DTA measure 2pb_updown3.dat Date: 2024319:1332 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 510.87 s Mass = 1129.000 mg data_number = 1270 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 0.7155 -4.8329 441.5665 446.3994 440.8459 1.0800 -4.8320 441.5664 446.3984 440.8491 1.4595 -4.8326 441.5705 446.4031 440.8437 1.8430 -4.8314 441.5611 446.3926 440.8472 2.3275 -4.8339 441.5430 446.3768 440.8444 2.6935 -4.8348 441.5386 446.3734 440.8377 3.0595 -4.8334 441.5545 446.3879 440.8456 3.4855 -4.8318 441.5654 446.3972 440.8437 3.9115 -4.8296 441.5608 446.3904 440.8360 4.2765 -4.8296 441.5597 446.3893 440.8405 4.6425 -4.8303 441.5531 446.3834 440.8525 5.1285 -4.8300 441.5645 446.3945 440.8433 5.4945 -4.8302 441.5650 446.3952 440.8254 5.8605 -4.8307 441.5586 446.3893 440.8302 6.2865 -4.8286 441.5599 446.3885 440.8343 6.7125 -4.8289 441.5536 446.3825 440.8282 7.0770 -4.8288 441.5465 446.3752 440.8254 7.5025 -4.8283 441.5585 446.3867 440.8234 7.9285 -4.8292 441.5703 446.3995 440.8357 8.2945 -4.8297 441.5755 446.4052 440.8404 8.6595 -4.8291 441.5692 446.3983 440.8328 9.1455 -4.8301 441.5566 446.3867 440.8218 9.5110 -4.8304 441.5614 446.3918 440.8343 9.8765 -4.8307 441.5713 446.4019 440.8232 10.3025 -4.8295 441.5607 446.3902 440.8122 10.7285 -4.8300 441.5614 446.3914 440.8011 11.0945 -4.8299 441.5646 446.3945 440.8093 11.5205 -4.8283 441.5641 446.3924 440.7960 11.9465 -4.8268 441.5680 446.3948 440.8075 12.3115 -4.8279 441.5666 446.3945 440.8078 12.6775 -4.8298 441.5552 446.3849 440.7980 13.1635 -4.8269 441.5637 446.3906 440.8041 13.5295 -4.8296 441.5684 446.3981 440.7777 13.8950 -4.8300 441.5672 446.3971 440.7733 14.3205 -4.8283 441.5721 446.4004 440.7758 14.7465 -4.8294 441.5528 446.3823 440.7794 15.1110 -4.8304 441.5776 446.4080 440.7769 15.4765 -4.8311 441.5875 446.4186 440.7775 15.9625 -4.8320 441.5850 446.4170 440.7826 16.3270 -4.8305 441.5834 446.4139 440.8273 16.6925 -4.8291 441.5796 446.4088 440.7999 17.1785 -4.8250 441.5642 446.3892 440.8046 17.5430 -4.8233 441.5597 446.3830 440.7905 17.9085 -4.8239 441.5715 446.3953 440.7802 18.3345 -4.8237 441.5795 446.4033 440.7864 18.7600 -4.8268 441.5923 446.4191 440.7840 19.1250 -4.8263 441.5945 446.4208 440.7856 19.4910 -4.8256 441.5941 446.4197 440.7942 19.9775 -4.8240 441.5914 446.4155 440.7899 20.3420 -4.8228 441.5801 446.4029 440.7815 20.7065 -4.8268 441.5963 446.4232 440.7768 21.1935 -4.8254 441.5886 446.4140 440.7780 21.5580 -4.8251 441.5993 446.4244 440.7855 21.9225 -4.8250 441.5949 446.4199 440.7706 22.3135 -4.8232 441.5917 446.4149 440.7625 22.7995 -4.8242 441.5901 446.4143 440.8139 23.1640 -4.8224 441.5887 446.4111 440.7673 23.5300 -4.8243 441.5962 446.4205 440.7539 23.9560 -4.8232 441.5940 446.4172 440.7619 24.3820 -4.8243 441.5958 446.4202 440.7698 24.7465 -4.8231 441.6039 446.4270 440.7534 25.1125 -4.8216 441.5963 446.4178 440.7305 