6996 -3.5194 403.7743 407.2937 390.9152 167.3103 -3.4907 403.7409 407.2316 390.6433 168.9069 -3.4853 403.6032 407.0885 390.4781 170.5165 -3.4943 403.4684 406.9627 390.3814 172.1148 -3.4607 403.3819 406.8425 390.1615 173.7263 -3.4677 403.2915 406.7592 389.9503 175.3378 -3.4801 403.1933 406.6735 389.6906 176.9341 -3.4759 403.0806 406.5565 389.5997 178.5465 -3.4736 402.8856 406.3592 389.2752 180.1444 -3.4593 402.8370 406.2964 389.1281 181.7559 -3.4333 402.6821 406.1154 388.8816 183.3679 -3.4314 402.5190 405.9504 388.6940 184.9791 -3.4385 402.4820 405.9204 388.5723 186.5764 -3.4298 402.3587 405.7885 388.3237 188.1719 -3.4041 402.2697 405.6738 388.1835 189.7976 -3.4152 402.1278 405.5430 387.9773 191.3959 -3.4219 401.9853 405.4073 387.7346 192.9929 -3.4196 401.8160 405.2356 387.5248 194.6055 -3.3985 401.7330 405.1314 387.3147 196.2036 -3.3967 401.5747 404.9714 387.0981 197.8006 -3.4061 401.4139 404.8200 386.8713 199.4271 -3.3849 401.3596 404.7445 386.7464 201.0239 -3.3756 401.2659 404.6415 386.5593 202.6209 -3.3657 401.0465 404.4122 386.3043 204.2318 -3.3576 400.9124 404.2700 386.0705 205.8425 -3.3383 400.7998 404.1381 385.9126 207.4531 -3.3256 400.7038 404.0294 385.7130 209.0504 -3.3258 400.5130 403.8388 385.5038 210.6608 -3.3266 400.3898 403.7164 385.2990 212.2574 -3.3151 400.2451 403.5602 385.0785 213.8694 -3.3198 400.1064 403.4262 384.8853 215.4808 -3.3069 399.9092 403.2161 384.6455 217.0789 -3.3094 399.8314 403.1408 384.4801 218.6766 -3.3037 399.7472 403.0509 384.3088 220.2900 -3.2899 399.5400 402.8299 384.0733 221.8860 -3.2921 399.4697 402.7619 383.8101 223.5134 -3.2828 399.2349 402.5177 383.6676 225.1100 -3.2735 399.1107 402.3843 383.4517 226.7070 -3.2782 398.9664 402.2446 383.2737 228.3041 -3.2605 398.7654 402.0259 383.0138 229.9163 -3.2682 398.6856 401.9537 382.9008 231.5291 -3.2596 398.5409 401.8004 382.6220 233.1418 -3.2652 398.4076 401.6728 382.4557 234.7381 -3.2426 398.3080 401.5506 382.2769 236.3344 -3.2266 398.1680 401.3946 382.0367 237.9465 -3.2293 398.0089 401.2381 381.8550 239.5586 -3.2257 397.8204 401.0462 381.7006 241.1708 -3.2121 397.6856 400.8977 381.4857 242.7676 -3.2177 397.5486 400.7663 381.2653 244.3655 -3.2159 397.3402 400.5561 381.0837 245.9626 -3.2087 397.2176 400.4262 380.8965 247.5894 -3.1958 397.0967 400.2926 380.6577 249.3066 -3.1973 396.9631 400.1603 380.4029 250.9780 -3.1966 396.7114 399.9080 380.1904 252.5919 -3.1855 396.6132 399.7986 379.9724 254.1899 -3.1857 396.4793 399.6650 379.8261 255.7879 -3.1809 396.3014 399.4824 379.6680 257.4600 -3.1774 396.1237 399.3011 379.3873 259.1610 -3.1786 396.0134 399.1920 379.1429 260.7729 -3.1558 395.8664 399.0222 378.9297 262.3701 -3.1557 395.6004 398.7561 378.7042 263.9670 -3.1520 395.5378 398.6898 378.5793 265.5935 -3.1432 395.3632 398.5064 378.3628 267.2053 -3.1300 395.2239 398.3540 378.0764 268.8025 -3.1265 395.0851 398.2116 377.9139 270.4006 -3.1241 394.7941 397.9182 377.8178 