DTA measure 1pb_updown3.dat Date: 2024319:1322 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 968.07 s Mass = 1129.000 mg data_number = 1205 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1405 -4.8013 440.0588 444.8601 439.1935 1.9618 -4.8000 440.0823 444.8823 439.1779 2.7523 -4.7970 440.0830 444.8800 439.2035 3.5435 -4.8001 440.0694 444.8694 439.1957 4.3653 -4.8001 440.0857 444.8858 439.1865 5.1560 -4.8024 440.0939 444.8963 439.1860 5.9770 -4.8044 440.0781 444.8825 439.1955 6.7665 -4.8008 440.0869 444.8878 439.1880 7.5570 -4.8019 440.0879 444.8899 439.1957 8.3790 -4.8007 440.0984 444.8991 439.1676 9.1703 -4.8005 440.0783 444.8787 439.1647 9.9905 -4.7998 440.0907 444.8905 439.1704 10.7843 -4.7983 440.0983 444.8966 439.2056 11.5758 -4.7999 440.0922 444.8921 439.1937 12.3963 -4.8003 440.0898 444.8902 439.1844 13.1575 -4.8019 440.0901 444.8920 439.1698 14.0100 -4.8036 440.0873 444.8909 439.1800 14.8015 -4.8045 440.0941 444.8986 439.1831 15.5930 -4.8059 440.1004 444.9063 439.1707 16.4155 -4.7997 440.0818 444.8815 439.1680 17.1765 -4.8015 440.0738 444.8753 439.1763 18.0278 -4.7832 440.1121 444.8954 439.1881 18.7898 -4.7844 440.1050 444.8894 439.1778 19.6120 -4.8041 440.0872 444.8913 439.1826 20.4335 -4.8090 440.0907 444.8997 439.1750 21.1945 -4.7982 440.1148 444.9130 439.1827 22.0458 -4.8006 440.1018 444.9024 439.1824 22.8075 -4.8089 440.1125 444.9214 439.1929 23.6280 -4.8077 440.1005 444.9082 439.1839 24.4195 -4.8073 440.1141 444.9214 439.1875 25.2115 -4.8072 440.1074 444.9146 439.1850 26.0638 -4.7992 440.0974 444.8966 439.2011 26.8238 -4.8016 440.1030 444.9045 439.2024 27.6455 -4.8078 440.0919 444.8997 439.2015 28.4418 -4.8086 440.1004 444.9090 439.1912 29.2340 -4.8048 440.0984 444.9031 439.1730 30.0563 -4.8061 440.1093 444.9154 439.1932 30.8170 -4.8113 440.1174 444.9286 439.1984 31.6688 -4.8054 440.1140 444.9194 439.1852 32.4583 -4.8067 440.0880 444.8946 439.2005 33.2480 -4.8108 440.1042 444.9151 439.2108 34.0690 -4.8161 440.1219 444.9380 439.2159 34.8298 -4.8169 440.1106 444.9275 439.2168 35.6810 -4.8140 440.1142 444.9282 439.2332 36.4720 -4.8085 440.1310 444.9395 439.2449 37.2623 -4.8067 440.1223 444.9290 439.2418 38.0840 -4.8092 440.1196 444.9288 439.2573 38.8438 -4.8083 440.1171 444.9254 439.2467 39.6945 -4.8097 440.1507 444.9605 439.2528 40.4848 -4.8023 440.1404 444.9426 439.2609 41.2763 -4.8073 440.1139 444.9212 439.2734 42.0968 -4.8069 440.1139 444.9208 439.2831 42.8585 -4.8067 440.1250 444.9316 439.2805 43.7093 -4.8094 440.1228 444.9321 439.2905 44.4988 -4.8125 440.1235 444.9360 439.3046 45.2905 -4.8133 440.1220 444.9353 439.3080 46.1125 -4.8096 440.1110 444.9207 439.3136 46.8745 -4.8154 440.1290 444.9445 439.3210 47.7265 -4.8144 440.1286 444.9430 439.3325 48.4878 -4.8140 440.1225 444.9365 439.3451 49.3080 -4.8116 440.1302 444.9418 439.3439 50.0933 -4.8104 440.1358 444.9462 439.3288 50.9265 -4.8090 440.1434 444.9524 439.3457 51.7168 -4.8102 440.1333 444.9434 439.3648 52.5070 -4.8109 440.1382 444.9491 439.3667 53.3285 -4.8094 440.1479 444.9574 439.3791 54.1198 -4.8083 440.1441 444.9524 439.3801 54.9405 -4.8097 440.1488 444.9585 439.3959 55.7315 -4.8105 440.1481 444.9586 439.3975 56.5210 -4.8068 440.1415 444.9483 439.3819 57.3723 -4.8006 440.1495 444.9501 439.3833 58.1313 -4.8033 440.1560 444.9592 439.3862 58.9518 -4.8088 440.1484 444.9573 439.3860 59.7438 -4.8108 440.1442 444.9550 439.4017 60.5363 -4.8119 440.1458 444.9577 439.4086 61.3888 -4.8107 440.1379 444.9486 439.4089 62.1478 -4.8130 440.1478 444.9608 439.4176 62.9688 -4.8123 440.1397 444.9519 439.4210 63.7603 -4.8093 440.1657 444.9750 439.4058 64.5503 -4.8091 440.1697 444.9788 439.4196 65.4018 -4.8119 440.1648 444.9767 439.4593 66.1625 -4.8138 440.1358 444.9495 439.4443 66.9840 -4.8104 440.1431 444.9536 439.4308 67.7755 -4.8117 440.1588 444.9705 439.4177 68.5668 -4.8097 440.1674 444.9771 439.4344 69.3880 -4.8099 440.1619 444.9718 439.4253 70.1785 -4.8104 440.1549 444.9653 439.4340 71.0000 -4.8110 440.1539 444.9649 439.4252 71.7915 -4.7911 440.1655 444.9566 439.4348 72.5830 -4.7935 440.1761 444.9697 439.4488 73.4040 -4.8038 440.1703 444.9741 439.4502 74.1948 -4.8072 440.1901 444.9973 439.4563 75.0165 -4.8049 440.1765 444.9814 439.4530 75.8083 -4.8049 440.1763 444.9813 439.4555 76.5990 -4.8091 440.1684 444.9775 439.4886 77.4205 -4.8060 440.1704 444.9764 439.4800 78.2125 -4.8004 440.1801 444.9805 439.4784 79.0335 -4.8003 440.1832 444.9835 439.4757 79.8245 -4.8033 440.1759 444.9792 439.4894 80.6148 -4.8025 440.1609 444.9634 439.4940 81.4353 -4.8062 440.1738 444.9800 439.5001 82.1968 -4.8070 440.1830 444.9900 439.4912 83.0488 -4.8040 440.1661 444.9701 439.4896 83.8400 -4.8051 440.1736 444.9787 439.4924 84.6313 -4.8082 440.1851 444.9933 439.5125 85.4530 -4.8010 440.1908 444.9918 439.5099 86.2140 -4.7989 440.1885 444.9874 439.5371 87.0660 -4.8060 440.1891 444.9951 439.5091 87.8580 -4.8085 440.1814 444.9899 439.4916 88.6485 -4.8063 440.1812 444.9875 439.5091 89.4698 -4.8067 440.2014 445.0081 439.5009 90.2315 -4.8073 440.2016 445.0090 439.5231 91.0833 -4.8068 440.2103 445.0170 439.5207 91.8728 -4.8098 440.1946 445.0045 439.5134 92.6645 -4.8072 440.1787 444.9859 439.5110 93.4865 -4.8063 440.1886 444.9948 439.5196 94.2483 -4.8094 440.1909 445.0003 439.5317 95.0988 -4.8143 440.2075 445.0218 439.5439 95.8598 -4.8162 440.2083 445.0245 439.5736 96.6815 -4.8158 440.1933 445.0091 439.5691 97.5035 -4.8127 440.2034 445.0161 439.5569 98.2655 -4.8132 440.1987 445.0119 439.5410 99.1165 -4.8138 440.2183 445.0321 439.5360 99.8775 -4.8174 440.2362 445.0536 439.5256 100.6995 -4.8179 440.2186 445.0365 439.5447 101.4985 -4.8147 440.2206 445.0354 439.5615 102.2925 -4.8145 440.2209 445.0355 439.5598 103.1145 -4.8157 440.2285 445.0442 439.5579 103.8765 -4.8162 440.2337 445.0500 439.5723 104.7288 -4.8195 440.2367 445.0562 439.5588 105.5185 -4.8216 440.2311 445.0527 439.5578 106.3095 -4.8212 440.2312 445.0524 439.5594 107.1313 -4.8178 440.2113 445.0291 439.5636 107.8928 -4.8192 440.2304 445.0496 439.5588 108.7448 -4.8251 440.2494 445.0745 439.5584 109.5058 -4.8231 440.2241 445.0473 439.5417 110.3278 -4.8221 440.2368 