DTA measure 1gyors_Pb Date: 2024410:139 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.19 s Mass = 1118.200 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1758 -3.0460 256.1943 259.2403 264.0348 1.9970 -3.0409 256.2248 259.2658 264.0368 2.8185 -3.0378 256.2516 259.2894 264.0137 3.5798 -3.0323 256.2789 259.3113 264.0397 4.4305 -3.0239 256.3191 259.3430 264.0324 5.2208 -3.0164 256.3666 259.3830 264.0513 6.0125 -3.0084 256.3802 259.3886 264.0650 6.8330 -3.0027 256.4232 259.4259 264.0732 7.5920 -2.9958 256.4483 259.4441 264.0702 8.4440 -2.9959 256.4724 259.4683 264.0919 9.2355 -2.9949 256.4907 259.4856 264.1236 10.0265 -3.0024 256.5413 259.5437 264.1163 10.9495 -2.9956 256.5951 259.5907 264.1453 11.8100 -2.9857 256.6095 259.5952 264.1821 12.6618 -2.9786 256.6309 259.6095 264.2165 13.4515 -2.9735 256.6814 259.6549 264.2389 14.2420 -2.9655 256.7174 259.6830 264.2668 15.0640 -2.9577 256.7507 259.7084 264.3050 15.8255 -2.9489 256.7787 259.7276 264.3535 16.6778 -2.9423 256.8058 259.7481 264.4153 17.4380 -2.9432 256.8311 259.7743 264.4609 18.2588 -2.9397 256.8639 259.8036 264.5414 19.0795 -2.9300 256.9049 259.8349 264.6051 19.8415 -2.9216 256.9428 259.8644 264.6751 20.6935 -2.9159 256.9795 259.8954 264.7595 21.4543 -2.9126 256.9898 259.9024 264.8309 22.2750 -2.9074 257.0225 259.9299 264.9119 23.0965 -2.9016 257.0492 259.9508 265.0020 23.8575 -2.8949 257.0786 259.9735 265.1025 24.7088 -2.8911 257.1092 260.0003 265.2126 25.4705 -2.8873 257.1416 260.0290 265.3150 26.2918 -2.8796 257.2031 260.0827 265.4180 27.1115 -2.8736 257.2251 260.0987 265.5353 27.8725 -2.8709 257.2405 260.1114 265.6477 28.7225 -2.8672 257.2663 260.1335 265.7835 29.4818 -2.8645 257.2873 260.1518 265.8948 30.3035 -2.8654 257.3437 260.2091 266.0203 31.1255 -2.8683 257.3551 260.2234 266.1542 31.8868 -2.8683 257.3928 260.2611 266.2931 32.7385 -2.8646 257.4293 260.2939 266.4616 33.4995 -2.8622 257.4520 260.3141 266.5984 34.3208 -2.8590 257.4779 260.3369 266.7332 35.1423 -2.8546 257.5275 260.3820 266.9016 35.9035 -2.8528 257.5600 260.4128 267.0389 36.7558 -2.8546 257.5817 260.4362 267.2123 37.5160 -2.8495 257.5975 260.4469 267.3571 38.3378 -2.8500 257.6207 260.4707 267.5018 39.1300 -2.8460 257.6636 260.5096 267.6557 39.9208 -2.8430 257.6908 260.5338 267.8185 40.7430 -2.8438 257.7366 260.5804 267.9934 41.5040 -2.8390 257.7670 260.6060 268.1432 42.3588 -2.8356 257.8122 260.6477 268.3240 43.1500 -2.8340 257.8641 260.6981 268.4996 43.9415 -2.8308 257.8723 260.7031 268.6656 44.7638 -2.8264 257.9008 260.7272 268.8419 45.5250 -2.8289 257.9308 260.7596 268.9898 46.3765 -2.8297 257.9773 260.8070 269.1591 47.1385 -2.8286 258.0029 260.8315 269.2987 47.9605 -2.8307 258.0206 260.8513 269.4647 48.7825 -2.8291 258.0613 260.8903 269.6515 49.5438 -2.8318 258.0949 260.9267 269.8046 50.3943 -2.8252 258.1291 260.9543 269.9821 51.1545 -2.8294 258.1614 260.9908 270.1213 51.9763 -2.8402 258.1905 261.0307 270.2844 52.7975 -2.8440 258.2263 261.0703 270.4489 53.5595 -2.8408 258.2533 261.0941 270.6154 54.4103 -2.8451 258.3021 261.1472 