25.5995 -4.8229 441.5979 446.4208 440.7539 25.9640 -4.8222 441.6156 446.4378 440.7456 26.3285 -4.8208 441.6228 446.4436 440.7518 26.7545 -4.8186 441.6307 446.4494 440.7391 27.1800 -4.8244 441.6029 446.4273 440.7492 27.5450 -4.8234 441.6085 446.4319 440.7515 27.9710 -4.8221 441.6058 446.4279 440.7436 28.3965 -4.8221 441.5864 446.4085 440.7451 28.7625 -4.8219 441.5982 446.4201 440.7262 29.1285 -4.8197 441.6012 446.4209 440.7335 29.6145 -4.8196 441.6065 446.4261 440.7367 29.9800 -4.8199 441.6034 446.4233 440.7556 30.3455 -4.8174 441.6124 446.4298 440.7550 30.7715 -4.8200 441.6213 446.4413 440.7469 31.1975 -4.8214 441.6255 446.4469 440.7460 31.5630 -4.8225 441.6189 446.4414 440.7504 31.9285 -4.8215 441.6173 446.4388 440.7530 32.4145 -4.8174 441.5926 446.4100 440.7567 32.7805 -4.8185 441.5958 446.4142 440.7567 33.1465 -4.8203 441.6141 446.4344 440.7513 33.6325 -4.8191 441.6146 446.4337 440.7546 33.9980 -4.7951 441.6270 446.4220 440.7495 34.3630 -4.7899 441.6083 446.3982 440.7618 34.7885 -4.8041 441.6170 446.4212 440.7766 35.2145 -4.8136 441.6158 446.4294 440.7871 35.5805 -4.8170 441.6045 446.4215 440.7729 35.9465 -4.8184 441.5945 446.4129 440.7764 36.4325 -4.8151 441.6049 446.4200 440.7475 36.7980 -4.8163 441.5826 446.3989 440.7410 37.1625 -4.8170 441.5904 446.4074 440.7505 37.6485 -4.8127 441.5943 446.4070 440.7730 38.0140 -4.8124 441.6064 446.4189 440.7704 38.3780 -4.8195 441.6048 446.4244 440.7873 38.8035 -4.8200 441.6123 446.4323 440.7891 39.2295 -4.8167 441.6107 446.4274 440.7833 39.5945 -4.8153 441.6290 446.4443 440.7776 39.9605 -4.8183 441.6120 446.4303 440.7737 40.4465 -4.8174 441.6157 446.4331 440.7837 40.8125 -4.8039 441.6314 446.4353 440.7834 41.1785 -4.8094 441.6281 446.4375 440.7841 41.6645 -4.8172 441.6248 446.4420 440.7570 42.0295 -4.8161 441.6220 446.4381 440.7755 42.3955 -4.8170 441.6174 446.4343 440.7713 42.7920 -4.8145 441.6172 446.4317 440.7649 43.2185 -4.8136 441.6094 446.4230 440.7864 43.6440 -4.8176 441.6271 446.4448 440.7792 44.0090 -4.8200 441.6327 446.4527 440.7823 44.3750 -4.8221 441.6322 446.4543 440.7781 44.8615 -4.8196 441.6252 446.4447 440.7781 45.2260 -4.8173 441.6243 446.4416 440.7825 45.5905 -4.8181 441.6170 446.4351 440.7896 46.0775 -4.8195 441.6219 446.4414 440.7813 46.4425 -4.8189 441.6338 446.4527 440.7831 46.8080 -4.8143 441.6258 446.4401 440.7825 47.2345 -4.8148 441.6317 446.4465 440.7690 47.6600 -4.8167 441.6287 446.4454 440.7650 48.0255 -4.8178 441.6379 446.4557 440.7919 48.3915 -4.8211 441.6238 446.4449 440.8003 48.8785 -4.8238 441.6319 446.4557 440.7930 49.2430 -4.8208 441.6292 446.4500 440.7793 49.6075 -4.8126 441.6182 446.4308 440.7898 50.0945 -4.8176 441.6201 446.4377 440.7945 50.4595 -4.8198 441.6265 446.4463 440.8127 50.8250 -4.8225 441.6440 446.4665 440.8037 51.2510 -4.8226 441.6363 446.4589 440.8009 51.6770 -4.8251 441.6444 446.4695 440.7847 