DTA measure 1lassumeres Date: 2024423:1554 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.45 s Mass = 5000.000 mg data_number = 1586 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1570 -0.6951 248.0626 248.7577 265.9092 1.9178 -0.6928 248.1915 248.8843 265.9273 2.7693 -0.6864 248.3416 249.0280 265.9329 3.5588 -0.6788 248.4849 249.1637 265.9498 4.3498 -0.6725 248.6188 249.2913 265.9723 5.1705 -0.6709 248.7680 249.4389 265.9863 5.9325 -0.6675 248.9107 249.5781 266.0229 6.7848 -0.6620 249.0571 249.7191 266.0236 7.5765 -0.6566 249.1787 249.8353 266.0638 8.3685 -0.6518 249.3378 249.9897 266.1014 9.1908 -0.6499 249.4797 250.1295 266.1623 9.9525 -0.6411 249.6149 250.2559 266.2028 10.8045 -0.6389 249.7584 250.3972 266.2699 11.5965 -0.6336 249.9054 250.5390 266.3253 12.3890 -0.6300 250.0433 250.6733 266.3905 13.2135 -0.6224 250.1963 250.8187 266.4752 13.9755 -0.6163 250.3224 250.9387 266.5432 14.8275 -0.6160 250.4617 251.0778 266.6550 15.5895 -0.6117 250.5914 251.2030 266.7349 16.4115 -0.6054 250.7277 251.3330 266.8310 17.2335 -0.6005 250.8704 251.4709 266.9304 17.9955 -0.5961 250.9929 251.5890 267.0325 18.8475 -0.5965 251.1510 251.7474 267.1522 19.6095 -0.5950 251.2760 251.8710 267.2727 20.4308 -0.5915 251.4192 252.0107 267.3821 21.2530 -0.5843 251.5568 252.1411 267.5175 22.0150 -0.5777 251.6711 252.2487 267.6243 22.8670 -0.5746 251.8149 252.3895 267.7698 23.6588 -0.5774 251.9630 252.5404 267.9000 24.4505 -0.5772 252.0974 252.6746 268.0521 25.2728 -0.5753 252.2472 252.8225 268.1917 26.0360 -0.5739 252.3701 252.9440 268.3228 26.8890 -0.5691 252.5112 253.0803 268.4676 27.6475 -0.5669 252.6419 253.2089 268.5930 28.4658 -0.5636 252.7824 253.3460 268.7298 29.2830 -0.5630 252.9223 253.4853 268.8688 30.0420 -0.5614 253.0416 253.6031 268.9991 30.8923 -0.5612 253.1844 253.7456 269.1282 31.6503 -0.5598 253.3097 253.8695 269.2549 32.4703 -0.5582 253.4562 254.0144 269.4083 33.2908 -0.5574 253.5853 254.1428 269.5216 34.0520 -0.5547 253.7138 254.2685 269.6499 34.9033 -0.5528 253.8572 254.4100 269.7603 35.6648 -0.5534 253.9881 254.5415 269.8645 36.4875 -0.5512 254.1237 254.6749 270.0002 37.2790 -0.5476 254.2638 254.8114 270.1050 38.0708 -0.5465 254.3871 254.9336 270.2223 38.8930 -0.5468 254.5308 255.0776 270.3320 39.6545 -0.5449 254.6543 255.1992 270.4297 40.5068 -0.5443 254.7861 255.3304 270.5383 41.2988 -0.5430 254.9148 255.4578 270.6459 42.0915 -0.5416 255.0433 255.5849 270.7530 42.9138 -0.5383 255.1938 255.7321 270.8487 43.6755 -0.5386 255.3141 255.8527 270.9551 44.5283 -0.5396 255.4596 255.9992 271.0610 45.2905 -0.5389 255.5908 256.1297 271.1742 46.1128 -0.5366 255.7268 256.2635 271.2674 46.9348 -0.5374 255.8511 256.3885 271.3700 47.6965 -0.5360 255.9709 256.5069 271.4427 48.5488 -0.5359 256.1138 256.6498 271.5624 49.3105 -0.5356 256.2334 256.7691 271.6589 50.1325 -0.5368 256.3762 256.9129 