271.9986 -3.1290 394.6600 397.7891 377.5790 273.6258 -3.1142 394.5856 397.6998 377.3551 275.2101 -3.1040 394.4441 397.5481 377.1899 276.8143 -3.0980 394.2599 397.3579 377.0005 278.4421 -3.0941 393.9953 397.0894 376.8154 280.0421 -3.0893 393.9560 397.0454 376.6011 281.6398 -3.1045 393.7553 396.8598 376.3324 283.2516 -3.0853 393.6209 396.7062 376.1200 284.8471 -3.0842 393.4277 396.5119 376.0136 286.4724 -3.0711 393.2286 396.2997 375.7761 288.0700 -3.0620 393.1038 396.1658 375.5573 289.6679 -3.0479 393.0280 396.0759 375.3082 291.2794 -3.0512 392.8550 395.9062 375.1307 292.8773 -3.0523 392.6679 395.7202 374.8067 294.4740 -3.0441 392.4043 395.4484 374.6819 296.0883 -3.0450 392.1802 395.2251 374.5255 297.7046 -3.0438 392.0349 395.0787 374.3280 299.3018 -3.0387 391.9235 394.9622 374.0877 300.9139 -3.0214 391.7863 394.8078 373.9472 302.5128 -3.0257 391.6024 394.6281 373.7134 304.1104 -3.0204 391.4175 394.4380 373.4388 305.7164 -2.9980 391.2925 394.2905 373.1966 307.3201 -2.9876 391.0922 394.0798 373.0267 308.9321 -2.9844 390.9568 393.9412 372.8683 310.5288 -2.9829 390.7161 393.6990 372.7063 312.1565 -2.9818 390.6086 393.5903 372.3824 313.7541 -2.9774 390.3902 393.3677 372.2019 315.3496 -2.9667 390.1978 393.1645 372.0019 316.9463 -2.9669 390.1118 393.0787 371.8310 318.5781 -2.9765 389.9529 392.9294 371.6028 320.1753 -2.9568 389.6935 392.6503 371.3904 321.7718 -2.9442 389.5989 392.5430 371.2464 323.3824 -2.9446 389.3189 392.2635 370.9430 324.9946 -2.9265 389.2147 392.1411 370.7707 326.5923 -2.9248 389.0356 391.9604 370.6468 328.1944 -2.9318 388.8991 391.8309 370.3664 329.8224 -2.9149 388.8008 391.7157 370.1446 331.4200 -2.9284 388.3986 391.3270 369.9507 333.0334 -2.9233 388.2507 391.1740 369.7870 334.6345 -2.9015 388.1580 391.0594 369.5726 336.2315 -2.8987 387.9921 390.8908 369.3819 337.8409 -2.8934 387.8571 390.7506 369.2085 339.4445 -2.8865 387.6427 390.5291 368.9628 341.0579 -2.8938 387.4159 390.3097 368.7576 342.6548 -2.8938 387.2920 390.1859 368.5777 344.2669 -2.8838 387.1301 390.0139 368.3889 345.8798 -2.8812 386.9953 389.8764 368.2169 347.4618 -2.8665 386.7652 389.6316 367.9789 349.0853 -2.8665 386.5507 389.4172 367.7624 350.6976 -2.8786 386.3824 389.2610 367.5710 352.2949 -2.8803 386.2383 389.1187 367.4015 353.8924 -2.8540 386.0061 388.8602 367.2493 355.4890 -2.8487 385.8378 388.6865 366.9973 357.1203 -2.8483 385.6654 388.5136 366.8698 358.7163 -2.8386 385.5644 388.4030 366.5547 360.3144 -2.8420 385.3165 388.1584 366.3559 361.9118 -2.8295 385.1734 388.0028 366.1510 363.5385 -2.8158 385.0063 387.8220 365.9406 365.1333 -2.8190 384.8238 387.6429 365.7925 366.7314 -2.8170 384.6770 387.4940 365.5931 368.3385 -2.7992 384.4866 387.2858 365.3666 369.9463 -2.8140 384.2653 387.0793 365.1617 371.5435 -2.8169 384.0431 386.8600 364.9820 373.1558 -2.8027 383.9030 386.7057 364.7734 374.7523 -2.7869 383.7579 386.5448 364.4978 376.3644 -2.7797 383.5713 386.3510 