DTA measure 2test.dat Date: 2024319:145 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1551.32 s Mass = 1129.000 mg data_number = 1926 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.4380 -4.7736 441.8863 446.6599 440.9291 2.1998 -4.7752 441.8929 446.6682 440.9324 3.0218 -4.7765 441.8831 446.6596 440.9500 3.8140 -4.7749 441.8820 446.6569 440.9559 4.6043 -4.7735 441.8821 446.6556 440.9243 5.4558 -4.7742 441.8809 446.6551 440.9544 6.1983 -4.7758 441.8633 446.6391 440.9746 7.0548 -4.7752 441.8642 446.6394 440.9904 7.8155 -4.7752 441.8854 446.6605 440.9828 8.6375 -4.7765 441.8843 446.6608 440.9894 9.4295 -4.7779 441.8756 446.6535 441.0063 10.2208 -4.7768 441.8794 446.6563 440.9840 11.0425 -4.7807 441.8765 446.6572 440.9849 11.8345 -4.7780 441.9004 446.6784 441.0381 12.6560 -4.7780 441.8970 446.6749 441.0180 13.4475 -4.7782 441.8799 446.6580 440.9947 14.2395 -4.7781 441.8987 446.6768 441.0119 15.0615 -4.7779 441.8876 446.6655 441.0311 15.8235 -4.7782 441.9001 446.6783 441.0282 16.6753 -4.7746 441.9045 446.6791 441.0367 17.4663 -4.7758 441.8913 446.6671 441.0362 18.2575 -4.7730 441.9183 446.6913 441.0224 19.0795 -4.7733 441.8897 446.6630 441.0416 19.8703 -4.7752 441.8819 446.6570 441.0417 20.6900 -4.7762 441.8741 446.6503 441.0524 21.4813 -4.7739 441.8669 446.6408 441.0396 22.2718 -4.7752 441.8876 446.6629 441.0436 23.0933 -4.7757 441.8931 446.6688 441.0429 23.8835 -4.7756 441.8898 446.6654 441.0395 24.7040 -4.7761 441.8928 446.6689 441.0311 25.4943 -4.7786 441.8932 446.6718 441.0195 26.2853 -4.7797 441.8930 446.6727 441.0178 27.0988 -4.7752 441.9046 446.6797 441.0565 27.8898 -4.7766 441.9370 446.7135 441.0457 28.7120 -4.7753 441.8943 446.6696 441.0208 29.5020 -4.7790 441.9035 446.6824 441.0044 30.3225 -4.7779 441.8937 446.6715 440.9935 31.1130 -4.7796 441.8993 446.6789 440.9690 31.9038 -4.7804 441.9008 446.6812 440.9789 32.7260 -4.7752 441.8914 446.6667 440.9828 33.5158 -4.7752 441.8959 446.6711 440.9857 34.3360 -4.7767 441.9011 446.6778 440.9890 35.1263 -4.7765 441.8876 446.6641 440.9802 35.9168 -4.7778 441.8910 446.6688 440.9703 36.7380 -4.7754 441.8868 446.6622 440.9562 37.5278 -4.7795 441.8989 446.6783 440.9187 38.3495 -4.7837 441.8909 446.6746 440.9168 39.1415 -4.7837 441.9016 446.6853 440.9159 39.9328 -4.7787 441.8980 446.6767 440.9167 40.7545 -4.7756 441.9003 446.6759 440.8925 41.5458 -4.7751 441.9109 446.6860 440.8840 42.3670 -4.7759 441.9067 446.6826 440.8782 43.1585 -4.7737 441.9017 446.6754 440.8821 43.9505 -4.7755 441.8891 446.6647 440.8675 44.7725 -4.7755 441.8985 446.6741 440.8482 45.5345 -4.7716 441.9062 446.6778 440.8453 46.3863 -4.7740 441.9086 446.6826 440.8340 47.1350 -4.7736 441.8907 446.6643 440.8215 48.0040 -4.7759 441.9152 446.6911 440.8188 48.7655 -4.7794 441.9233 446.7028 440.8336 49.5855 -4.7764 441.9140 446.6904 440.8070 50.3775 -4.7735 441.9099 446.6834 