52.0425 -4.8269 441.6504 446.4773 440.7894 52.4085 -4.8252 441.6522 446.4773 440.7941 52.8950 -4.8149 441.6498 446.4647 440.7914 53.2605 -4.8216 441.6295 446.4510 440.7905 53.6255 -4.8222 441.6277 446.4500 440.7883 54.0515 -4.8236 441.6451 446.4687 440.7990 54.4775 -4.8239 441.6598 446.4837 440.8030 54.8430 -4.8213 441.6823 446.5036 440.7797 55.2695 -4.8227 441.6807 446.5033 440.7829 55.6955 -4.8187 441.6527 446.4714 440.7933 56.0615 -4.8143 441.6572 446.4715 440.7868 56.4275 -4.8184 441.6548 446.4732 440.7849 56.9135 -4.8221 441.6471 446.4691 440.7749 57.2795 -4.8237 441.6508 446.4745 440.7815 57.6455 -4.8218 441.6440 446.4657 440.8031 58.0715 -4.8206 441.6431 446.4637 440.7973 58.4975 -4.8240 441.6469 446.4709 440.7930 58.8620 -4.8257 441.6476 446.4733 440.8006 59.2275 -4.8275 441.6384 446.4659 440.7735 59.7135 -4.8283 441.6343 446.4626 440.7844 60.0795 -4.8299 441.6365 446.4664 440.7878 60.4455 -4.8268 441.6451 446.4719 440.7931 60.9315 -4.8274 441.6736 446.5011 440.8156 61.2970 -4.8267 441.6726 446.4993 440.8023 61.6620 -4.8252 441.6641 446.4893 440.7856 62.0875 -4.8227 441.6566 446.4793 440.7890 62.5135 -4.8239 441.6554 446.4794 440.7931 62.8945 -4.8239 441.6405 446.4644 440.7951 63.2765 -4.8243 441.6638 446.4881 440.7804 63.7025 -4.8265 441.6473 446.4738 440.7760 64.1285 -4.8284 441.6487 446.4771 440.7772 64.4935 -4.8264 441.6413 446.4677 440.7744 64.8585 -4.8283 441.6580 446.4863 440.7761 65.3445 -4.8279 441.6612 446.4891 440.7747 65.7105 -4.8269 441.6578 446.4848 440.7798 66.0755 -4.8278 441.6604 446.4882 440.7889 66.5015 -4.8272 441.6456 446.4728 440.7912 66.9265 -4.8271 441.6368 446.4639 440.7698 67.2925 -4.8268 441.6668 446.4936 440.7690 67.7185 -4.8273 441.6622 446.4896 440.7975 68.1445 -4.8270 441.6586 446.4855 440.7983 68.5100 -4.8278 441.6565 446.4843 440.8142 68.8765 -4.8261 441.6638 446.4899 440.8184 69.3625 -4.8291 441.6543 446.4834 440.8074 69.7275 -4.8300 441.6503 446.4803 440.8132 70.0940 -4.8287 441.6561 446.4848 440.8141 70.5200 -4.8278 441.6497 446.4776 440.8026 70.9460 -4.8270 441.6492 446.4763 440.7990 71.3100 -4.8271 441.6471 446.4742 440.8074 71.7355 -4.8258 441.6531 446.4789 440.8001 72.1610 -4.8266 441.6624 446.4890 440.7921 72.5265 -4.8298 441.6522 446.4820 440.8029 72.8925 -4.8304 441.6508 446.4812 440.7927 73.3795 -4.8263 441.6558 446.4821 440.7877 73.7445 -4.8271 441.6577 446.4847 440.8189 74.1105 -4.8271 441.6619 446.4891 440.8167 74.5370 -4.8300 441.6582 446.4882 440.8258 74.9630 -4.8307 441.6621 446.4928 440.8122 75.3275 -4.8285 441.6623 446.4908 440.8051 75.6935 -4.8307 441.6626 446.4933 440.7953 76.1805 -4.8313 441.6549 446.4862 440.7896 76.5450 -4.8291 441.6653 446.4944 440.7988 76.9095 -4.8295 441.6614 446.4909 440.7922 77.3965 -4.8301 441.6537 446.4838 440.7838 77.7610 -4.8309 441.6497 446.4806 440.7998 78.1265 -4.8332 441.6661 446.4993 440.8084 