270.7839 55.1715 -2.8399 258.3324 261.1723 270.9079 55.9930 -2.8341 258.3641 261.1982 271.0542 56.7845 -2.8330 258.3985 261.2315 271.2020 57.5765 -2.8442 258.4482 261.2924 271.3609 58.4280 -2.8514 258.4838 261.3352 271.5106 59.1895 -2.8538 258.5269 261.3808 271.6534 60.0095 -2.8545 258.5426 261.3971 271.7840 60.8013 -2.8567 258.5935 261.4502 271.9275 61.5923 -2.8607 258.6074 261.4681 272.0499 62.4438 -2.8579 258.6643 261.5222 272.2106 63.2048 -2.8569 258.6988 261.5556 272.3383 64.0288 -2.8605 258.7313 261.5918 272.4796 64.8210 -2.8650 258.7611 261.6261 272.6121 65.6125 -2.8678 258.8154 261.6832 272.7276 66.4345 -2.8705 258.8284 261.6990 272.8732 67.2245 -2.8750 258.8606 261.7356 272.9927 68.0455 -2.8787 258.9085 261.7873 273.1291 68.8660 -2.8814 258.9551 261.8365 273.2438 69.6575 -2.8829 258.9778 261.8607 273.3558 70.4783 -2.8756 259.0311 261.9067 273.4647 71.2710 -2.8803 259.0748 261.9551 273.6064 72.0623 -2.8852 259.1128 261.9980 273.7253 72.9133 -2.8831 259.1552 262.0382 273.8501 73.6728 -2.8876 259.1815 262.0692 273.9399 74.4945 -2.8965 259.2179 262.1143 274.0679 75.2865 -2.9050 259.2513 262.1563 274.1821 76.0785 -2.9130 259.2925 262.2055 274.2891 76.9305 -2.9101 259.3418 262.2519 274.4002 77.6918 -2.9092 259.3767 262.2859 274.5237 78.5148 -2.9100 259.4282 262.3382 274.6254 79.3063 -2.9152 259.4493 262.3644 274.7559 80.0970 -2.9194 259.4742 262.3936 274.8484 80.9180 -2.9218 259.5209 262.4427 274.9667 81.7088 -2.9292 259.5667 262.4959 275.0574 82.5303 -2.9365 259.6208 262.5573 275.1760 83.3215 -2.9386 259.6639 262.6025 275.3046 84.1135 -2.9411 259.6935 262.6346 275.4053 84.9353 -2.9447 259.7455 262.6902 275.5006 85.7255 -2.9458 259.7812 262.7270 275.5944 86.5463 -2.9508 259.8378 262.7887 275.7232 87.3368 -2.9582 259.8742 262.8324 275.8336 88.1270 -2.9602 259.9124 262.8727 275.9283 88.9490 -2.9641 259.9626 262.9267 276.0379 89.7400 -2.9674 260.0115 262.9789 276.1538 90.5618 -2.9734 260.0369 263.0103 276.2553 91.3535 -2.9794 260.0607 263.0400 276.4005 92.1445 -2.9831 260.1179 263.1011 276.4996 92.9670 -2.9868 260.1527 263.1395 276.6134 93.7580 -2.9959 260.1728 263.1688 276.7157 94.5793 -3.0014 260.2417 263.2431 276.8204 95.3705 -3.0058 260.2689 263.2747 276.9390 96.1610 -3.0082 260.3217 263.3299 277.0585 96.9828 -3.0133 260.3872 263.4005 277.1624 97.7728 -3.0137 260.4183 263.4320 277.2761 98.5940 -3.0239 260.4648 263.4887 277.4096 99.3853 -3.0291 260.4994 263.5285 277.5240 100.1765 -3.0367 260.5233 263.5601 277.6501 100.9985 -3.0446 260.5994 263.6440 277.7949 101.7905 -3.0503 260.6371 263.6875 277.8909 102.6125 -3.0548 260.6772 263.7320 278.0104 103.4045 -3.0576 260.7248 263.7824 278.1396 104.1965 -3.0645 260.7649 263.8294 278.2554 105.0180 -3.0713 260.8047 263.8760 278.3891 105.7785 -3.0793 260.8415 263.9209 278.5166 106.6305 -3.0859 260.9266 264.0125 278.6372 107.4215 -3.0919 260.9655 264.0574 278.7477 108.2135 -3.0961 261.0123 264.1084 278.8687 109.0343 -3.1024 261.0596 264.1620 279.0067 109.7945 -3.1070 261.0974 264.2044 279.1223 110.6465 -3.1118 261.1595 264.2713 279.2673 