271.7685 50.9545 -0.5357 256.5168 257.0525 271.8820 51.7165 -0.5357 256.6479 257.1836 271.9727 52.5685 -0.5321 256.7862 257.3183 272.0784 53.3605 -0.5322 256.9176 257.4498 272.1700 54.1525 -0.5328 257.0357 257.5685 272.2747 54.9748 -0.5325 257.1763 257.7088 272.3839 55.7375 -0.5343 257.3108 257.8451 272.4763 56.5900 -0.5329 257.4622 257.9951 272.5835 57.3825 -0.5325 257.5640 258.0965 272.6895 58.1753 -0.5313 257.6932 258.2245 272.7801 58.9953 -0.5322 257.8327 258.3649 272.8858 59.7550 -0.5311 257.9526 258.4837 272.9737 60.6038 -0.5345 258.0954 258.6299 273.0888 61.3630 -0.5358 258.2181 258.7539 273.1744 62.1823 -0.5374 258.3642 258.9016 273.2638 63.0015 -0.5385 258.4918 259.0303 273.3670 63.7613 -0.5396 258.6106 259.1502 273.4455 64.6118 -0.5386 258.7463 259.2848 273.5376 65.3585 -0.5400 258.8630 259.4030 273.6348 66.2155 -0.5391 258.9941 259.5333 273.7318 66.9775 -0.5385 259.1229 259.6614 273.8181 67.7995 -0.5397 259.2738 259.8136 273.9240 68.6215 -0.5410 259.4009 259.9419 274.0234 69.3835 -0.5426 259.5165 260.0592 274.1208 70.2355 -0.5425 259.6517 260.1942 274.2244 70.9975 -0.5434 259.7745 260.3179 274.3398 71.8195 -0.5449 259.8987 260.4436 274.4555 72.6420 -0.5457 260.0325 260.5781 274.5653 73.4045 -0.5458 260.1611 260.7069 274.6779 74.2565 -0.5477 260.3105 260.8582 274.7999 75.0185 -0.5477 260.4353 260.9830 274.9008 75.8403 -0.5462 260.5641 261.1103 275.0261 76.6623 -0.5488 260.6951 261.2439 275.1580 77.4243 -0.5506 260.8060 261.3566 275.2650 78.2765 -0.5517 260.9397 261.4914 275.3888 79.0680 -0.5535 261.0578 261.6113 275.5071 79.8608 -0.5544 261.1906 261.7450 275.6318 80.6828 -0.5558 261.3143 261.8701 275.7476 81.4445 -0.5550 261.4524 262.0074 275.8613 82.2973 -0.5581 261.5887 262.1468 275.9927 83.0595 -0.5588 261.7094 262.2682 276.1191 83.8818 -0.5622 261.8450 262.4072 276.2618 84.7038 -0.5628 261.9754 262.5382 276.3641 85.4655 -0.5642 262.0922 262.6564 276.4623 86.3178 -0.5641 262.2248 262.7889 276.5753 87.1098 -0.5659 262.3613 262.9273 276.6802 87.9015 -0.5686 262.4843 263.0529 276.8009 88.7235 -0.5698 262.6009 263.1707 276.9115 89.4855 -0.5713 262.7264 263.2977 277.0147 90.3375 -0.5731 262.8671 263.4401 277.1232 91.1263 -0.5755 262.9753 263.5508 277.2308 91.9158 -0.5781 263.1001 263.6781 277.3301 92.7348 -0.5784 263.2436 263.8220 277.4238 93.4940 -0.5800 263.3597 263.9397 277.5220 94.3430 -0.5813 263.4945 264.0758 277.6386 95.1020 -0.5832 263.6068 264.1900 277.7204 95.9215 -0.5863 263.7324 264.3187 277.8098 96.7408 -0.5873 263.8688 264.4561 277.9163 97.5010 -0.5875 263.9827 264.5702 278.0250 98.3518 -0.5902 264.1307 264.7209 278.1233 99.1128 -0.5928 264.2506 264.8433 278.2132 99.9348 -0.5947 264.3730 264.9677 278.3147 100.7270 -0.5969 264.4953 265.0922 278.4025 101.5185 -0.5960 264.6092 265.2052 278.4961 102.3708 -0.5989 264.7439 265.3428 278.5946 103.1325 -0.5982 264.8751 