445.0589 439.5480 111.1500 -4.8215 440.2612 445.0827 439.5598 111.9108 -4.8233 440.2436 445.0669 439.5470 112.7630 -4.8255 440.2402 445.0657 439.5503 113.5240 -4.8255 440.2440 445.0696 439.5620 114.3448 -4.8224 440.2298 445.0522 439.5606 115.1368 -4.8214 440.2405 445.0620 439.5631 115.9285 -4.8207 440.2401 445.0607 439.5699 116.7505 -4.8221 440.2515 445.0736 439.5717 117.5425 -4.8232 440.2580 445.0812 439.5704 118.3643 -4.8245 440.2668 445.0912 439.5700 119.1555 -4.8233 440.2474 445.0707 439.5631 119.9475 -4.8250 440.2692 445.0942 439.5869 120.7695 -4.8231 440.2502 445.0733 439.5837 121.5470 -4.8247 440.2618 445.0865 439.5649 122.3840 -4.8235 440.2427 445.0662 439.5649 123.1458 -4.8252 440.2341 445.0592 439.5670 123.9985 -4.8229 440.2530 445.0759 439.5673 124.7603 -4.8255 440.2450 445.0705 439.5665 125.5805 -4.8220 440.2581 445.0801 439.5519 126.3725 -4.8221 440.2482 445.0703 439.5640 127.1638 -4.8239 440.2592 445.0831 439.5589 128.0155 -4.8203 440.2695 445.0898 439.5707 128.7775 -4.8206 440.2667 445.0873 439.5684 129.5975 -4.8241 440.2737 445.0977 439.5987 130.3885 -4.8208 440.2724 445.0932 439.5830 131.1803 -4.8193 440.2778 445.0971 439.5814 132.0320 -4.8173 440.2505 445.0678 439.5765 132.7940 -4.8186 440.2609 445.0795 439.5890 133.6158 -4.8193 440.2853 445.1046 439.5969 134.4075 -4.8169 440.2860 445.1029 439.6042 135.1985 -4.8209 440.2731 445.0939 439.6008 136.0213 -4.8171 440.3003 445.1174 439.5972 136.8128 -4.8185 440.3068 445.1252 439.5933 137.6348 -4.8143 440.2939 445.1083 439.5758 138.4270 -4.8168 440.2932 445.1100 439.5779 139.2178 -4.8205 440.2918 445.1123 439.5830 140.0390 -4.8190 440.3102 445.1292 439.5829 140.7995 -4.8195 440.3003 445.1198 439.5855 141.6515 -4.8180 440.3037 445.1216 439.5973 142.4290 -4.8167 440.3081 445.1247 439.5746 143.2553 -4.8151 440.3034 445.1185 439.5638 144.0458 -4.8135 440.2915 445.1050 439.5716 144.8360 -4.8158 440.2969 445.1127 439.5533 145.6570 -4.8173 440.3139 445.1312 439.5441 146.4478 -4.8159 440.3048 445.1207 439.5245 147.2683 -4.8150 440.3163 445.1313 439.5141 148.0588 -4.8127 440.3221 445.1349 439.5088 148.8483 -4.8120 440.3181 445.1301 439.5201 149.6698 -4.8124 440.3108 445.1231 439.5293 150.4598 -4.8103 440.3139 445.1243 439.5196 151.2810 -4.8105 440.3157 445.1262 439.5027 152.0720 -4.8125 440.3229 445.1354 439.4965 152.8628 -4.8105 440.3136 445.1242 439.4884 153.6850 -4.8087 440.3125 445.1211 439.5000 154.4775 -4.8093 440.3259 445.1351 439.4695 155.3048 -4.8019 440.3222 445.1241 439.4805 156.0973 -4.7976 440.3239 445.1215 439.4574 156.8880 -4.7984 440.3242 445.1226 439.4527 157.7083 -4.8024 440.3247 445.1271 439.4421 158.4695 -4.8036 440.3252 445.1288 439.4508 159.3218 -4.8037 440.3144 445.1181 439.4270 160.0823 -4.7938 440.3528 445.1466 439.4200 160.9033 -4.7862 440.3451 445.1313 439.4184 161.7248 -4.7913 440.3225 445.1138 439.4181 162.5003 -4.7943 440.3378 445.1321 439.4171 163.3055 -4.7967 440.3344 445.1311 439.4267 164.0965 -4.7995 440.3312 445.1306 439.4188 164.9490 -4.7984 440.3328 445.1312 439.4212 165.7085 -4.7992 440.3422 