440.8019 51.1680 -4.7743 441.9000 446.6743 440.8021 52.0198 -4.7725 441.8973 446.6699 440.7895 52.7798 -4.7749 441.9142 446.6891 440.7758 53.6003 -4.7742 441.9275 446.7018 440.7943 54.4220 -4.7705 441.9077 446.6782 440.7795 55.1830 -4.7698 441.8907 446.6605 440.7580 56.0338 -4.7693 441.8928 446.6620 440.7537 56.7940 -4.7669 441.9099 446.6769 440.7944 57.6153 -4.7633 441.9087 446.6720 440.7732 58.4370 -4.7640 441.9083 446.6723 440.7607 59.1985 -4.7664 441.9184 446.6848 440.7418 60.0503 -4.7659 441.9133 446.6792 440.7311 60.8108 -4.7662 441.9055 446.6717 440.7202 61.6323 -4.7672 441.8868 446.6540 440.7322 62.4535 -4.7669 441.8975 446.6644 440.7174 63.2145 -4.7670 441.8832 446.6502 440.7050 64.0663 -4.7666 441.8852 446.6518 440.6953 64.8275 -4.7671 441.8909 446.6579 440.6870 65.6493 -4.7682 441.9121 446.6802 440.6765 66.4705 -4.7660 441.9165 446.6825 440.6825 67.2315 -4.7651 441.9186 446.6837 440.6713 68.0573 -4.7639 441.9017 446.6656 440.6746 68.8495 -4.7640 441.9102 446.6742 440.6649 69.6715 -4.7615 441.9185 446.6800 440.6824 70.4330 -4.7645 441.9106 446.6752 440.6818 71.2845 -4.7642 441.8971 446.6612 440.6550 72.0753 -4.7611 441.8982 446.6593 440.6518 72.8658 -4.7622 441.9099 446.6721 440.6492 73.6873 -4.7625 441.9061 446.6686 440.6692 74.4475 -4.7626 441.9267 446.6893 440.6651 75.2990 -4.7606 441.9128 446.6734 440.6517 76.0903 -4.7623 441.9008 446.6631 440.6373 76.8805 -4.7628 441.8913 446.6540 440.6618 77.7020 -4.7618 441.8874 446.6492 440.6554 78.4630 -4.7620 441.9005 446.6624 440.6624 79.3148 -4.7591 441.8968 446.6559 440.6726 80.1050 -4.7561 441.8977 446.6538 440.6604 80.8950 -4.7570 441.8994 446.6564 440.6678 81.7160 -4.7584 441.8977 446.6562 440.6642 82.4765 -4.7573 441.9021 446.6593 440.6649 83.3288 -4.7587 441.8994 446.6581 440.6718 84.1198 -4.7583 441.9020 446.6603 440.6705 84.9108 -4.7555 441.9007 446.6563 440.6601 85.7328 -4.7582 441.8863 446.6445 440.6640 86.4935 -4.7590 441.9002 446.6592 440.6742 87.3453 -4.7576 441.9077 446.6653 440.6745 88.0938 -4.7556 441.8900 446.6456 440.6983 88.9620 -4.7553 441.8884 446.6438 440.6951 89.7220 -4.7558 441.8861 446.6419 440.6994 90.5430 -4.7573 441.8767 446.6340 440.6996 91.3345 -4.7573 441.8802 446.6375 440.6928 92.1258 -4.7580 441.8914 446.6493 440.6888 92.9475 -4.7598 441.8782 446.6380 440.7147 93.7385 -4.7564 441.8707 446.6271 440.6978 94.5598 -4.7554 441.8668 446.6223 440.7060 95.3495 -4.7530 441.8967 446.6498 440.7193 96.1403 -4.7528 441.8902 446.6430 440.7324 96.9915 -4.7560 441.8897 446.6456 440.7391 97.7518 -4.7562 441.8829 446.6392 440.7337 98.5730 -4.7540 441.8946 446.6486 440.7484 99.3645 -4.7571 441.8959 446.6530 440.7614 100.1555 -4.7553 441.8971 446.6524 440.7617 100.9773 -4.7527 441.8961 446.6487 440.7604 101.7675 -4.7535 441.8823 446.6358 440.7704 102.5888 -4.7549 441.8795 446.6344 440.7763 103.3800 -4.7563 441.8819 