DTA measure 12lassu_Pb Date: 2024410:1456 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.15 s Mass = 100.000 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1970 -3.4441 212.2921 215.7363 241.8096 1.9873 -3.4553 212.3643 215.8196 241.7797 2.8090 -3.4686 212.4530 215.9216 241.7509 3.5998 -3.4802 212.5253 216.0055 241.7155 4.4218 -3.4935 212.6161 216.1095 241.7150 5.2140 -3.5051 212.6877 216.1928 241.7078 6.0055 -3.5168 212.7555 216.2723 241.7089 6.8270 -3.5305 212.8407 216.3712 241.7074 7.5870 -3.5431 212.9170 216.4600 241.7075 8.4385 -3.5549 213.0120 216.5668 241.6941 9.2280 -3.5672 213.0911 216.6582 241.7144 10.0193 -3.5779 213.1613 216.7392 241.7426 10.8405 -3.5894 213.2475 216.8369 241.7533 11.6018 -3.6000 213.3249 216.9248 241.7997 12.4535 -3.6114 213.4024 217.0138 241.8246 13.2155 -3.6217 213.4952 217.1170 241.8650 14.0370 -3.6315 213.5655 217.1970 241.9013 14.8585 -3.6409 213.6457 217.2866 241.9204 15.6205 -3.6522 213.7157 217.3678 241.9987 16.4725 -3.6639 213.8148 217.4787 242.0579 17.2335 -3.6740 213.8958 217.5698 242.1197 18.0550 -3.6838 213.9596 217.6434 242.2047 18.8475 -3.6940 214.0386 217.7326 242.2669 19.6395 -3.7042 214.1095 217.8138 242.3524 20.4605 -3.7101 214.2115 217.9216 242.4327 21.2518 -3.7182 214.2840 218.0022 242.5370 22.0743 -3.7283 214.3767 218.1050 242.6409 22.8655 -3.7366 214.4590 218.1956 242.7363 23.6563 -3.7466 214.5480 218.2946 242.8441 24.4783 -3.7554 214.6290 218.3844 242.9846 25.2388 -3.7651 214.7144 218.4795 243.0831 26.0908 -3.7733 214.7893 218.5626 243.2059 26.8823 -3.7827 214.8568 218.6395 243.3343 27.6728 -3.7924 214.9312 218.7236 243.4567 28.4950 -3.8051 215.0433 218.8484 243.5963 29.2550 -3.8113 215.1114 218.9227 243.7349 30.1068 -3.8183 215.1972 219.0155 243.8904 30.8960 -3.8246 215.2702 219.0949 244.0335 31.6860 -3.8336 215.3531 219.1867 244.1817 32.5080 -3.8444 215.4407 219.2851 244.3201 33.2690 -3.8531 215.5116 219.3647 244.4576 34.1208 -3.8583 215.6071 219.4654 244.6200 34.9125 -3.8691 215.6962 219.5653 244.7678 35.7038 -3.8771 215.7718 219.6489 244.9227 36.5235 -3.8830 215.8553 219.7384 245.0792 37.2855 -3.8930 215.9385 219.8315 245.2351 38.1373 -3.9024 216.0211 219.9235 245.3833 38.8985 -3.9112 216.1093 220.0205 245.5244 39.7200 -3.9170 216.2037 220.1207 245.6942 40.5415 -3.9233 216.2811 220.2043 245.8441 41.3020 -3.9112 216.3634 220.2747 245.9808 42.1528 -3.9198 216.4494 220.3693 246.1378 42.9145 -3.9407 216.5403 220.4810 246.2725 43.7365 -3.9587 216.6418 220.6006 246.4431 44.5325 -3.9674 216.7226 220.6900 246.5805 45.3248 -3.9776 216.8095 220.7870 246.7260 46.1765 -3.9847 216.8979 220.8826 246.8736 46.9378 -3.9927 216.9751 220.9678 247.0216 47.7590 -3.9916 217.0612 221.0527 247.1476 48.5495 -3.9742 217.1433 221.1175 247.2925 49.3395 -4.0036 217.2314 221.2351 247.4382 50.1908 -4.0212 217.3571 221.3783 247.5911 50.9508 -4.0316 217.4228 221.4544 247.6993 51.7723 -4.0420 217.5046 221.5466 247.8366 52.5640 -4.0466 217.5902 221.6368 247.9476 53.3548 -4.0505 217.6786 221.7291 248.0716 54.2068 -4.0617 217.7738 221.8355 