364.3239 377.9853 -2.7772 383.3568 386.1340 364.1487 379.5763 -2.7749 383.2190 385.9940 363.9024 381.1736 -2.7795 383.0052 385.7847 363.7343 382.7995 -2.7739 382.8603 385.6342 363.5167 384.3969 -2.7644 382.6734 385.4378 363.3187 385.9936 -2.7560 382.4171 385.1731 363.0442 387.6015 -2.7505 382.3324 385.0828 362.7791 389.2111 -2.7410 382.1544 384.8954 362.5131 390.8229 -2.7284 381.9505 384.6788 362.2640 392.4213 -2.7216 381.8071 384.5287 362.0132 394.0179 -2.7158 381.6300 384.3459 361.9036 395.6440 -2.7031 381.4099 384.1130 361.6757 397.2550 -2.7058 381.1675 383.8733 361.3446 398.8488 -2.7008 381.0737 383.7745 361.1314 400.4669 -2.6954 380.7908 383.4862 361.0451 402.0651 -2.6882 380.6341 383.3222 360.7845 403.6621 -2.6963 380.4837 383.1799 360.5567 405.2735 -2.6939 380.3045 382.9985 360.5768 406.8704 -2.6939 380.1241 382.8179 360.4576 408.4790 -2.6761 379.8728 382.5489 360.2190 410.0779 -2.6801 379.6903 382.3704 360.1038 411.6905 -2.7060 379.4823 382.1883 359.9245 413.3031 -2.7123 379.3499 382.0623 359.6707 414.8995 -2.7212 379.2175 381.9387 359.4713 416.4971 -2.7192 378.9343 381.6535 359.3030 418.1084 -2.7161 378.7510 381.4671 359.0551 419.7331 -2.7142 378.6086 381.3228 359.0027 421.3295 -2.6987 378.4529 381.1517 358.8895 422.9250 -2.6815 378.2015 380.8830 358.5981 424.5383 -2.6674 378.0402 380.7076 358.3366 426.1336 -2.6723 377.7958 380.4681 358.2786 427.7596 -2.6575 377.6497 380.3072 358.0952 429.3566 -2.6571 377.5336 380.1907 357.8840 430.9538 -2.6540 377.3418 379.9958 357.6883 432.5515 -2.6389 377.1585 379.7974 357.4654 434.1613 -2.6344 376.9986 379.6330 357.2428 435.7730 -2.6354 376.7946 379.4300 356.9945 437.3833 -2.6266 376.6135 379.2401 356.7218 439.0230 -2.6125 376.4007 379.0132 356.4338 440.7815 -2.6125 376.1805 378.7931 356.2507 442.3925 -2.5870 376.0306 378.6176 355.9464 444.0038 -2.6042 375.8329 378.4370 355.8358 445.6008 -2.6010 375.6883 378.2893 355.5723 447.1975 -2.5946 375.3477 377.9423 355.3097 448.8059 -2.5890 375.2531 377.8421 355.1088 450.4310 -2.5833 375.0540 377.6373 355.0272 452.0266 -2.5821 374.8577 377.4398 354.7786 453.6218 -2.5648 374.6504 377.2152 354.5193 455.2334 -2.5740 374.5612 377.1352 354.3644 456.8283 -2.5620 374.3001 376.8621 354.1342 458.4548 -2.5534 374.1205 376.6739 353.9430 460.0520 -2.5656 373.8641 376.4297 353.7195 461.6478 -2.5523 373.6286 376.1809 353.4987 463.2600 -2.5541 373.5009 376.0550 353.2075 464.8694 -2.5482 373.4010 375.9492 353.0621 466.4803 -2.5428 373.1670 375.7097 352.8136 468.0780 -2.5390 372.9798 375.5188 352.5923 469.7389 -2.5284 372.7270 375.2554 352.4843 471.4869 -2.5161 372.5264 375.0425 352.3399 473.0980 -2.5062 372.3812 374.8874 352.0210 474.7076 -2.5041 372.1651 374.6692 351.7434 476.3036 -2.4961 371.9968 374.4929 351.5369 477.9148 -2.5103 371.7211 374.2314 351.3923 479.5109 -2.4883 371.6124 374.1007 351.1476 481.1373 -2.4836 371.4274 373.9110 350.9343 482.7341 -2.4881 371.2399 