DTA measure 2Pb_4 Date: 2024416:1154 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 970.97 s Mass = 953.400 mg data_number = 1209 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1018 -1.9529 229.3902 231.3431 261.5493 1.9228 -1.9518 229.5126 231.4644 261.5165 2.7430 -1.9478 229.6407 231.5884 261.5073 3.5043 -1.9476 229.7600 231.7076 261.5010 4.3560 -1.9437 229.8889 231.8327 261.5131 5.1175 -1.9452 229.9944 231.9396 261.5045 5.9398 -1.9442 230.1189 232.0630 261.5111 6.7595 -1.9397 230.2397 232.1794 261.5162 7.5215 -1.9386 230.3582 232.2968 261.5226 8.3735 -1.9340 230.4859 232.4198 261.5538 9.1348 -1.9290 230.6113 232.5403 261.5702 9.9565 -1.9120 230.7312 232.6432 261.5855 10.7780 -1.9023 230.8396 232.7418 261.6414 11.5390 -1.9046 230.9517 232.8563 261.6845 12.3905 -1.9008 231.0628 232.9636 261.7293 13.1518 -1.8973 231.1832 233.0804 261.7720 13.9735 -1.8709 231.3195 233.1904 261.8253 14.7955 -1.8541 231.4531 233.3072 261.8986 15.5558 -1.8742 231.5594 233.4336 261.9692 16.4065 -1.8722 231.6661 233.5383 262.0575 17.1665 -1.8733 231.7722 233.6455 262.1480 17.9890 -1.8753 231.9044 233.7798 262.2475 18.8095 -1.8797 232.0145 233.8942 262.3382 19.5695 -1.8772 232.1370 234.0143 262.4434 20.4208 -1.8735 232.2514 234.1249 262.5589 21.1818 -1.8753 232.3674 234.2426 262.6488 22.0023 -1.8780 232.4910 234.3690 262.7548 22.8228 -1.8686 232.6084 234.4770 262.8860 23.5818 -1.8708 232.7217 234.5925 263.0124 24.4340 -1.8702 232.8382 234.7084 263.1370 25.1973 -1.8730 232.9620 234.8350 263.2746 26.0205 -1.8718 233.0767 234.9485 263.3881 26.8408 -1.8709 233.2095 235.0804 263.5389 27.6008 -1.8409 233.3121 235.1531 263.6763 28.4573 -1.8400 233.4193 235.2593 263.8317 29.2050 -1.8202 233.5289 235.3491 263.9616 30.0628 -1.8478 233.6753 235.5231 264.1183 30.8215 -1.8378 233.7682 235.6060 264.2642 31.6418 -1.8099 233.8909 235.7008 264.4089 32.4615 -1.8367 234.0075 235.8442 264.5543 33.2213 -1.8381 234.1238 235.9619 264.7121 34.0725 -1.8548 234.2408 236.0956 264.8997 34.8335 -1.8710 234.3510 236.2220 265.0263 35.6553 -1.8735 234.4735 236.3470 265.1808 36.4765 -1.8738 234.5777 236.4516 265.3301 37.2373 -1.8766 234.6782 236.5548 265.4793 38.0875 -1.8797 234.8251 236.7048 265.6371 38.8778 -1.8748 234.9111 236.7859 265.7986 39.6680 -1.8819 235.0413 236.9232 265.9507 40.4875 -1.8848 235.1714 237.0562 266.1064 41.2488 -1.8871 235.2881 237.1752 266.2587 42.1003 -1.8883 235.4149 237.3032 266.4022 42.8905 -1.8873 235.5158 237.4031 266.5387 43.6813 -1.8876 235.6388 237.5265 266.6944 44.5025 -1.8907 235.7594 237.6501 266.8372 45.2620 -1.8926 235.8557 237.7483 266.9792 46.1130 -1.8935 236.0014 237.8949 267.1193 46.9053 -1.8926 236.1140 238.0066 267.2474 47.6950 -1.8906 236.2233 238.1139 267.3878 48.5163 -1.8909 236.3481 238.2390 267.5146 49.2768 -1.8907 236.4503 238.3410 267.6365 50.1288 -1.8884 236.5720 238.4604 267.7790 50.9190 -1.8897 236.6942 238.5839 267.8859 51.7103 -1.8931 236.8090 238.7021 268.0163 52.5320 -1.8944 236.9212 238.8156 268.1278 53.2910 -1.8978 237.0411 238.9388 268.2530 54.1415 -1.8963 237.1725 239.0688 268.3792 54.9310 -1.8980 237.2819 239.1799 268.4980 55.7218 -1.8985 237.3897 239.2882 268.5934 56.5435 -1.9009 237.5092 239.4101 268.7094 57.3038 -1.9021 237.6358 239.5379 268.8011 58.1570 -1.9038 237.7695 239.6733 268.9087 58.9468 -1.9046 237.8595 239.7641 269.0154 59.7395 -1.9068 237.9798 239.8866 269.1159 60.5615 -1.9074 238.1016 