111.4085 -3.1213 261.1848 264.3061 279.3750 112.2295 -3.1270 261.2473 264.3744 279.4924 113.0513 -3.1326 261.2949 264.4275 279.6243 113.8105 -3.1383 261.3320 264.4703 279.7288 114.6613 -3.1420 261.3782 264.5202 279.8649 115.4228 -3.1514 261.4246 264.5761 279.9949 116.2445 -3.1606 261.4691 264.6297 280.1366 117.0360 -3.1671 261.5389 264.7060 280.2771 117.8270 -3.1721 261.5728 264.7449 280.3734 118.6790 -3.1797 261.6137 264.7934 280.5159 119.4400 -3.1882 261.6816 264.8698 280.6518 120.2618 -3.1936 261.7181 264.9117 280.7673 121.0538 -3.1996 261.7482 264.9479 280.8966 121.8443 -3.2058 261.8073 265.0131 281.0205 122.6955 -3.2138 261.8834 265.0972 281.1761 123.4558 -3.2223 261.9161 265.1384 281.3030 124.2768 -3.2273 261.9461 265.1734 281.4297 125.0673 -3.2332 262.0229 265.2561 281.5744 125.8583 -3.2313 262.1031 265.3344 281.7211 126.6795 -3.2431 262.1365 265.3796 281.8559 127.4708 -3.2543 262.1762 265.4305 282.0014 128.2925 -3.2628 262.2182 265.4810 282.1441 129.0835 -3.2656 262.2836 265.5492 282.2924 129.8753 -3.2722 262.3335 265.6057 282.4104 130.6965 -3.2828 262.4049 265.6877 282.5744 131.4878 -3.2892 262.4401 265.7294 282.7266 132.3095 -3.2976 262.4927 265.7902 282.8465 133.1005 -3.3036 262.5406 265.8442 282.9876 133.8915 -3.3116 262.5900 265.9016 283.1247 134.7125 -3.3214 262.6601 265.9815 283.2717 135.4745 -3.3261 262.7078 266.0339 283.3928 136.3265 -3.3362 262.7777 266.1139 283.5508 137.1185 -3.3455 262.8437 266.1892 283.6903 137.9085 -3.3545 262.8686 266.2231 283.8395 138.7283 -3.3624 262.9205 266.2829 283.9980 139.4888 -3.3699 262.9804 266.3504 284.1153 140.3410 -3.3784 263.0361 266.4146 284.2669 141.1330 -3.3842 263.0990 266.4831 284.4136 141.9243 -3.3914 263.1575 266.5489 284.5368 142.7460 -3.4036 263.2237 266.6273 284.6865 143.5068 -3.4120 263.2834 266.6954 284.8164 144.3588 -3.4194 263.3281 266.7475 284.9403 145.1198 -3.4291 263.3903 266.8194 285.0625 145.9418 -3.4334 263.4324 266.8658 285.2056 146.7640 -3.4396 263.4819 266.9215 285.3344 147.5258 -3.4516 263.5508 267.0024 285.4506 148.3773 -3.4609 263.6179 267.0788 285.6003 149.1375 -3.4699 263.6805 267.1504 285.7021 149.9595 -3.4803 263.7266 267.2068 285.8200 150.7815 -3.4912 263.7897 267.2809 285.9568 151.5435 -3.5000 263.8364 267.3363 286.0534 152.3953 -3.5082 263.8951 267.4033 286.1904 153.1555 -3.5109 263.9571 267.4681 286.3093 153.9773 -3.5199 264.0435 267.5634 286.4321 154.7978 -3.5287 264.0815 267.6101 286.5352 155.5583 -3.5414 264.1534 267.6948 286.6348 156.4093 -3.5504 264.2179 267.7684 286.7628 157.1705 -3.5589 264.2773 267.8362 286.8845 157.9923 -3.5635 264.3350 267.8985 286.9913 158.8135 -3.5704 264.4067 267.9771 287.1043 159.5755 -3.5793 264.4573 268.0366 287.2015 160.4265 -3.5875 264.5210 268.1085 287.3368 161.1875 -3.5960 264.5716 268.1676 287.4508 162.0093 -3.6039 264.6173 268.2212 287.5539 162.8303 -3.6116 264.7007 268.3123 287.6867 163.5905 -3.6203 264.7783 268.3987 287.7985 164.4423 -3.6282 264.8425 268.4707 287.9282 165.2030 -3.6365 264.8975 268.5340 288.0293 166.0248 -3.6475 264.9643 268.6119 