78.5525 -4.8311 441.6650 446.4961 440.8098 78.9785 -4.8302 441.6707 446.5009 440.8083 79.3430 -4.8292 441.6842 446.5134 440.7944 79.7685 -4.8293 441.6658 446.4951 440.7972 80.1945 -4.8289 441.6713 446.5001 440.7964 80.5595 -4.8297 441.6743 446.5040 440.8015 80.9255 -4.8278 441.6665 446.4943 440.7979 81.4105 -4.8260 441.6656 446.4916 440.7881 81.7760 -4.8280 441.6668 446.4948 440.7978 82.1405 -4.8303 441.6602 446.4905 440.8068 82.5665 -4.8304 441.6611 446.4915 440.8030 82.9925 -4.8316 441.6443 446.4758 440.7931 83.3745 -4.8301 441.6455 446.4756 440.7939 83.7605 -4.8306 441.6594 446.4900 440.7888 84.1265 -4.8294 441.6630 446.4923 440.7832 84.6125 -4.8292 441.6857 446.5148 440.7862 84.9780 -4.8287 441.6745 446.5032 440.7864 85.3435 -4.8273 441.6668 446.4941 440.7795 85.8295 -4.8263 441.6525 446.4788 440.7731 86.1950 -4.8289 441.6470 446.4759 440.7823 86.5600 -4.8308 441.6696 446.5004 440.7708 86.9855 -4.8277 441.6806 446.5083 440.7663 87.4115 -4.8269 441.6879 446.5149 440.7835 87.7770 -4.8272 441.6770 446.5042 440.7892 88.1425 -4.8293 441.6691 446.4984 440.8181 88.6285 -4.8277 441.6573 446.4850 440.7947 88.9945 -4.8296 441.6764 446.5060 440.7996 89.3595 -4.8298 441.6815 446.5112 440.7760 89.8455 -4.8286 441.6807 446.5093 440.7763 90.2110 -4.8279 441.6740 446.5019 440.7590 90.5765 -4.8270 441.6718 446.4988 440.7694 91.0025 -4.8252 441.6806 446.5058 440.7662 91.4285 -4.8223 441.6812 446.5035 440.7727 91.7935 -4.8234 441.6750 446.4984 440.7609 92.1595 -4.8261 441.6834 446.5096 440.7633 92.6455 -4.8262 441.6910 446.5172 440.7684 93.0110 -4.7973 441.6837 446.4810 440.7561 93.3765 -4.8070 441.6848 446.4918 440.7526 93.7750 -4.8164 441.6564 446.4727 440.7381 94.1740 -4.8236 441.6745 446.4981 440.7430 94.6605 -4.8256 441.6714 446.4970 440.7535 95.0255 -4.8246 441.6702 446.4947 440.7467 95.3905 -4.8228 441.6736 446.4965 440.7500 95.8170 -4.8223 441.6649 446.4872 440.7454 96.2430 -4.8163 441.6566 446.4729 440.7512 96.6075 -4.8167 441.6682 446.4849 440.7479 96.9735 -4.8194 441.6891 446.5085 440.7309 97.4605 -4.8216 441.6801 446.5017 440.7293 97.8250 -4.8224 441.6733 446.4958 440.7446 98.1905 -4.8252 441.6778 446.5030 440.7572 98.6775 -4.8255 441.6535 446.4791 440.7554 99.0420 -4.8277 441.6627 446.4905 440.7515 99.4075 -4.8222 441.6716 446.4938 440.7505 99.8340 -4.8241 441.6740 446.4981 440.7401 100.2600 -4.8268 441.6701 446.4969 440.7568 100.6255 -4.8191 441.6663 446.4855 440.7481 100.9905 -4.8198 441.6672 446.4870 440.7363 101.4775 -4.8171 441.6765 446.4936 440.7348 101.8420 -4.8187 441.6782 446.4968 440.7366 102.2075 -4.8212 441.6738 446.4950 440.7323 102.6340 -4.8233 441.6794 446.5027 440.7359 103.0600 -4.8212 441.6798 446.5011 440.7503 103.4240 -4.8206 441.6770 446.4976 440.7471 103.8495 -4.8223 441.6756 446.4979 440.7495 104.2755 -4.8260 441.6757 446.5017 440.7442 104.6415 -4.8257 441.6448 446.4705 