445.1414 439.4056 166.5295 -4.7993 440.3281 445.1274 439.3987 167.3215 -4.8007 440.3318 445.1326 439.4019 168.1135 -4.7980 440.3544 445.1524 439.4045 168.9648 -4.7997 440.3509 445.1506 439.3985 169.7275 -4.8010 440.3399 445.1409 439.4398 170.5495 -4.7992 440.3440 445.1432 439.4275 171.3410 -4.7948 440.3337 445.1285 439.4320 172.1313 -4.7946 440.3207 445.1153 439.4246 172.9525 -4.7947 440.3293 445.1240 439.4173 173.7135 -4.7956 440.3350 445.1306 439.4160 174.5655 -4.7994 440.3435 445.1429 439.3998 175.3565 -4.8000 440.3483 445.1483 439.4022 176.1485 -4.7994 440.3474 445.1468 439.4136 176.9700 -4.8001 440.3610 445.1611 439.4130 177.7303 -4.8017 440.3598 445.1616 439.4233 178.5813 -4.8027 440.3447 445.1474 439.4323 179.3725 -4.8020 440.3401 445.1421 439.4325 180.1645 -4.8011 440.3570 445.1581 439.4395 180.9863 -4.8036 440.3214 445.1250 439.4190 181.7473 -4.8052 440.3427 445.1479 439.4463 182.5990 -4.8056 440.3666 445.1721 439.4506 183.3503 -4.8101 440.3767 445.1869 439.4504 184.2070 -4.8074 440.3589 445.1662 439.4531 184.9678 -4.7888 440.3507 445.1395 439.4600 185.7895 -4.7974 440.3643 445.1617 439.5051 186.5810 -4.7994 440.3663 445.1657 439.4815 187.3725 -4.8032 440.3586 445.1618 439.4743 188.2248 -4.7936 440.3502 445.1438 439.4934 188.9848 -4.8014 440.3516 445.1530 439.4931 189.8065 -4.8027 440.3425 445.1452 439.5072 190.5978 -4.8061 440.3638 445.1699 439.4927 191.3895 -4.7984 440.3648 445.1632 439.5080 192.2415 -4.8004 440.3597 445.1601 439.5174 193.0028 -4.7974 440.3535 445.1510 439.5101 193.8253 -4.8066 440.3585 445.1651 439.5123 194.6163 -4.8025 440.3613 445.1638 439.5169 195.4075 -4.8061 440.3568 445.1629 439.5152 196.2295 -4.8000 440.3677 445.1677 439.5174 197.0205 -4.8046 440.3679 445.1725 439.5120 197.8425 -4.8070 440.3683 445.1753 439.5427 198.6088 -4.8068 440.3645 445.1713 439.5441 199.4320 -4.8087 440.3529 445.1616 439.5491 200.2525 -4.8080 440.3498 445.1579 439.5360 201.0138 -4.8061 440.3605 445.1667 439.5565 201.8638 -4.8033 440.3648 445.1680 439.5445 202.6255 -4.8049 440.3748 445.1797 439.5597 203.4533 -4.8050 440.3676 445.1726 439.5542 204.2325 -4.8049 440.3749 445.1798 439.5496 205.0545 -4.8057 440.3764 445.1821 439.5471 205.8465 -4.8041 440.3867 445.1908 439.5388 206.6385 -4.8041 440.3683 445.1725 439.5446 207.4905 -4.8038 440.3562 445.1600 439.5469 208.2523 -4.8025 440.3649 445.1674 439.5560 209.0748 -4.8007 440.3709 445.1717 439.5617 209.8655 -4.8047 440.3768 445.1815 439.5739 210.6560 -4.8067 440.3657 445.1724 439.5822 211.4780 -4.8061 440.3735 445.1796 439.5725 212.2690 -4.8053 440.3763 445.1816 439.5611 213.0903 -4.8047 440.3829 445.1876 439.5650 213.8558 -4.8036 440.3913 445.1949 439.5376 214.6850 -4.8074 440.3868 445.1942 439.5433 215.4765 -4.8041 440.3959 445.2000 439.5445 216.2983 -4.8050 440.3813 445.1863 439.5606 217.0873 -4.8014 440.3831 445.1845 439.5726 217.9085 -4.8038 440.3753 445.1791 439.5397 218.7000 -4.8009 440.3826 445.1836 439.5325 219.4908 -4.8025 440.3907 445.1931 439.5212 220.3125 -4.8035 440.3911 445.1946 439.5115 221.0745 -4.8037 440.3851 