248.2086 54.9670 -4.0686 217.8572 221.9258 248.3390 55.7880 -4.0739 217.9529 222.0268 248.4585 56.6090 -4.0814 218.0539 222.1353 248.5789 57.3698 -4.0900 218.1453 222.2354 248.6857 58.2218 -4.0994 218.2151 222.3145 248.8168 58.9815 -4.1187 218.2983 222.4170 248.9189 59.8020 -4.1228 218.3882 222.5110 249.0406 60.6235 -4.1217 218.4837 222.6054 249.1429 61.3853 -4.1280 218.5562 222.6843 249.2544 62.2365 -4.1391 218.6588 222.7979 249.3624 62.9975 -4.1474 218.7442 222.8916 249.4658 63.8188 -4.1533 218.8593 223.0126 249.5506 64.7398 -4.1587 218.9535 223.1122 249.6753 65.6038 -4.1677 219.0449 223.2126 249.7960 66.4555 -4.1775 219.1487 223.3262 249.8908 67.2165 -4.1843 219.2378 223.4221 249.9979 68.0385 -4.1929 219.3158 223.5087 250.0747 68.8295 -4.1992 219.4085 223.6077 250.1456 69.6205 -4.2051 219.4985 223.7036 250.2499 70.4715 -4.2099 219.5982 223.8081 250.3351 71.2325 -4.2175 219.6940 223.9115 250.4519 72.0545 -4.2262 219.7865 224.0127 250.5187 72.8455 -4.2316 219.8762 224.1077 250.5916 73.6355 -4.2365 219.9700 224.2065 250.6622 74.4863 -4.2426 220.0400 224.2826 250.7595 75.2470 -4.2490 220.1397 224.3887 250.8370 76.0688 -4.2522 220.2409 224.4930 250.9413 76.8615 -4.2613 220.3370 224.5983 251.0291 77.6525 -4.2662 220.4191 224.6853 251.1007 78.4750 -4.2750 220.4999 224.7749 251.1950 79.2355 -4.2825 220.5929 224.8754 251.2966 80.0878 -4.2869 220.7049 224.9918 251.3799 80.8790 -4.2906 220.8098 225.1004 251.4678 81.6700 -4.2966 220.8871 225.1837 251.5518 82.4920 -4.3000 220.9793 225.2793 251.6568 83.2520 -4.3046 221.0727 225.3773 251.7494 84.1035 -4.3116 221.1526 225.4643 251.8374 84.8635 -4.3151 221.2458 225.5609 251.9140 85.6853 -4.3114 221.3536 225.6649 251.9989 86.5065 -4.3247 221.4530 225.7777 252.0984 87.2683 -4.3304 221.5357 225.8661 252.1857 88.1195 -4.3342 221.6229 225.9571 252.2826 88.8808 -4.3379 221.7152 226.0531 252.3836 89.7020 -4.3435 221.8150 226.1586 252.4528 90.4925 -4.3508 221.9102 226.2610 252.5431 91.2845 -4.3559 221.9983 226.3542 252.6659 92.1365 -4.3612 222.0844 226.4456 252.7573 92.8970 -4.3669 222.1850 226.5519 252.8415 93.7183 -4.3701 222.2792 226.6493 252.9388 94.5085 -4.3771 222.3700 226.7471 253.0385 95.3003 -4.3804 222.4578 226.8382 253.1304 96.1203 -4.3752 222.5454 226.9206 253.2239 96.9110 -4.3836 222.6457 227.0293 253.3451 97.7325 -4.3892 222.7329 227.1221 253.4460 98.5235 -4.3979 222.8405 227.2384 253.5458 99.3140 -4.4044 222.9224 227.3268 253.6440 100.1350 -4.4078 223.0307 227.4385 253.7617 100.9245 -4.4094 223.1239 227.5333 253.8701 101.7458 -4.4157 223.2162 227.6319 253.9801 102.5370 -4.4231 223.3197 227.7428 254.0810 103.3278 -4.4277 223.4143 227.8419 254.1797 104.1490 -4.4290 223.5190 227.9480 254.2729 104.9390 -4.4349 223.5984 228.0333 254.3906 105.7590 -4.4389 223.6938 228.1328 254.5186 106.5500 -4.4461 223.7778 228.2239 254.6121 107.3413 -4.4524 223.8776 228.3300 254.7170 108.1930 -4.4552 223.9752 228.4305 254.8306 108.9540 -4.4596 224.0632 228.5229 254.9451 109.7755 -4.4656 224.1603 228.6258 255.0628 110.5675 -4.4686 224.2588 228.7274 255.1597 