DTA measure 16_meres_updown4 Date: 202449:1152 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.30 s Mass = 1325.900 mg data_number = 1586 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2095 -0.7712 246.3066 247.0778 265.9759 2.0018 -0.7645 246.4610 247.2255 265.9882 2.7945 -0.7584 246.6237 247.3821 266.0130 3.6168 -0.7575 246.7647 247.5221 266.0139 4.3785 -0.7538 246.9098 247.6636 266.0213 5.2308 -0.7480 247.0911 247.8391 266.0386 6.0225 -0.7419 247.2253 247.9672 266.0492 6.8145 -0.7368 247.3781 248.1149 266.0872 7.6368 -0.7312 247.5238 248.2550 266.1210 8.3985 -0.7276 247.6675 248.3951 266.1519 9.2508 -0.7182 247.8295 248.5477 266.1923 10.0425 -0.7150 247.9738 248.6888 266.2305 10.8345 -0.7123 248.1277 248.8400 266.2801 11.6565 -0.7094 248.2855 248.9949 266.3373 12.4485 -0.7053 248.4305 249.1358 266.4034 13.2705 -0.7025 248.5695 249.2720 266.4702 14.0625 -0.7016 248.7182 249.4198 266.5432 14.8555 -0.6956 248.8735 249.5692 266.6208 15.6775 -0.6942 249.0235 249.7176 266.6969 16.4695 -0.6899 249.1659 249.8558 266.7817 17.2915 -0.6826 249.3194 250.0019 266.8729 18.0835 -0.6789 249.4574 250.1362 266.9819 18.8755 -0.6790 249.6040 250.2831 267.0855 19.7275 -0.6757 249.7643 250.4400 267.2027 20.4890 -0.6691 249.8947 250.5638 267.3027 21.3108 -0.6673 250.0340 250.7014 267.4335 22.1033 -0.6678 250.1777 250.8455 267.5564 22.8955 -0.6648 250.3248 250.9896 267.6777 23.7435 -0.6582 250.4877 251.1459 267.8179 24.4990 -0.6639 250.6295 251.2934 267.9358 25.3170 -0.6645 250.7756 251.4401 268.0592 26.1058 -0.6646 250.9035 251.5681 268.1920 26.8965 -0.6584 251.0545 251.7129 268.3244 27.7445 -0.6523 251.1980 251.8503 268.4713 28.5030 -0.6501 251.3282 251.9783 268.6122 29.3218 -0.6461 251.4726 252.1187 268.7456 30.1418 -0.6434 251.6219 252.2653 268.8768 30.9008 -0.6376 251.7657 252.4034 268.9950 31.7510 -0.6358 251.9185 252.5543 269.1381 32.5125 -0.6356 252.0510 252.6866 269.2633 33.3343 -0.6331 252.1924 252.8255 269.3768 34.1565 -0.6316 252.3320 252.9636 269.5135 34.9185 -0.6304 252.4721 253.1025 269.6264 35.7698 -0.6285 252.6174 253.2458 269.7597 36.5320 -0.6288 252.7607 253.3895 269.8613 37.3538 -0.6290 252.9211 253.5501 269.9917 38.1758 -0.6265 253.0591 253.6856 270.1308 38.9378 -0.6273 253.2015 253.8288 270.2425 39.7900 -0.6262 253.3406 253.9667 270.3845 40.5538 -0.6249 253.4686 254.0935 270.4881 41.3768 -0.6239 253.6186 254.2425 270.5778 42.1990 -0.6213 253.7677 254.3890 270.6921 42.9605 -0.6218 253.8887 254.5105 270.7993 43.8128 -0.6214 254.0400 254.6614 270.9053 44.5745 -0.6210 254.1751 254.7961 270.9994 45.3968 -0.6195 254.3155 254.9350 271.0918 46.2190 -0.6204 254.4513 255.0717 271.2056 46.9815 -0.6223 254.5972 255.2196 271.3012 47.8343 -0.6207 254.7431 255.3638 271.3886 48.6268 -0.6188 254.8864 255.5051 271.4825 49.4195 -0.6185 255.0247 255.6432 271.5778 50.2418 -0.6152 255.1398 255.7550 