240.0090 269.2300 61.3230 -1.9086 238.2129 240.1215 269.3270 62.1743 -1.9074 238.3367 240.2441 269.4271 62.9338 -1.9069 238.4348 240.3418 269.5209 63.7570 -1.9077 238.5601 240.4678 269.6338 64.5785 -1.9088 238.6859 240.5948 269.7256 65.3385 -1.9123 238.8046 240.7169 269.8022 66.1893 -1.9136 238.9240 240.8376 269.8969 66.9505 -1.9168 239.0355 240.9523 269.9850 67.7715 -1.9152 239.1507 241.0659 270.0986 68.5635 -1.9178 239.2709 241.1888 270.1749 69.3553 -1.9182 239.3726 241.2908 270.2698 70.1763 -1.9175 239.5073 241.4248 270.3750 70.9660 -1.9176 239.6262 241.5439 270.4708 71.7860 -1.9169 239.7416 241.6585 270.5605 72.5763 -1.9163 239.8732 241.7894 270.6452 73.3663 -1.9152 239.9983 241.9135 270.7258 74.1880 -1.9204 240.1144 242.0349 270.8395 74.9775 -1.9231 240.2255 242.1486 270.9091 75.7980 -1.9221 240.3369 242.2590 271.0044 76.5890 -1.9246 240.4479 242.3725 271.0858 77.3793 -1.9263 240.5597 242.4860 271.1790 78.2010 -1.9254 240.6826 242.6080 271.2649 78.9928 -1.9298 240.8070 242.7368 271.3423 79.8138 -1.9325 240.9316 242.8641 271.4296 80.6048 -1.9299 241.0284 242.9583 271.5274 81.3965 -1.9307 241.1279 243.0586 271.6155 82.2188 -1.9314 241.2550 243.1864 271.7071 82.9793 -1.9330 241.3813 243.3143 271.7941 83.8305 -1.9341 241.5088 243.4428 271.8857 84.6215 -1.9345 241.6264 243.5609 271.9600 85.4128 -1.9370 241.7307 243.6677 272.0477 86.2320 -1.9370 241.8426 243.7796 272.1445 86.9920 -1.9358 241.9731 243.9088 272.2306 87.8433 -1.9384 242.0767 244.0150 272.3141 88.6328 -1.9401 242.2164 244.1565 272.3974 89.4230 -1.9419 242.3156 244.2575 272.5010 90.2430 -1.9444 242.4335 244.3778 272.5963 91.0323 -1.9436 242.5524 244.4960 272.6975 91.8533 -1.9437 242.6741 244.6178 272.7884 92.6428 -1.9439 242.7811 244.7249 272.8628 93.4345 -1.9435 242.9062 244.8497 272.9725 94.2565 -1.9448 243.0250 244.9698 273.0836 95.0175 -1.9467 243.0971 245.0438 273.1610 95.8695 -1.9483 243.2221 245.1704 273.2933 96.6613 -1.9503 243.3377 245.2880 273.3787 97.4513 -1.9483 243.4598 245.4081 273.4780 98.2718 -1.9484 243.5727 245.5211 273.5757 99.0305 -1.9490 243.6924 245.6414 273.6620 99.8818 -1.9523 243.8025 245.7548 273.7753 100.6713 -1.9509 243.9258 245.8767 273.8694 101.4610 -1.9527 244.0426 245.9953 273.9821 102.2820 -1.9552 244.1472 246.1025 274.0918 103.0418 -1.9526 244.2530 246.2056 274.1801 103.8930 -1.9506 244.3887 246.3394 274.2965 104.6838 -1.9561 244.5049 246.4610 274.3949 105.4750 -1.9572 244.6249 246.5822 274.5069 106.2968 -1.9594 244.7398 246.6992 274.6025 107.0578 -1.9629 244.8440 246.8069 274.7046 107.9093 -1.9630 244.9651 246.9280 274.8195 108.6988 -1.9655 245.0835 247.0490 274.9138 109.4903 -1.9645 245.2056 247.1701 275.0144 110.3115 -1.9708 245.3076 247.2784 275.1091 111.0720 -1.9699 245.4225 247.3923 275.2132 111.9235 -1.9688 245.5367 247.5055 275.3230 112.6855 -1.9691 245.6441 247.6132 275.4217 113.5068 -1.9712 245.7668 247.7380 275.5341 114.3275 -1.9720 245.8938 247.8658 275.6433 115.0888 -1.9744 246.0121 247.9865 275.7442 115.9405 -1.9757 246.1251 248.1008 275.8640 116.7030 -1.9793 246.2335 248.2128 275.9704 117.5250 -1.9801 246.3383 248.3183 276.0762 118.3450 -1.9802 246.4720 248.4522 276.1898 119.1053 -1.9791 246.5796 248.5587 276.2904 119.9563 -1.9810 246.7066 248.6876 276.3915 120.7458 -1.9817 246.7976 248.7793 276.4860 121.5363 -1.9840 246.9260 248.9100 276.6003 122.3573 -1.9848 247.0500 249.0349 276.7088 123.1183 -1.9860 