111.3580 -4.4733 224.3408 228.8140 255.2652 112.2083 -4.4759 224.4476 228.9236 255.3881 112.9688 -4.4833 224.5537 229.0370 255.4865 113.7900 -4.4901 224.6507 229.1407 255.5970 114.5805 -4.4931 224.7367 229.2298 255.7018 115.3715 -4.4982 224.8354 229.3337 255.8043 116.2225 -4.5012 224.9447 229.4459 255.9259 116.9845 -4.5041 225.0181 229.5222 256.0254 117.8060 -4.5060 225.1085 229.6145 256.1579 118.5975 -4.5125 225.2051 229.7177 256.2586 119.3888 -4.5183 225.3009 229.8191 256.3713 120.2403 -4.5218 225.4068 229.9287 256.5069 121.0008 -4.5265 225.5061 230.0326 256.5978 121.8220 -4.5297 225.5918 230.1216 256.7144 122.6135 -4.5307 225.7106 230.2413 256.8115 123.4048 -4.5360 225.7898 230.3257 256.9229 124.2570 -4.5439 225.9007 230.4446 257.0568 125.0185 -4.5477 225.9929 230.5406 257.1683 125.8398 -4.5523 226.0965 230.6488 257.2805 126.6320 -4.5534 226.1836 230.7370 257.3865 127.4225 -4.5565 226.2691 230.8255 257.4928 128.2740 -4.5623 226.3755 230.9377 257.6145 129.0340 -4.5663 226.4569 231.0232 257.7125 129.8550 -4.5716 226.5569 231.1285 257.8250 130.6460 -4.5777 226.6548 231.2325 257.9451 131.4365 -4.5814 226.7650 231.3464 258.0511 132.2880 -4.5854 226.8519 231.4373 258.1669 133.0498 -4.5902 226.9460 231.5362 258.2755 133.8713 -4.5932 227.0571 231.6503 258.4096 134.6630 -4.5978 227.1485 231.7463 258.5027 135.4535 -4.6012 227.2477 231.8489 258.6150 136.3045 -4.6059 227.3399 231.9458 258.7292 137.0658 -4.6116 227.4177 232.0293 258.8351 137.8870 -4.6154 227.5232 232.1386 258.9330 138.6785 -4.6203 227.6272 232.2475 259.0294 139.4693 -4.6243 227.7382 232.3625 259.1518 140.3205 -4.6276 227.8379 232.4656 259.2769 141.0810 -4.6312 227.9319 232.5631 259.3734 141.9020 -4.6342 228.0373 232.6714 259.4886 142.6935 -4.6348 228.1300 232.7648 259.5900 143.4845 -4.6382 228.2302 232.8684 259.6916 144.3055 -4.6454 228.3324 232.9777 259.8103 145.0960 -4.6482 228.4252 233.0734 259.9284 145.9168 -4.6538 228.5286 233.1824 260.0291 146.6890 -4.6584 228.6256 233.2840 260.1338 147.5233 -4.6632 228.7287 233.3919 260.2576 148.3145 -4.6663 228.8079 233.4741 260.3663 149.1058 -4.6717 228.9031 233.5748 260.4822 149.9273 -4.6766 229.0168 233.6935 260.5955 150.6878 -4.6828 229.1050 233.7878 260.6899 151.5398 -4.6871 229.2265 233.9136 260.7780 152.3310 -4.6882 229.3170 234.0051 260.8987 153.1218 -4.6924 229.4316 234.1240 261.0109 153.9425 -4.6934 229.5333 234.2267 261.1246 154.7025 -4.6970 229.5977 234.2947 261.2176 155.5548 -4.6997 229.7012 234.4009 261.3428 156.3445 -4.7056 229.8070 234.5126 261.4366 157.1350 -4.7084 229.9049 234.6132 261.5392 157.9570 -4.7162 230.0051 234.7213 261.6529 158.7173 -4.7202 230.0960 234.8162 261.7491 159.5690 -4.7235 230.2156 234.9391 261.8698 160.3305 -4.7261 230.3213 235.0474 261.9792 161.1525 -4.7254 230.4378 235.1632 262.0841 161.9435 -4.7313 230.5192 235.2505 262.1916 162.7348 -4.7356 230.6034 235.3390 262.2938 163.5865 -4.7409 230.7197 235.4606 262.4108 164.3485 -4.7433 230.8092 235.5525 262.5101 165.1700 -4.7471 230.8938 235.6409 262.6405 165.9610 -4.7529 230.9967 235.7496 