288.1506 166.8170 -3.6534 265.0232 268.6766 288.2841 167.6080 -3.6621 265.0874 268.7495 288.4024 168.4615 -3.6689 265.1299 268.7987 288.5447 169.2230 -3.6797 265.2038 268.8835 288.6523 170.0448 -3.6868 265.2895 268.9763 288.7752 170.8365 -3.6950 265.3448 269.0398 288.8744 171.6270 -3.7040 265.3938 269.0978 289.0281 172.4790 -3.7143 265.4760 269.1903 289.1478 173.2408 -3.7229 265.5507 269.2736 289.2534 174.0618 -3.7306 265.5984 269.3290 289.3691 174.8530 -3.7356 265.6733 269.4089 289.5037 175.6440 -3.7420 265.7342 269.4761 289.6495 176.4655 -3.7521 265.7969 269.5490 289.7751 177.2265 -3.7581 265.8556 269.6136 289.8967 178.0783 -3.7711 265.9239 269.6950 290.0212 178.8683 -3.7834 265.9903 269.7737 290.1479 179.6588 -3.7933 266.0484 269.8417 290.2755 180.4805 -3.8029 266.1394 269.9423 290.4322 181.2418 -3.8131 266.2080 270.0211 290.5741 182.0935 -3.8228 266.2669 270.0897 290.6918 182.8845 -3.8343 266.3314 270.1657 290.8146 183.6765 -3.8438 266.4083 270.2522 290.9462 184.4973 -3.8500 266.4718 270.3218 291.1034 185.2580 -3.8574 266.5469 270.4043 291.2317 186.1093 -3.8659 266.6195 270.4854 291.3675 186.8695 -3.8767 266.6694 270.5462 291.4960 187.6908 -3.8837 266.7449 270.6286 291.6274 188.5108 -3.8904 266.8245 270.7149 291.7649 189.2713 -3.9010 266.8811 270.7821 291.9120 190.1228 -3.9081 266.9758 270.8839 292.0590 190.9133 -3.9165 267.0373 270.9538 292.1987 191.7043 -3.9245 267.1020 271.0265 292.3212 192.5253 -3.9334 267.1758 271.1092 292.4761 193.2860 -3.9432 267.2479 271.1911 292.6019 194.1380 -3.9481 267.3173 271.2654 292.7381 194.8998 -3.9583 267.3762 271.3345 292.8742 195.7215 -3.9649 267.4570 271.4219 293.0242 196.5165 -3.9771 267.5302 271.5073 293.1666 197.3085 -3.9873 267.6084 271.5957 293.3091 198.1310 -3.9924 267.6836 271.6760 293.4511 198.9228 -4.0042 267.7501 271.7542 293.5668 199.7445 -4.0149 267.8381 271.8530 293.7102 200.5365 -4.0240 267.9203 271.9443 293.8535 201.3285 -4.0317 267.9724 272.0041 293.9996 202.1505 -4.0435 268.0425 272.0860 294.1520 202.9125 -4.0524 268.1244 272.1768 294.2709 203.7633 -4.0571 268.2198 272.2769 294.4273 204.5545 -4.0682 268.2951 272.3633 294.5548 205.3465 -4.0750 268.3605 272.4355 294.6791 206.1668 -4.0840 268.4477 272.5317 294.8431 206.9278 -4.0977 268.5284 272.6261 294.9679 207.7793 -4.1004 268.5726 272.6730 295.1028 208.5688 -4.1061 268.6521 272.7582 295.2517 209.3603 -4.1162 268.7341 272.8502 295.4070 210.1803 -4.1256 268.8151 272.9407 295.5560 210.9408 -4.1371 268.8823 273.0194 295.6651 211.7913 -4.1452 268.9806 273.1258 295.7903 212.5808 -4.1554 269.0387 273.1941 295.9391 213.3713 -4.1627 269.1113 273.2740 296.0732 214.1913 -4.1731 269.1926 273.3656 296.2177 214.9523 -4.1821 269.2814 273.4635 296.3301 215.8038 -4.1905 269.3543 273.5448 296.4798 216.5953 -4.1969 269.4408 273.6377 296.5962 217.3863 -4.2069 269.5171 273.7240 296.7284 218.2080 -4.2146 269.5941 273.8087 296.8536 218.9685 -4.2251 269.6925 273.9175 296.9598 219.8200 -4.2331 269.7688 274.0019 297.0807 220.5818 -4.2397 269.8463 274.0861 297.1799 221.4038 -4.2476 269.9247 274.1723 