265.4734 278.6928 103.9545 -0.6033 265.0072 265.6105 278.7865 104.7468 -0.6060 265.1313 265.7373 278.8849 105.5385 -0.6060 265.2542 265.8603 278.9763 106.3605 -0.6088 265.3878 265.9966 279.0754 107.1525 -0.6121 265.5047 266.1168 279.1650 107.9748 -0.6121 265.6305 266.2426 279.2603 108.7665 -0.6130 265.7629 266.3759 279.3600 109.5585 -0.6093 265.8791 266.4885 279.4541 110.3805 -0.6144 265.9972 266.6116 279.5573 111.1730 -0.6184 266.1377 266.7562 279.6805 111.9965 -0.6151 266.2560 266.8712 279.7799 112.7885 -0.6207 266.3761 266.9969 279.8907 113.5805 -0.6280 266.5105 267.1385 280.0073 114.4025 -0.6267 266.6251 267.2518 280.1243 115.1945 -0.6306 266.7464 267.3770 280.2423 116.0165 -0.6312 266.8823 267.5135 280.3500 116.7925 -0.6322 266.9994 267.6316 280.4481 117.6140 -0.6367 267.1408 267.7775 280.5575 118.4365 -0.6392 267.2611 267.9003 280.6793 119.1990 -0.6428 267.3764 268.0193 280.7821 120.0515 -0.6437 267.5070 268.1507 280.9143 120.8135 -0.6454 267.6199 268.2653 281.0339 121.6365 -0.6448 267.7504 268.3951 281.1434 122.4288 -0.6428 267.8585 268.5013 281.2512 123.2190 -0.6419 267.9942 268.6361 281.3628 124.0675 -0.6498 268.1334 268.7832 281.4898 124.8265 -0.6588 268.2479 268.9068 281.6045 125.6453 -0.6620 268.3830 269.0450 281.7432 126.4338 -0.6600 268.4828 269.1428 281.8388 127.2230 -0.6591 268.6133 269.2725 281.9518 128.0720 -0.6669 268.7480 269.4149 282.0756 128.8333 -0.6699 268.8604 269.5303 282.1823 129.6538 -0.6717 268.9993 269.6709 282.2997 130.4433 -0.6693 269.1118 269.7811 282.4120 131.2323 -0.6716 269.2319 269.9035 282.5289 132.0830 -0.6781 269.3699 270.0480 282.6467 132.8455 -0.6810 269.4850 270.1660 282.7488 133.6680 -0.6761 269.6234 270.2996 282.8539 134.4598 -0.6830 269.7426 270.4256 282.9579 135.2515 -0.6843 269.8583 270.5427 283.0463 136.0753 -0.6889 269.9685 270.6574 283.1520 136.8675 -0.6894 270.0970 270.7864 283.2435 137.6898 -0.6919 270.2222 270.9141 283.3311 138.4818 -0.6955 270.3371 271.0327 283.4290 139.2735 -0.6979 270.4691 271.1670 283.5240 140.0958 -0.7017 270.5794 271.2811 283.6196 140.8875 -0.7037 270.7015 271.4052 283.7015 141.7098 -0.7052 270.8303 271.5355 283.8149 142.5018 -0.7061 270.9626 271.6688 283.8953 143.2935 -0.7092 271.0903 271.7995 283.9669 144.1458 -0.7084 271.2129 271.9213 284.0696 144.9085 -0.7107 271.3350 272.0457 284.1472 145.7315 -0.7131 271.4651 272.1781 284.2530 146.5238 -0.7159 271.5823 272.2982 284.3723 147.3155 -0.7201 271.7055 272.4257 284.4671 148.1683 -0.7246 271.8275 272.5521 284.5706 148.9305 -0.7275 271.9412 272.6687 284.6655 149.7533 -0.7294 272.0752 272.8046 284.7736 150.5455 -0.7324 272.1847 272.9171 284.8981 151.3375 -0.7347 272.3022 273.0369 285.0004 152.1895 -0.7372 272.4312 273.1684 285.1054 152.9515 -0.7396 272.5580 273.2976 285.2180 153.7735 -0.7427 272.6761 273.4188 285.3196 154.5655 -0.7461 272.7932 273.5394 285.4307 