262.7206 166.7518 -4.7557 231.1005 235.8561 262.8279 167.5740 -4.7571 231.1992 235.9563 262.9367 168.3648 -4.7594 231.3030 236.0624 263.0635 169.1855 -4.7658 231.4125 236.1783 263.1685 169.9475 -4.7695 231.4866 236.2561 263.2595 170.7993 -4.7722 231.6273 236.3994 263.3594 171.5888 -4.7762 231.7155 236.4917 263.4650 172.3798 -4.7814 231.8180 236.5994 263.5630 173.2005 -4.7844 231.9164 236.7008 263.6669 173.9615 -4.7896 232.0071 236.7967 263.7759 174.8128 -4.7923 232.1092 236.9015 263.8889 175.6035 -4.7940 232.2106 237.0047 263.9925 176.3940 -4.7986 232.3054 237.1040 264.0986 177.2163 -4.8023 232.4115 237.2138 264.1941 177.9760 -4.8041 232.5112 237.3154 264.2902 178.8280 -4.8092 232.6199 237.4291 264.3994 179.6203 -4.8135 232.7332 237.5468 264.4904 180.4113 -4.8185 232.8130 237.6315 264.5781 181.2315 -4.8206 232.9153 237.7358 264.7012 181.9908 -4.8234 233.0253 237.8487 264.7974 182.8428 -4.8243 233.1257 237.9499 264.9131 183.6328 -4.8274 233.2241 238.0515 265.0159 184.4220 -4.8309 233.3142 238.1451 265.1175 185.2420 -4.8338 233.4266 238.2604 265.2090 186.0323 -4.8382 233.5326 238.3708 265.2836 186.8533 -4.8423 233.6251 238.4674 265.3981 187.6053 -4.8459 233.7197 238.5656 265.5024 188.4798 -4.8465 233.8310 238.6775 265.5996 189.2408 -4.8497 233.9429 238.7926 265.6854 190.0625 -4.8533 234.0248 238.8781 265.7991 190.8543 -4.8563 234.1407 238.9970 265.8862 191.6463 -4.8609 234.2271 239.0880 265.9867 192.4675 -4.8641 234.3367 239.2007 266.0762 193.2585 -4.8682 234.4561 239.3244 266.1704 194.0805 -4.8672 234.5589 239.4261 266.2923 194.8725 -4.8715 234.6559 239.5273 266.3927 195.6643 -4.8756 234.7430 239.6186 266.4939 196.4855 -4.8788 234.8533 239.7321 266.5813 197.2775 -4.8838 234.9556 239.8394 266.6796 198.0990 -4.8852 235.0649 239.9501 266.7669 198.8903 -4.8875 235.1771 240.0645 266.8613 199.6810 -4.8898 235.2780 240.1678 266.9474 200.5023 -4.8887 235.3667 240.2554 267.0607 201.2930 -4.8927 235.4658 240.3585 267.1630 202.1143 -4.8979 235.5591 240.4570 267.2718 202.9050 -4.9015 235.6780 240.5795 267.3584 203.6958 -4.9024 235.7775 240.6798 267.4565 204.5170 -4.9052 235.8696 240.7749 267.5656 205.3078 -4.9096 235.9736 240.8832 267.6563 206.1298 -4.9117 236.0756 240.9873 267.7501 206.9223 -4.9152 236.1753 241.0906 267.8449 207.7145 -4.9177 236.2846 241.2024 267.9452 208.5330 -4.9207 236.3885 241.3092 268.0294 209.3245 -4.9247 236.4945 241.4192 268.1092 210.1468 -4.9270 236.5861 241.5131 268.2185 210.9068 -4.9310 236.6949 241.6258 268.3098 211.7588 -4.9343 236.8109 241.7452 268.4211 212.5495 -4.9378 236.9056 241.8434 268.5085 213.3413 -4.9389 237.0066 241.9455 268.5979 214.1625 -4.9405 237.1109 242.0514 268.7191 214.9238 -4.9434 237.2160 242.1594 268.8063 215.7755 -4.9462 237.3164 242.2626 268.9148 216.5368 -4.9499 237.4061 242.3561 268.9876 217.3580 -4.9527 237.5160 242.4687 269.0937 218.1795 -4.9560 237.6229 242.5788 269.2045 218.9415 -4.9592 237.7130 242.6722 269.3095 219.7935 -4.9586 237.8462 242.8049 269.4234 220.5560 -4.9610 237.9462 242.9072 269.5150 221.3833 -4.9660 238.0361 243.0021 