446.6382 440.7899 104.1705 -4.7567 441.8968 446.6535 440.7882 104.9920 -4.7561 441.8866 446.6427 440.7848 105.7535 -4.7566 441.8660 446.6226 440.7887 106.6060 -4.7562 441.8815 446.6378 440.7895 107.3970 -4.7554 441.8935 446.6489 440.7991 108.1898 -4.7550 441.8934 446.6484 440.8029 108.9860 -4.7557 441.8756 446.6313 440.8132 109.8070 -4.7560 441.8874 446.6434 440.8201 110.5980 -4.7539 441.8837 446.6376 440.8091 111.3888 -4.7547 441.8676 446.6223 440.8036 112.2403 -4.7536 441.8683 446.6219 440.8087 113.0015 -4.7534 441.8965 446.6499 440.8168 113.8233 -4.7529 441.8948 446.6478 440.8234 114.6145 -4.7551 441.8784 446.6335 440.8361 115.4060 -4.7536 441.8755 446.6291 440.8495 116.2275 -4.7531 441.8782 446.6312 440.8560 117.0185 -4.7527 441.8770 446.6296 440.8505 117.8405 -4.7514 441.8660 446.6175 440.8553 118.6315 -4.7484 441.8772 446.6255 440.8663 119.4235 -4.7532 441.8854 446.6386 440.8685 120.2448 -4.7552 441.8839 446.6392 440.8650 121.0065 -4.7553 441.8829 446.6381 440.8517 121.8583 -4.7550 441.8677 446.6227 440.8612 122.6490 -4.7557 441.8785 446.6343 440.8647 123.4405 -4.7592 441.8699 446.6292 440.8556 124.2623 -4.7570 441.8877 446.6447 440.8518 125.0235 -4.7612 441.8860 446.6471 440.8512 125.8750 -4.7585 441.8855 446.6440 440.8551 126.6673 -4.7580 441.8729 446.6309 440.8442 127.4583 -4.7560 441.8704 446.6264 440.8490 128.2800 -4.7549 441.8642 446.6191 440.8477 129.0613 -4.7552 441.8602 446.6154 440.8437 129.8920 -4.7538 441.8737 446.6274 440.8432 130.6535 -4.7563 441.8761 446.6325 440.8469 131.5058 -4.7578 441.8881 446.6459 440.8436 132.2668 -4.7578 441.8987 446.6565 440.8365 133.0888 -4.7599 441.8861 446.6460 440.8455 133.8810 -4.7591 441.8869 446.6460 440.8527 134.6713 -4.7576 441.8803 446.6379 440.8324 135.5223 -4.7604 441.8787 446.6391 440.8210 136.2825 -4.7586 441.8793 446.6380 440.8265 137.1045 -4.7595 441.8833 446.6428 440.8355 137.8955 -4.7598 441.8757 446.6355 440.8324 138.6863 -4.7576 441.8708 446.6284 440.8289 139.5373 -4.7563 441.8815 446.6379 440.8247 140.2975 -4.7606 441.8729 446.6335 440.8334 141.1180 -4.7622 441.8755 446.6377 440.8418 141.9095 -4.7600 441.8732 446.6332 440.8284 142.7010 -4.7598 441.8651 446.6249 440.8083 143.5525 -4.7600 441.8672 446.6272 440.8061 144.3145 -4.7599 441.8735 446.6334 440.8153 145.1355 -4.7590 441.8820 446.6411 440.8284 145.9275 -4.7610 441.8676 446.6286 440.8302 146.7190 -4.7618 441.8905 446.6522 440.8291 147.5703 -4.7617 441.8613 446.6231 440.8337 148.3308 -4.7585 441.8722 446.6307 440.8381 149.1525 -4.7607 441.8765 446.6372 440.8247 149.9445 -4.7602 441.8768 446.6370 440.8202 150.7653 -4.7621 441.8720 446.6341 440.8156 151.5570 -4.7642 441.8673 446.6315 440.8060 152.3478 -4.7613 441.8511 446.6124 440.8131 153.1695 -4.7618 441.8727 446.6345 440.8132 153.9308 -4.7629 441.8663 446.6292 440.8002 154.7828 -4.7638 441.8704 446.6342 440.8067 