440.7335 105.0075 -4.8240 441.6705 446.4945 440.7169 105.4935 -4.8227 441.6830 446.5056 440.7243 105.8590 -4.8230 441.6794 446.5024 440.7306 106.2245 -4.8228 441.6736 446.4964 440.7214 106.6505 -4.8216 441.6736 446.4952 440.7391 107.0765 -4.8216 441.6798 446.5014 440.7466 107.4415 -4.8222 441.6748 446.4970 440.7450 107.8075 -4.8224 441.6657 446.4881 440.7423 108.2935 -4.8222 441.6713 446.4934 440.7368 108.6595 -4.8209 441.6735 446.4944 440.7469 109.0255 -4.8221 441.6845 446.5066 440.7496 109.5115 -4.8207 441.6930 446.5137 440.7503 109.8775 -4.8159 441.6850 446.5009 440.7532 110.2435 -4.8186 441.6830 446.5016 440.7671 110.6695 -4.8176 441.6735 446.4911 440.7663 111.0955 -4.8116 441.6904 446.5019 440.7506 111.4615 -4.8104 441.6916 446.5020 440.7413 111.8275 -4.8142 441.6754 446.4896 440.7471 112.3135 -4.8200 441.6809 446.5009 440.7303 112.6790 -4.8183 441.6982 446.5165 440.7254 113.0435 -4.8040 441.6855 446.4895 440.7391 113.4695 -4.7998 441.6743 446.4741 440.7261 113.8955 -4.8082 441.6847 446.4929 440.7399 114.2740 -4.8107 441.6876 446.4983 440.7322 114.6535 -4.8135 441.6984 446.5120 440.7502 115.0795 -4.8133 441.7038 446.5171 440.7388 115.5055 -4.8122 441.6927 446.5050 440.7518 115.8715 -4.8145 441.6831 446.4976 440.7554 116.2375 -4.8075 441.6885 446.4961 440.7431 116.7250 -4.8064 441.6978 446.5041 440.7581 117.0900 -4.8122 441.7004 446.5125 440.7526 117.4555 -4.8140 441.6953 446.5093 440.7544 117.8815 -4.8159 441.6866 446.5025 440.7517 118.3075 -4.8150 441.6820 446.4971 440.7567 118.6725 -4.8161 441.6761 446.4922 440.7532 119.0985 -4.8205 441.6818 446.5023 440.7563 119.5240 -4.8237 441.6852 446.5089 440.7530 119.8880 -4.8185 441.6862 446.5047 440.7471 120.2545 -4.8146 441.6819 446.4964 440.7507 120.7405 -4.8219 441.6693 446.4913 440.7603 121.1050 -4.8292 441.6797 446.5089 440.7592 121.4710 -4.8305 441.6875 446.5180 440.7579 121.8975 -4.8338 441.6865 446.5203 440.7602 122.3230 -4.8297 441.6864 446.5161 440.7494 122.6870 -4.8212 441.6792 446.5004 440.7421 123.1130 -4.8131 441.6858 446.4989 440.7352 123.5390 -4.8114 441.6761 446.4876 440.7327 123.9035 -4.8091 441.6860 446.4951 440.7285 124.2695 -4.8045 441.6883 446.4928 440.7542 124.7105 -4.7973 441.7004 446.4976 440.7531 125.0755 -4.8257 441.7072 446.5329 440.7622 125.5625 -4.8405 441.6979 446.5384 440.7706 125.9270 -4.8461 441.6945 446.5406 440.7624 126.2930 -4.8498 441.6868 446.5366 440.7592 126.7195 -4.8537 441.6818 446.5355 440.7658 127.1450 -4.8538 441.6782 446.5320 440.7491 127.5090 -4.8488 441.6792 446.5281 440.7464 127.8735 -4.8435 441.6987 446.5421 440.7488 128.3600 -4.8375 441.6931 446.5306 440.7602 128.7255 -4.8371 441.6925 446.5297 440.7708 129.0915 -4.8369 441.6759 446.5128 440.7684 129.5175 -4.8339 441.6909 446.5247 440.7924 129.9435 -4.8332 441.6887 446.5219 440.7730 130.3085 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