269.6273 222.1745 -4.9672 238.1397 243.1068 269.7357 222.9665 -4.9700 238.2502 243.2202 269.8359 223.7885 -4.9720 238.3297 243.3017 269.9446 224.5485 -4.9774 238.4481 243.4255 270.0564 225.4003 -4.9798 238.5688 243.5486 270.1726 226.1923 -4.9825 238.6707 243.6531 270.2681 226.9833 -4.9850 238.7650 243.7500 270.3744 227.8053 -4.9846 238.8447 243.8293 270.4847 228.5770 -4.9864 238.9503 243.9367 270.6128 229.4090 -4.9896 239.0676 244.0572 270.7254 230.1700 -4.9927 239.1770 244.1698 270.8346 231.0218 -4.9926 239.2838 244.2764 270.9513 231.7820 -4.9969 239.3802 244.3771 271.0630 232.6030 -5.0014 239.4678 244.4692 271.1832 233.4240 -5.0076 239.5864 244.5941 271.2919 234.1850 -5.0075 239.6787 244.6862 271.4064 235.0365 -5.0107 239.7933 244.8039 271.5457 235.7958 -5.0121 239.9011 244.9132 271.6483 236.6170 -5.0145 240.0009 245.0154 271.7804 237.4078 -5.0176 240.1117 245.1293 271.8802 238.1985 -5.0173 240.2007 245.2180 271.9853 239.0495 -5.0185 240.3180 245.3365 272.0993 239.8115 -5.0223 240.4252 245.4475 272.2285 240.6330 -5.0280 240.5326 245.5607 272.3551 241.4243 -5.0301 240.6229 245.6531 272.4543 242.2155 -5.0337 240.7184 245.7521 272.5675 243.0375 -5.0365 240.8202 245.8567 272.6956 243.8285 -5.0412 240.9237 245.9649 272.8130 244.6503 -5.0420 241.0476 246.0896 272.9322 245.4415 -5.0469 241.1629 246.2098 273.0426 246.2328 -5.0470 241.2603 246.3072 273.1515 247.0545 -5.0508 241.3594 246.4103 273.2422 247.8448 -5.0530 241.4869 246.5399 273.3515 248.6663 -5.0552 241.5891 246.6442 273.4545 249.4318 -5.0577 241.6803 246.7380 273.5803 250.2835 -5.0617 241.7865 246.8482 273.6695 251.0435 -5.0619 241.8759 246.9377 273.7784 251.8648 -5.0625 241.9875 247.0500 273.8893 252.6853 -5.0666 242.1020 247.1686 273.9998 253.4465 -5.0692 242.1986 247.2678 274.0840 254.2988 -5.0735 242.3058 247.3793 274.1861 255.0590 -5.0761 242.4123 247.4884 274.2758 255.8800 -5.0764 242.5170 247.5933 274.3892 256.7010 -5.0801 242.6247 247.7048 274.4829 257.4625 -5.0822 242.7197 247.8019 274.5844 258.3150 -5.0810 242.8333 247.9143 274.6861 259.0743 -5.0834 242.9370 248.0204 274.7801 259.8840 -5.0872 243.0441 248.1314 274.8740 260.7055 -5.0876 243.1440 248.2317 274.9512 261.4958 -5.0891 243.2534 248.3425 275.0354 262.2875 -5.0923 243.3506 248.4429 275.1281 263.1398 -5.0942 243.4660 248.5602 275.2244 263.9015 -5.0959 243.5703 248.6662 275.3059 264.7238 -5.0987 243.6726 248.7713 275.3942 265.5145 -5.0997 243.7733 248.8729 275.4984 266.3060 -5.1005 243.8679 248.9684 275.5815 267.1575 -5.1028 243.9818 249.0846 275.6686 267.9178 -5.1048 244.0767 249.1815 275.7551 268.7378 -5.1070 244.1829 249.2899 275.8473 269.5575 -5.1125 244.3085 249.4210 275.9462 270.3185 -5.1141 244.4102 249.5243 276.0418 271.1728 -5.1160 244.5246 249.6407 276.1470 271.9345 -5.1202 244.6147 249.7349 276.2280 272.7565 -5.1176 244.7264 249.8440 276.3200 273.5485 -5.1202 244.8153 249.9355 276.4395 274.3398 -5.1229 244.9317 250.0546 276.5382 275.1913 -5.1242 245.0521 250.1763 276.6287 275.9510 -5.1274 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