155.5730 -4.7653 441.8755 446.6408 440.7996 156.3638 -4.7649 441.8723 446.6371 440.8116 157.1860 -4.7629 441.8640 446.6269 440.8105 157.9470 -4.7615 441.8703 446.6318 440.7877 158.7990 -4.7609 441.8798 446.6408 440.7962 159.5508 -4.7593 441.8763 446.6356 440.7947 160.3665 -4.7591 441.8612 446.6202 440.8114 161.1880 -4.7592 441.8774 446.6366 440.8296 162.0095 -4.7602 441.8782 446.6383 440.8297 162.7705 -4.7580 441.8760 446.6341 440.8427 163.6223 -4.7612 441.8801 446.6413 440.8250 164.4135 -4.7615 441.8678 446.6293 440.8118 165.2055 -4.7618 441.8895 446.6513 440.8275 166.0573 -4.7619 441.8916 446.6535 440.8348 166.8175 -4.7648 441.8811 446.6459 440.8603 167.6385 -4.7637 441.8796 446.6433 440.8395 168.4295 -4.7638 441.8787 446.6425 440.8276 169.2203 -4.7596 441.8718 446.6314 440.8287 170.0718 -4.7599 441.8815 446.6413 440.8567 170.8335 -4.7601 441.8718 446.6319 440.8620 171.6555 -4.7598 441.8498 446.6096 440.8549 172.4475 -4.7607 441.8611 446.6218 440.8547 173.2388 -4.7739 441.8375 446.6113 440.8446 174.0605 -4.7936 441.8315 446.6251 440.8485 174.8505 -4.8017 441.8303 446.6319 440.8558 175.6715 -4.8170 441.8196 446.6366 440.8381 176.4633 -4.8202 441.8157 446.6359 440.7608 177.2540 -4.8292 441.8080 446.6371 440.5808 178.0750 -4.8442 441.7857 446.6299 440.3464 178.8650 -4.8665 441.7575 446.6241 440.0863 179.6863 -4.8956 441.7479 446.6435 439.7493 180.4578 -4.9312 441.6942 446.6254 439.4431 181.3100 -4.9775 441.6477 446.6252 439.1167 182.0708 -5.0208 441.6119 446.6327 438.7737 182.8923 -5.0689 441.5529 446.6217 438.4116 183.6840 -5.1200 441.4967 446.6167 438.0397 184.4753 -5.1740 441.4459 446.6200 437.7412 185.3275 -5.2338 441.3674 446.6012 437.4633 186.0875 -5.2924 441.3080 446.6003 437.2302 186.9090 -5.3547 441.2459 446.6006 437.0321 187.7005 -5.4135 441.1813 446.5948 436.8804 188.4918 -5.4700 441.1380 446.6080 436.7633 189.3425 -5.5260 441.0794 446.6054 436.6710 190.1018 -5.5767 441.0385 446.6152 436.6061 190.9230 -5.6282 440.9739 446.6022 436.5283 191.7148 -5.6815 440.9235 446.6050 436.4916 192.5058 -5.7317 440.8558 446.5875 436.4684 193.3275 -5.7834 440.8160 446.5994 436.4539 194.1195 -5.8318 440.7609 446.5927 436.4431 194.9415 -5.8812 440.7159 446.5970 436.4342 195.7335 -5.9260 440.6655 446.5915 436.4284 196.5255 -5.9723 440.6076 446.5799 436.4509 197.3475 -6.0199 440.5514 446.5713 436.4438 198.1385 -6.0647 440.4948 446.5595 436.4538 198.9600 -6.1096 440.4404 446.5500 436.4607 199.7505 -6.1519 440.3846 446.5365 436.4794 200.5468 -6.1961 440.3477 446.5438 436.5041 201.3555 -6.2394 440.2949 446.5344 436.5249 202.1463 -6.2811 440.2380 446.5191 436.5452 202.9680 -6.3224 440.1898 446.5122 436.5630 203.7593 -6.3608 440.1477 446.5085 436.5869 204.5805 -6.4034 440.0738 446.4773 436.5987 205.3720 -6.4444 440.0328 446.4771 436.5922 206.1635 -6.4825 439.9726 446.4552 436.6330 206.9855 -6.5253 439.9174 