271.6750 51.0035 -0.6139 255.2796 255.8935 271.7553 51.8555 -0.6133 255.4423 256.0556 271.8438 52.6478 -0.6139 255.5868 256.2007 271.9279 53.4405 -0.6144 255.7186 256.3330 272.0277 54.2625 -0.6133 255.8586 256.4719 272.1017 55.0240 -0.6128 255.9986 256.6114 272.2003 55.8728 -0.6095 256.1328 256.7423 272.3037 56.6610 -0.6116 256.2499 256.8615 272.4030 57.4500 -0.6112 256.4009 257.0120 272.5113 58.2683 -0.6120 256.5521 257.1642 272.6162 59.0270 -0.6123 256.6817 257.2939 272.7029 59.8750 -0.6137 256.8099 257.4237 272.8160 60.6630 -0.6151 256.9524 257.5675 272.9274 61.4523 -0.6167 257.1080 257.7247 273.0367 62.2723 -0.6164 257.2204 257.8368 273.1546 63.0325 -0.6165 257.3487 257.9652 273.2517 63.8835 -0.6167 257.4859 258.1027 273.3821 64.6455 -0.6197 257.6142 258.2339 273.4651 65.4675 -0.6209 257.7625 258.3834 273.5813 66.2895 -0.6221 257.9084 258.5306 273.7126 67.0515 -0.6231 258.0459 258.6690 273.8174 67.9035 -0.6206 258.1788 258.7994 273.9301 68.6655 -0.6227 258.3097 258.9324 274.0325 69.4875 -0.6249 258.4515 259.0764 274.1530 70.2795 -0.6287 258.5895 259.2182 274.2668 71.0715 -0.6293 258.7246 259.3539 274.3802 71.9235 -0.6295 258.8748 259.5043 274.5102 72.6855 -0.6307 258.9877 259.6184 274.6087 73.5075 -0.6320 259.1043 259.7363 274.7204 74.2995 -0.6342 259.2487 259.8830 274.8387 75.0915 -0.6362 259.3937 260.0299 274.9682 75.9433 -0.6375 259.5230 260.1605 275.0717 76.7053 -0.6390 259.6633 260.3023 275.1919 77.5275 -0.6421 259.8069 260.4490 275.3043 78.3195 -0.6428 259.9275 260.5703 275.4229 79.1113 -0.6451 260.0709 260.7159 275.5278 79.9330 -0.6456 260.2027 260.8483 275.6517 80.7248 -0.6482 260.3397 260.9878 275.7614 81.5468 -0.6479 260.4657 261.1135 275.8754 82.3388 -0.6512 260.6012 261.2523 275.9950 83.1305 -0.6523 260.7256 261.3779 276.0892 83.9528 -0.6540 260.8518 261.5058 276.1970 84.7445 -0.6550 260.9981 261.6530 276.3095 85.5675 -0.6585 261.1381 261.7966 276.4083 86.3480 -0.6601 261.2708 261.9309 276.5097 87.1708 -0.6614 261.4015 262.0629 276.6068 87.9590 -0.6653 261.5237 262.1890 276.6955 88.7470 -0.6712 261.6550 262.3262 276.7837 89.5650 -0.6708 261.7964 262.4672 276.8806 90.3530 -0.6706 261.9180 262.5886 276.9721 91.1725 -0.6704 262.0541 262.7245 277.0659 91.9613 -0.6725 262.1877 262.8602 277.1659 92.7500 -0.6761 262.3082 262.9842 277.2632 93.5693 -0.6787 262.4539 263.1326 277.3586 94.3593 -0.6783 262.5909 263.2691 277.4409 95.1795 -0.6841 262.7156 263.3997 277.5514 95.9698 -0.6860 262.8401 263.5261 277.6467 96.7615 -0.6873 262.9662 263.6535 277.7360 97.5838 -0.6919 263.0900 263.7820 277.8542 98.3755 -0.6937 263.2298 263.9235 277.9529 99.1978 -0.7005 263.3695 264.0699 278.0547 99.9898 -0.7065 263.4810 264.1875 278.1602 100.7815 -0.7092 263.6155 264.3247 278.2594 101.6043 -0.7103 263.7495 264.4597 278.3714 102.3665 -0.7099 263.8722 264.5821 278.4947 103.2188 -0.7081 264.0188 