445.1888 439.5118 221.9258 -4.8009 440.4107 445.2116 439.5114 222.7175 -4.8020 440.3925 445.1945 439.5060 223.5090 -4.8004 440.3873 445.1877 439.5141 224.2968 -4.7997 440.3834 445.1831 439.5114 225.1375 -4.8004 440.3924 445.1928 439.5015 225.8995 -4.7985 440.3869 445.1854 439.5268 226.7503 -4.7980 440.3886 445.1865 439.5060 227.5113 -4.7990 440.3994 445.1984 439.4869 228.3325 -4.8029 440.3975 445.2004 439.4983 229.1545 -4.8034 440.3927 445.1961 439.4870 229.9155 -4.8026 440.3991 445.2017 439.4811 230.7665 -4.8029 440.4014 445.2042 439.4739 231.5285 -4.8023 440.4129 445.2152 439.4678 232.3493 -4.8001 440.4097 445.2098 439.4698 233.2008 -4.7998 440.3607 445.1604 439.4794 233.9610 -4.8013 440.3863 445.1876 439.4852 234.7815 -4.8018 440.3707 445.1725 439.4674 235.5728 -4.8043 440.3935 445.1978 439.4739 236.3640 -4.8040 440.4001 445.2041 439.4848 237.1908 -4.8010 440.3902 445.1913 439.4818 237.9800 -4.8016 440.4042 445.2057 439.4803 238.8010 -4.8014 440.3932 445.1946 439.4716 239.5923 -4.8025 440.4062 445.2087 439.4781 240.3835 -4.8045 440.4198 445.2243 439.4734 241.2358 -4.8028 440.3940 445.1969 439.4849 241.9968 -4.8034 440.4137 445.2171 439.4638 242.8188 -4.8035 440.4029 445.2065 439.4644 243.6105 -4.7796 440.4140 445.1936 439.4618 244.4140 -4.7588 440.4071 445.1659 439.4518 245.2198 -4.7864 440.4046 445.1910 439.4418 246.0105 -4.8007 440.3979 445.1986 439.4612 246.8325 -4.8035 440.4168 445.2203 439.4468 247.6235 -4.7955 440.4255 445.2209 439.4367 248.4440 -4.8036 440.4142 445.2178 439.4476 249.2353 -4.8054 440.4112 445.2166 439.4429 250.0253 -4.8043 440.4125 445.2167 439.4388 250.8465 -4.8032 440.4066 445.2098 439.4281 251.6378 -4.8035 440.4107 445.2142 439.4236 252.4590 -4.8031 440.4042 445.2073 439.4312 253.2505 -4.7979 440.4021 445.2000 439.4318 254.0420 -4.8006 440.4336 445.2342 439.4235 254.8625 -4.8017 440.3957 445.1974 439.4301 255.6528 -4.8019 440.4137 445.2156 439.4239 256.4745 -4.8019 440.4186 445.2204 439.4154 257.2665 -4.7982 440.4201 445.2182 439.3993 258.0580 -4.7989 440.4132 445.2122 439.3973 258.8790 -4.8060 440.4215 445.2275 439.3946 259.6698 -4.8077 440.4209 445.2286 439.3908 260.4918 -4.8074 440.4110 445.2185 439.3835 261.2840 -4.8094 440.4170 445.2264 439.3869 262.0755 -4.8059 440.4259 445.2318 439.3835 262.8975 -4.8055 440.4328 445.2382 439.3764 263.6578 -4.8065 440.4332 445.2398 439.3761 264.5105 -4.8062 440.4139 445.2201 439.3831 265.2650 -4.8030 440.4094 445.2124 439.3669 266.1260 -4.8014 440.4116 445.2130 439.3607 266.8865 -4.8006 440.3956 445.1962 439.3722 267.7078 -4.7991 440.4106 445.2097 439.3499 268.4983 -4.8013 440.4184 445.2197 439.3370 269.2895 -4.8035 440.4433 445.2468 439.3385 270.1415 -4.8036 440.4216 445.2252 439.3447 270.9035 -4.8045 440.3974 445.2020 439.3653 271.7245 -4.8025 440.4064 445.2089 439.3580 272.5163 -4.8068 440.4178 445.2245 439.3594 273.3073 -4.8043 440.4160 445.2203 439.3451 274.1280 -4.8011 440.4141 445.2152 439.3466 274.9188 -4.8026 440.4198 445.2224 439.3600 275.7403 -4.7992 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