446.4427 436.6675 207.7465 -6.5638 439.8578 446.4216 436.6926 208.5990 -6.6066 439.8155 446.4220 436.7159 209.3910 -6.6451 439.7672 446.4123 436.7556 210.1818 -6.6807 439.7016 446.3823 436.7880 211.0098 -6.7181 439.6417 446.3598 436.8148 211.7710 -6.7523 439.6006 446.3528 436.8396 212.6225 -6.7925 439.5331 446.3255 436.8556 213.3845 -6.8284 439.4853 446.3137 436.8741 214.2058 -6.8648 439.4211 446.2859 436.8907 215.0265 -6.9021 439.3560 446.2581 436.9007 215.7878 -6.9358 439.3180 446.2539 436.9310 216.6395 -6.9728 439.2739 446.2467 436.9422 217.4008 -7.0052 439.2011 446.2062 436.9822 218.2218 -7.0263 439.1345 446.1608 436.9985 219.0420 -7.0644 439.0844 446.1488 437.0163 219.8030 -7.0988 439.0272 446.1260 437.0292 220.6548 -7.1496 438.9774 446.1270 437.0399 221.4025 -7.1840 438.9276 446.1117 437.0826 222.2605 -7.2166 438.8737 446.0903 437.1166 223.0225 -7.2427 438.8272 446.0698 437.1549 223.8445 -7.2684 438.7867 446.0550 437.1888 224.6665 -7.2911 438.7243 446.0154 437.2134 225.4263 -7.3121 438.6784 445.9905 437.2581 226.2773 -7.3343 438.6414 445.9757 437.2785 227.0390 -7.3496 438.6036 445.9531 437.3165 227.8613 -7.3650 438.5584 445.9234 437.3440 228.6533 -7.3793 438.5098 445.8891 437.3901 229.4433 -7.3897 438.4775 445.8673 437.4453 230.2948 -7.4003 438.4397 445.8400 437.4761 231.0550 -7.4081 438.4068 445.8149 437.4782 231.8793 -7.4139 438.3528 445.7667 437.5124 232.6710 -7.4196 438.3232 445.7429 437.5407 233.4613 -7.4265 438.2899 445.7164 437.5601 234.2830 -7.4265 438.2649 445.6914 437.5852 235.0730 -7.4165 438.2528 445.6693 437.6080 235.8943 -7.4242 438.2271 445.6513 437.6458 236.6845 -7.4280 438.2098 445.6378 437.6716 237.4758 -7.4286 438.1741 445.6027 437.7024 238.2975 -7.4233 438.1477 445.5710 437.7375 239.0895 -7.4243 438.1000 445.5243 437.7491 239.9108 -7.4236 438.0742 445.4978 437.7646 240.7003 -7.4173 438.0644 445.4817 437.7814 241.5048 -7.4126 438.0341 445.4467 437.8110 242.3135 -7.4064 438.0233 445.4298 437.8305 243.1050 -7.4012 438.0058 445.4069 437.8576 243.9265 -7.3969 437.9855 445.3824 437.8598 244.6880 -7.3913 437.9602 445.3515 437.8907 245.5393 -7.3843 437.9594 445.3437 437.9128 246.3305 -7.3712 437.9245 445.2957 437.9240 247.1213 -7.3629 437.8991 445.2620 437.9348 247.9425 -7.3550 437.8951 445.2501 437.9461 248.7038 -7.3482 437.8748 445.2230 437.9745 249.5553 -7.3375 437.8483 445.1858 437.9814 250.3165 -7.3244 437.8711 445.1955 438.0065 251.1405 -7.3113 437.8446 445.1560 438.0207 251.9080 -7.3000 437.8292 445.1292 438.0200 252.7363 -7.2838 437.8098 445.0936 438.0120 253.5273 -7.2710 437.7823 445.0532 438.0394 254.3490 -7.2558 437.7832 445.0390 438.0606 255.1388 -7.2434 437.7773 445.0207 438.0577 255.9598 -7.2319 437.7404 444.9723 438.0889 256.7520 -7.2188 437.7336 444.9525 438.1147 257.5428 -7.2073 437.7236 444.9309 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