155.3580 -0.7476 272.9253 273.6729 285.5407 156.2075 -0.7483 273.0524 273.8007 285.6582 156.9660 -0.7514 273.1583 273.9097 285.7636 157.7845 -0.7533 273.2868 274.0401 285.8617 158.5730 -0.7567 273.4057 274.1624 285.9650 159.3620 -0.7582 273.5168 274.2750 286.0751 160.1808 -0.7604 273.6339 274.3943 286.1910 160.9700 -0.7650 273.7713 274.5363 286.3018 161.7890 -0.7680 273.8950 274.6630 286.4185 162.5793 -0.7706 274.0109 274.7815 286.5033 163.3705 -0.7722 274.1335 274.9057 286.6289 164.1925 -0.7753 274.2468 275.0221 286.7342 164.9545 -0.7766 274.3643 275.1410 286.8361 165.8065 -0.7786 274.4864 275.2650 286.9644 166.5685 -0.7827 274.6063 275.3890 287.0479 167.3905 -0.7841 274.7243 275.5085 287.1518 168.2125 -0.7863 274.8420 275.6283 287.2728 168.9745 -0.7920 274.9596 275.7516 287.3817 169.8273 -0.7958 275.0913 275.8871 287.4969 170.5895 -0.7952 275.2116 276.0068 287.5933 171.4123 -0.7966 275.3513 276.1479 287.7020 172.2045 -0.7978 275.4575 276.2553 287.8194 172.9975 -0.8015 275.5704 276.3718 287.9416 173.8195 -0.8051 275.7029 276.5080 288.0287 174.6115 -0.8063 275.8206 276.6268 288.1371 175.4335 -0.8117 275.9316 276.7432 288.2498 176.2255 -0.8142 276.0632 276.8774 288.3561 177.0168 -0.8145 276.1927 277.0072 288.4741 177.8390 -0.8178 276.3106 277.1284 288.5708 178.6308 -0.8199 276.4262 277.2462 288.6695 179.4528 -0.8265 276.5438 277.3703 288.7819 180.2448 -0.8283 276.6655 277.4938 288.8871 181.0375 -0.8299 276.7770 277.6069 288.9893 181.8598 -0.8330 276.9094 277.7424 289.1007 182.6515 -0.8340 277.0373 277.8713 289.1903 183.4738 -0.8357 277.1449 277.9806 289.2909 184.2658 -0.8389 277.2606 278.0995 289.4114 185.0575 -0.8418 277.3912 278.2330 289.5045 185.8800 -0.8465 277.5224 278.3689 289.6176 186.6725 -0.8482 277.6422 278.4905 289.7194 187.4948 -0.8490 277.7558 278.6048 289.8302 188.2830 -0.8483 277.8778 278.7261 289.9336 189.0720 -0.8502 277.9867 278.8368 290.0399 189.8900 -0.8552 278.1124 278.9676 290.1547 190.6480 -0.8590 278.2341 279.0931 290.2556 191.4960 -0.8576 278.3619 279.2195 290.3741 192.2840 -0.8644 278.4846 279.3490 290.4692 193.0730 -0.8582 278.5889 279.4470 290.5603 193.8910 -0.8599 278.7024 279.5623 290.6669 194.6805 -0.8651 278.8292 279.6943 290.7654 195.4990 -0.8696 278.9404 279.8099 290.8822 196.2898 -0.8761 279.0647 279.9407 290.9880 197.0815 -0.8812 279.1876 280.0688 291.0889 197.9038 -0.8831 279.3059 280.1890 291.1935 198.6955 -0.8866 279.4148 280.3014 291.2894 199.5178 -0.8899 279.5380 280.4278 291.4057 200.3098 -0.8909 279.6566 280.5475 291.5098 201.1015 -0.8952 279.7645 280.6597 291.6083 201.9235 -0.8919 279.8892 280.7810 291.7122 202.7155 -0.8949 280.0366 280.9316 291.8048 203.5375 -0.8998 280.1587 281.0586 291.9212 204.3295 -0.9063 280.2652 281.1715 292.0240 205.1215 -0.9085 280.3885 281.2969 292.1236 205.9440 -0.9062 280.4981 281.4043 292.2217 206.7365 -0.9100 280.6192 