264.7268 278.5995 104.0108 -0.7066 264.1632 264.8698 278.6998 104.8025 -0.7079 264.2784 264.9863 278.8288 105.6248 -0.7093 264.4036 265.1129 278.9321 106.3865 -0.7109 264.5198 265.2308 279.0292 107.2388 -0.7138 264.6722 265.3860 279.1416 108.0005 -0.7171 264.7956 265.5127 279.2464 108.8228 -0.7190 264.9243 265.6433 279.3746 109.6445 -0.7227 265.0628 265.7855 279.4837 110.4065 -0.7266 265.1813 265.9080 279.5884 111.2585 -0.7282 265.3223 266.0505 279.6855 112.0505 -0.7277 265.4519 266.1796 279.7901 112.8425 -0.7276 265.5764 266.3041 279.8984 113.6645 -0.7300 265.6977 266.4277 280.0139 114.4265 -0.7327 265.8254 266.5581 280.1230 115.2790 -0.7352 265.9802 266.7154 280.2287 116.0715 -0.7364 266.1041 266.8405 280.3428 116.8633 -0.7400 266.2220 266.9620 280.4610 117.6853 -0.7445 266.3568 267.1013 280.5778 118.4465 -0.7451 266.4768 267.2220 280.6751 119.2980 -0.7474 266.6117 267.3590 280.7774 120.0863 -0.7517 266.7322 267.4840 280.8883 120.8745 -0.7520 266.8602 267.6122 280.9919 121.6925 -0.7515 266.9912 267.7427 281.1085 122.4508 -0.7517 267.1045 267.8562 281.2170 123.2990 -0.7546 267.2584 268.0130 281.3226 124.0868 -0.7546 267.3716 268.1262 281.4332 124.8755 -0.7598 267.4912 268.2510 281.5359 125.6950 -0.7649 267.6352 268.4000 281.6397 126.4860 -0.7687 267.7581 268.5267 281.7501 127.3063 -0.7690 267.8899 268.6589 281.8706 128.0965 -0.7707 268.0234 268.7941 281.9779 128.8875 -0.7737 268.1484 268.9222 282.0742 129.7095 -0.7758 268.2786 269.0544 282.1794 130.4715 -0.7790 268.3922 269.1712 282.2837 131.3240 -0.7802 268.5298 269.3099 282.4013 132.1165 -0.7816 268.6610 269.4426 282.5175 132.9085 -0.7828 268.7816 269.5644 282.6207 133.7305 -0.7868 268.8972 269.6840 282.7132 134.4925 -0.7895 269.0171 269.8066 282.8141 135.3440 -0.7916 269.1622 269.9538 282.9305 136.1360 -0.7938 269.2774 270.0712 283.0515 136.9343 -0.7962 269.4057 270.2020 283.1537 137.7448 -0.7983 269.5270 270.3254 283.2619 138.5365 -0.7979 269.6657 270.4635 283.3662 139.3590 -0.8027 269.7977 270.6004 283.4850 140.1205 -0.7997 269.9216 270.7213 283.5784 140.9728 -0.8012 270.0457 270.8470 283.6806 141.7648 -0.8040 270.1703 270.9742 283.7903 142.5565 -0.8107 270.2992 271.1099 283.8926 143.3788 -0.8145 270.4285 271.2430 283.9912 144.1705 -0.8194 270.5402 271.3596 284.0969 144.9935 -0.8223 270.6786 271.5009 284.2120 145.7858 -0.8231 270.7970 271.6201 284.3197 146.5785 -0.8303 270.9198 271.7501 284.4155 147.4008 -0.8293 271.0535 271.8828 284.5283 148.1925 -0.8297 271.1736 272.0033 284.6400 149.0148 -0.8281 271.2851 272.1132 284.7343 149.8065 -0.8343 271.4181 272.2525 284.8407 150.5985 -0.8395 271.5429 272.3824 284.9371 151.4205 -0.8426 271.6633 272.5059 285.0489 152.2118 -0.8458 271.7983 272.6441 285.1529 153.0300 -0.8493 271.9242 272.7735 285.2652 153.8180 -0.8510 272.0455 272.8965 285.3714 154.6060 -0.8529 272.1823 273.0352 285.4726 