373.7279 350.7287 484.3469 -2.4865 370.9847 373.4712 350.5423 485.9441 -2.4903 370.8582 373.3485 350.3897 487.5400 -2.4736 370.6723 373.1459 350.1267 489.1664 -2.4580 370.4682 372.9261 349.9377 490.7616 -2.4570 370.2734 372.7304 349.7689 492.3736 -2.4561 370.0696 372.5256 349.5357 493.9703 -2.4453 369.8402 372.2855 349.3147 495.5681 -2.4429 369.7251 372.1681 349.1125 497.1956 -2.4434 369.5009 371.9443 348.9188 498.7904 -2.4399 369.3333 371.7732 348.6227 500.4489 -2.4323 369.0718 371.5040 348.5630 502.2054 -2.4382 369.0198 371.4580 348.2971 503.8033 -2.4413 368.7381 371.1794 348.1542 505.4316 -2.4304 368.5490 370.9794 347.8287 507.0280 -2.4242 368.3210 370.7451 347.6834 508.6236 -2.4157 368.1999 370.6156 347.4333 510.2359 -2.4015 367.9807 370.3822 347.3058 511.8316 -2.3949 367.7274 370.1223 347.0506 513.4595 -2.3952 367.5355 369.9306 346.9141 515.0560 -2.3914 367.4212 369.8125 346.6759 516.6504 -2.4095 367.1086 369.5181 346.6415 518.2620 -2.3816 366.9515 369.3331 346.3438 519.8584 -2.3686 366.8267 369.1953 345.9905 521.4849 -2.3761 366.6405 369.0166 345.8850 523.0824 -2.3596 366.3555 368.7151 345.5970 524.6770 -2.3462 366.2239 368.5701 345.4379 526.2891 -2.3563 365.9900 368.3463 345.2236 527.8850 -2.3543 365.8040 368.1582 345.0556 529.5124 -2.3482 365.6460 367.9942 344.8823 531.1570 -2.3450 365.4644 367.8094 344.6842 532.9085 -2.3447 365.2144 367.5590 344.3632 534.5044 -2.3530 365.0096 367.3625 344.3247 536.1319 -2.3614 364.7956 367.1570 344.1105 537.7274 -2.3510 364.6072 366.9582 343.8225 539.3383 -2.3497 364.3967 366.7464 343.6194 540.9355 -2.3419 364.1617 366.5035 343.4023 542.5329 -2.3471 364.0141 366.3612 343.2265 544.1608 -2.3357 363.6685 366.0042 343.0438 545.7566 -2.3267 363.5337 365.8604 342.8736 547.3685 -2.3263 363.4483 365.7747 342.5589 548.9648 -2.3125 363.1745 365.4870 342.4513 550.5609 -2.3143 362.9432 365.2576 342.3375 552.1898 -2.3208 362.6933 365.0141 342.1365 553.7868 -2.3176 362.5960 364.9136 341.8580 555.3830 -2.2947 362.3750 364.6698 341.6650 556.9928 -2.2894 362.1433 364.4328 341.5186 558.5899 -2.2937 361.9198 364.2136 341.2480 560.2171 -2.2864 361.6097 363.8961 341.0857 561.8129 -2.2910 361.4617 363.7527 340.9504 563.4091 -2.2898 361.1545 363.4443 340.6353 565.0185 -2.2800 360.9724 363.2524 340.3984 566.6151 -2.2810 360.8007 363.0817 340.3058 568.2414 -2.2742 360.6421 362.9164 340.1252 569.8380 -2.2708 360.3655 362.6364 339.9440 571.4355 -2.2586 360.2679 362.5265 339.6544 573.0454 -2.2634 360.1139 362.3774 339.4471 574.6404 -2.2670 359.9103 362.1774 339.2222 576.2520 -2.2549 359.7631 362.0180 338.9382 577.8633 -2.2297 359.5829 361.8127 338.5731 579.4610 -2.2246 359.3874 361.6120 338.2810 581.0734 -2.2124 359.1586 361.3709 337.9894 582.6704 -2.2017 358.9467 361.1485 337.7122 584.2828 -2.2191 358.7550 360.9742 337.4943 585.8949 -2.1890 358.5189 360.7079 337.3113 587.4925 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