297.3097 222.2260 -4.2569 269.9904 274.2473 297.4167 222.9865 -4.2673 270.0606 274.3279 297.5393 223.8378 -4.2771 270.1478 274.4249 297.6649 224.5988 -4.2838 270.2305 274.5143 297.7647 225.4205 -4.2912 270.3139 274.6051 297.8884 226.2278 -4.3011 270.4045 274.7056 297.9915 227.0245 -4.3131 270.4783 274.7915 298.1196 227.8465 -4.3245 270.5536 274.8781 298.2426 228.6075 -4.3322 270.6228 274.9550 298.3550 229.4593 -4.3373 270.7328 275.0701 298.4852 230.2195 -4.3457 270.8093 275.1550 298.5968 231.0413 -4.3541 270.8914 275.2455 298.7275 231.8625 -4.3637 270.9637 275.3275 298.8393 232.6240 -4.3723 271.0523 275.4246 298.9466 233.4755 -4.3817 271.1225 275.5041 299.0696 234.2365 -4.3894 271.2081 275.5975 299.1714 235.0585 -4.3994 271.3069 275.7063 299.3082 235.8805 -4.4044 271.4006 275.8050 299.4458 236.6403 -4.4123 271.4589 275.8711 299.5386 237.4915 -4.4200 271.5476 275.9676 299.6775 238.2523 -4.4293 271.6273 276.0566 299.7977 239.0733 -4.4391 271.7261 276.1652 299.9240 239.8943 -4.4475 271.8114 276.2589 300.0406 240.6560 -4.4570 271.8750 276.3320 300.1496 241.5080 -4.4634 271.9798 276.4431 300.2904 242.2688 -4.4714 272.0446 276.5160 300.3892 243.0900 -4.4808 272.1472 276.6280 300.5303 243.9093 -4.4897 272.2270 276.7167 300.6439 244.6700 -4.4978 272.3129 276.8107 300.7465 245.5220 -4.5044 272.4066 276.9111 300.8987 246.3130 -4.5123 272.4892 277.0014 301.0269 247.1045 -4.5212 272.5892 277.1104 301.1662 247.9270 -4.5300 272.6569 277.1869 301.2896 248.6875 -4.5366 272.7346 277.2712 301.4255 249.5400 -4.5462 272.8447 277.3909 301.5685 250.3018 -4.5524 272.9260 277.4785 301.7076 251.1235 -4.5606 273.0031 277.5637 301.8464 251.9450 -4.5700 273.1038 277.6738 301.9692 252.7055 -4.5801 273.1792 277.7593 302.0932 253.5568 -4.5880 273.2927 277.8806 302.2428 254.3175 -4.5961 273.3696 277.9657 302.3696 255.1395 -4.6049 273.4663 278.0712 302.5167 255.9315 -4.6153 273.5441 278.1594 302.6343 256.7225 -4.6208 273.6428 278.2636 302.8056 257.5725 -4.6290 273.7234 278.3524 302.9437 258.3340 -4.6365 273.7994 278.4358 303.0864 259.1550 -4.6454 273.8995 278.5450 303.2474 259.9465 -4.6562 273.9933 278.6495 303.3791 260.7380 -4.6642 274.0614 278.7256 303.5245 261.5595 -4.6730 274.1594 278.8323 303.6575 262.3515 -4.6813 274.2419 278.9232 303.8070 263.1730 -4.6865 274.3354 279.0220 303.9518 263.9643 -4.6960 274.4224 279.1184 304.0839 264.7550 -4.7037 274.5170 279.2207 304.2369 265.5765 -4.7122 274.6095 279.3216 304.3814 266.3373 -4.7222 274.7014 279.4236 304.5027 267.1890 -4.7316 274.8101 279.5416 304.6596 267.9800 -4.7399 274.8985 279.6383 304.7849 268.7708 -4.7474 274.9940 279.7414 304.9299 269.5930 -4.7579 275.0908 279.8487 305.0818 270.3538 -4.7667 275.1562 279.9229 305.2070 271.2060 -4.7718 275.2684 280.0402 305.3620 271.9668 -4.7801 275.3659 280.1461 305.4930 272.7885 -4.7877 275.4494 280.2371 305.6372 273.6100 -4.7984 275.5433 280.3417 305.7771 274.3705 -4.8037 275.6249 280.4286 305.8975 275.2220 -4.8082 275.7311 280.5393 306.0332 275.9838 -4.8171 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