155.4548 -0.8561 272.3158 273.1719 285.5695 156.2130 -0.8580 272.4272 273.2853 285.6765 157.0328 -0.8607 272.5466 273.4073 285.7863 157.8210 -0.8646 272.6731 273.5377 285.8962 158.6100 -0.8684 272.7960 273.6644 285.9954 159.4595 -0.8685 272.9216 273.7901 286.1035 160.2188 -0.8735 273.0454 273.9189 286.1999 161.0405 -0.8729 273.1680 274.0409 286.3088 161.8325 -0.8761 273.2894 274.1655 286.4109 162.6245 -0.8800 273.4011 274.2811 286.5133 163.4765 -0.8826 273.5439 274.4265 286.6271 164.2385 -0.8838 273.6696 274.5534 286.7188 165.0605 -0.8868 273.8011 274.6879 286.8230 165.8525 -0.8910 273.9175 274.8085 286.9162 166.6445 -0.8917 274.0402 274.9319 287.0227 167.4965 -0.8946 274.1791 275.0737 287.1246 168.2658 -0.8948 274.2944 275.1892 287.2166 169.0885 -0.8962 274.4157 275.3119 287.3353 169.8805 -0.8985 274.5327 275.4312 287.4346 170.6725 -0.9000 274.6487 275.5487 287.5277 171.5245 -0.9028 274.8080 275.7108 287.6281 172.2865 -0.9094 274.9160 275.8254 287.7395 173.1085 -0.9143 275.0356 275.9499 287.8353 173.9005 -0.9170 275.1498 276.0668 287.9201 174.6923 -0.9223 275.2623 276.1846 288.0137 175.5445 -0.9233 275.4004 276.3237 288.1249 176.3063 -0.9237 275.5158 276.4394 288.2141 177.1278 -0.9263 275.6372 276.5636 288.3124 177.9500 -0.9284 275.7755 276.7039 288.4119 178.7115 -0.9283 275.8884 276.8167 288.5197 179.5643 -0.9329 276.0126 276.9456 288.6200 180.3265 -0.9368 276.1334 277.0702 288.7008 181.1488 -0.9406 276.2599 277.2005 288.7972 181.9708 -0.9419 276.3874 277.3292 288.9011 182.7325 -0.9453 276.4947 277.4399 288.9883 183.5848 -0.9498 276.6356 277.5854 289.1080 184.3450 -0.9527 276.7460 277.6987 289.2010 185.1623 -0.9519 276.8761 277.8280 289.2946 185.9800 -0.9546 277.0021 277.9568 289.3992 186.7380 -0.9577 277.1011 278.0588 289.4970 187.5863 -0.9609 277.2234 278.1843 289.6153 188.3465 -0.9631 277.3485 278.3116 289.7357 189.1680 -0.9700 277.4837 278.4537 289.8508 189.9863 -0.9768 277.5932 278.5700 289.9617 190.7450 -0.9783 277.7169 278.6952 290.0632 191.5943 -0.9810 277.8431 278.8241 290.1915 192.3540 -0.9846 277.9681 278.9527 290.3113 193.1758 -0.9891 278.0686 279.0577 290.4218 193.9978 -0.9897 278.2066 279.1963 290.5403 194.7595 -0.9894 278.3310 279.3205 290.6578 195.6118 -0.9923 278.4539 279.4462 290.7828 196.3735 -0.9976 278.5665 279.5641 290.8903 197.1955 -1.0030 278.6892 279.6922 291.0261 197.9878 -1.0080 278.7989 279.8069 291.1338 198.7798 -1.0093 278.9174 279.9267 291.2563 199.6318 -1.0114 279.0594 280.0708 291.3759 200.3935 -1.0134 279.1687 280.1821 291.4828 201.2158 -1.0168 279.2945 280.3113 291.6023 202.0078 -1.0184 279.4045 280.4229 291.7140 202.7995 -1.0232 279.5281 280.5512 291.8105 203.6515 -1.0215 279.6674 280.6889 291.9272 204.4135 -1.0275 279.7874 280.8149 292.0165 205.2355 -1.0304 279.8932 280.9237 292.1247 206.0298 -1.0360 280.0136 281.0496 292.2212 206.8235 -1.0327 280.1325 