281.5292 292.3341 207.5595 -0.9115 280.7501 281.6615 292.4456 208.3525 -0.9145 280.8604 281.7749 292.5439 209.1445 -0.9179 280.9739 281.8918 292.6358 209.9665 -0.9201 281.0979 282.0180 292.7434 210.7585 -0.9229 281.2120 282.1349 292.8457 211.5805 -0.9252 281.3328 282.2579 292.9420 212.3725 -0.9276 281.4616 282.3892 293.0495 213.1645 -0.9304 281.5843 282.5147 293.1530 213.9865 -0.9345 281.7067 282.6412 293.2563 214.7785 -0.9369 281.8224 282.7593 293.3571 215.6000 -0.9399 281.9221 282.8621 293.4637 216.3925 -0.9455 282.0538 282.9994 293.5652 217.1835 -0.9479 282.1607 283.1086 293.6801 218.0358 -0.9486 282.2889 283.2375 293.7886 218.7975 -0.9508 282.4013 283.3521 293.8801 219.6185 -0.9536 282.5267 283.4804 293.9782 220.4363 -0.9557 282.6494 283.6050 294.0848 221.1943 -0.9591 282.7455 283.7046 294.1687 222.0428 -0.9613 282.8760 283.8374 294.2802 222.8003 -0.9627 283.0036 283.9663 294.3690 223.6203 -0.9640 283.1278 284.0918 294.4770 224.4393 -0.9701 283.2477 284.2178 294.5789 225.1998 -0.9747 283.3565 284.3312 294.6522 226.0495 -0.9771 283.4659 284.4430 294.7690 226.8110 -0.9799 283.5964 284.5763 294.8566 227.6323 -0.9790 283.7163 284.6953 294.9781 228.4535 -0.9811 283.8279 284.8090 295.0760 229.2153 -0.9850 283.9344 284.9194 295.1940 230.0680 -0.9882 284.0505 285.0386 295.3099 230.8303 -0.9913 284.1844 285.1758 295.4038 231.6525 -0.9937 284.3056 285.2992 295.5174 232.4443 -0.9963 284.4086 285.4049 295.6373 233.2355 -0.9968 284.5244 285.5212 295.7390 234.0583 -1.0003 284.6615 285.6617 295.8652 234.8498 -1.0031 284.7708 285.7739 295.9826 235.6718 -1.0054 284.8896 285.8950 296.1116 236.4638 -1.0032 285.0045 286.0077 296.2299 237.2555 -1.0107 285.1201 286.1308 296.3277 238.0785 -1.0131 285.2377 286.2508 296.4519 238.8415 -1.0182 285.3574 286.3756 296.5690 239.6938 -1.0222 285.4751 286.4973 296.6989 240.4858 -1.0250 285.6057 286.6306 296.8274 241.2775 -1.0260 285.7262 286.7522 296.9492 242.1000 -1.0323 285.8412 286.8735 297.0817 242.8625 -1.0346 285.9393 286.9739 297.1964 243.7148 -1.0354 286.0561 287.0915 297.3001 244.5068 -1.0353 286.1869 287.2223 297.4157 245.2995 -1.0396 286.2935 287.3332 297.5223 246.1215 -1.0428 286.4044 287.4471 297.6580 246.8835 -1.0392 286.5317 287.5709 297.7385 247.7355 -1.0409 286.6591 287.7000 297.8591 248.5275 -1.0468 286.7759 287.8227 297.9701 249.3245 -1.0547 286.8800 287.9347 298.0753 250.1325 -1.0579 287.0146 288.0725 298.1692 250.9245 -1.0604 287.1277 288.1881 298.2610 251.7450 -1.0596 287.2456 288.3052 298.3665 252.5040 -1.0644 287.3523 288.4167 298.4713 253.3530 -1.0670 287.4877 288.5546 298.5719 254.1410 -1.0706 287.6055 288.6762 298.6513 254.9288 -1.0672 287.7193 288.7865 298.7441 255.7470 -1.0659 287.8332 288.8991 298.8552 256.5050 -1.0759 287.9467 289.0227 298.9619 257.3535 -1.0714 288.0755 289.1469 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