281.1652 292.3311 207.6470 -1.0334 280.2561 281.2896 292.4325 208.4405 -1.0339 280.3830 281.4168 292.5106 209.2628 -1.0363 280.4917 281.5280 292.6298 210.0545 -1.0409 280.6353 281.6762 292.7271 210.8465 -1.0385 280.7477 281.7862 292.8286 211.6685 -1.0472 280.8697 281.9169 292.9232 212.4605 -1.0489 280.9905 282.0394 293.0200 213.2825 -1.0557 281.0994 282.1551 293.1131 214.0745 -1.0595 281.2193 282.2788 293.1958 214.8665 -1.0547 281.3379 282.3925 293.2818 215.7180 -1.0564 281.4779 282.5343 293.3895 216.4773 -1.0655 281.5853 282.6508 293.4683 217.2948 -1.0665 281.7136 282.7802 293.5674 218.0828 -1.0704 281.8301 282.9005 293.6610 218.8705 -1.0723 281.9432 283.0156 293.7523 219.7190 -1.0737 282.0811 283.1549 293.8682 220.5070 -1.0776 282.1746 283.2522 293.9815 221.2958 -1.0783 282.2927 283.3710 294.0776 222.1143 -1.0842 282.4217 283.5059 294.1926 222.9040 -1.0854 282.5383 283.6237 294.2966 223.7235 -1.0869 282.6681 283.7550 294.4146 224.5138 -1.0892 282.7915 283.8807 294.5296 225.3048 -1.0945 282.8973 283.9919 294.6266 226.1265 -1.0963 283.0152 284.1115 294.7367 226.8885 -1.0980 283.1326 284.2306 294.8334 227.7405 -1.1022 283.2571 284.3593 294.9551 228.5025 -1.1067 283.3874 284.4941 295.0753 229.3245 -1.1075 283.5172 284.6246 295.1847 230.1465 -1.1102 283.6276 284.7378 295.3155 230.9083 -1.1134 283.7486 284.8620 295.4349 231.7605 -1.1162 283.8622 284.9784 295.5319 232.5220 -1.1160 283.9643 285.0804 295.6407 233.3438 -1.1203 284.0947 285.2150 295.7560 234.1658 -1.1210 284.2350 285.3560 295.8654 234.9275 -1.1220 284.3474 285.4695 295.9729 235.7798 -1.1248 284.4539 285.5787 296.1008 236.5415 -1.1294 284.5710 285.7004 296.2002 237.3638 -1.1365 284.6974 285.8339 296.3099 238.1858 -1.1394 284.8135 285.9529 296.4570 238.9475 -1.1444 284.9198 286.0641 296.5639 239.7998 -1.1490 285.0483 286.1973 296.6799 240.5615 -1.1520 285.1621 286.3141 296.7806 241.3845 -1.1528 285.2752 286.4280 296.8958 242.1790 -1.1550 285.3914 286.5464 297.0093 242.9735 -1.1558 285.5161 286.6719 297.1186 243.8258 -1.1595 285.6320 286.7915 297.2528 244.5875 -1.1656 285.7433 286.9090 297.3670 245.4095 -1.1669 285.8821 287.0490 297.4814 246.2015 -1.1683 285.9957 287.1640 297.5941 246.9935 -1.1718 286.1282 287.3000 297.6828 247.8453 -1.1757 286.2512 287.4269 297.7841 248.6050 -1.1793 286.3570 287.5363 297.8831 249.4228 -1.1833 286.4683 287.6516 297.9933 250.2028 -1.1835 286.5885 287.7720 298.0900 251.0220 -1.1869 286.7115 287.8984 298.1884 251.8103 -1.1888 286.8262 288.0150 298.2789 252.6000 -1.1905 286.9417 288.1322 298.3644 253.4485 -1.1941 287.0766 288.2707 298.4693 254.2070 -1.1962 287.1735 288.3697 298.5483 255.0258 -1.1987 287.2939 288.4926 298.6341 255.8443 -1.2017 287.4129 288.6146 298.7218 256.6048 -1.2053 287.5219 288.7272 298.8084 257.4568 -1.2104 287.6506 288.8610 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