247.1531 249.1391 276.8118 123.9698 -1.9880 247.2684 249.2564 276.9276 124.7593 -1.9887 247.3817 249.3705 277.0318 125.5490 -1.9924 247.4879 249.4803 277.1410 126.3700 -1.9938 247.6054 249.5992 277.2491 127.1595 -1.9937 247.7175 249.7112 277.3578 127.9800 -1.9930 247.8455 249.8385 277.4603 128.7693 -1.9947 247.9765 249.9712 277.5553 129.5590 -1.9974 248.0866 250.0840 277.6546 130.4098 -2.0011 248.1936 250.1947 277.7708 131.1700 -2.0017 248.2922 250.2939 277.8731 131.9938 -1.9992 248.4102 250.4094 277.9780 132.7840 -2.0028 248.5369 250.5397 278.0810 133.5740 -2.0034 248.6540 250.6574 278.1678 134.4243 -1.9980 248.7613 250.7594 278.2871 135.1835 -1.9963 248.8840 250.8803 278.4057 136.0030 -2.0045 248.9852 250.9898 278.5111 136.8225 -2.0058 249.1086 251.1144 278.6059 137.5828 -2.0086 249.2229 251.2315 278.6981 138.4335 -2.0052 249.3396 251.3448 278.8234 139.1950 -2.0099 249.4421 251.4520 278.9242 140.0163 -2.0126 249.5588 251.5714 279.0364 140.8375 -2.0172 249.6806 251.6977 279.1423 141.6073 -2.0165 249.7919 251.8083 279.2498 142.4370 -2.0198 249.9090 251.9288 279.3984 143.1963 -2.0169 250.0076 252.0245 279.5052 144.0473 -2.0187 250.1354 252.1542 279.6128 144.8365 -2.0234 250.2394 252.2628 279.7186 145.6270 -2.0293 250.3472 252.3765 279.8479 146.4485 -2.0321 250.4776 252.5096 279.9776 147.2380 -2.0358 250.5785 252.6144 280.1136 148.0580 -2.0352 250.6927 252.7278 280.2298 148.8483 -2.0352 250.8090 252.8442 280.3485 149.6383 -2.0384 250.9217 252.9601 280.4564 150.4890 -2.0435 251.0457 253.0892 280.5785 151.2490 -2.0385 251.1482 253.1867 280.6924 152.0705 -2.0433 251.2656 253.3088 280.8292 152.8610 -2.0430 251.3708 253.4138 280.9433 153.6513 -2.0471 251.4819 253.5290 281.0484 154.5028 -2.0479 251.6303 253.6782 281.1916 155.2630 -2.0487 251.7227 253.7714 281.3022 156.0845 -2.0513 251.8405 253.8918 281.4074 156.9058 -2.0521 251.9605 254.0125 281.5308 157.6653 -2.0539 252.0616 254.1155 281.6221 158.5168 -2.0563 252.1922 254.2484 281.7425 159.3068 -2.0594 252.3091 254.3684 281.8457 160.0970 -2.0585 252.4214 254.4799 281.9500 160.9175 -2.0554 252.5304 254.5858 282.0621 161.7088 -2.0582 252.6512 254.7095 282.1519 162.5298 -2.0613 252.7732 254.8346 282.2652 163.3195 -2.0626 252.8933 254.9559 282.3609 164.1110 -2.0589 252.9836 255.0425 282.4861 164.9325 -2.0631 253.1124 255.1755 282.5878 165.7228 -2.0635 253.2020 255.2655 282.6995 166.5438 -2.0668 253.3126 255.3794 282.8077 167.3335 -2.0664 253.4366 255.5031 282.8900 168.1240 -2.0699 253.5571 255.6270 282.9855 168.9745 -2.0633 253.6895 255.7528 283.1019 169.7358 -2.0704 253.7955 255.8659 283.1868 170.5568 -2.0772 253.8981 255.9753 283.2936 171.3475 -2.0687 254.0297 256.0984 283.3948 172.1380 -2.0721 254.1301 256.2022 283.4915 172.9880 -2.0777 254.2554 256.3331 283.6126 173.7495 -2.0809 254.3557 256.4366 283.6760 174.5703 -2.0861 254.4833 256.5694 283.7819 175.3610 -2.0865 254.5962 256.6827 283.8953 176.1513 -2.0885 254.7102 256.7987 283.9859 177.0020 -2.0914 254.8149 256.9063 284.0851 177.7630 -2.0927 254.9304 257.0230 284.1919 178.5840 -2.0948 255.0410 257.1358 284.2797 179.3740 -2.0961 255.1593 257.2554 284.3776 180.1655 -2.0956 255.2670 257.3626 284.4904 181.0170 -2.0930 255.3935 257.4865 284.5866 181.7780 -2.0960 255.4926 257.5886 284.6613 182.5995 -2.0975 255.6028 257.7003 284.7460 183.3895 -2.0996 255.7172 257.8168 284.8416 184.1815 -2.1014 255.8140 257.9155 284.9185 185.0058 -2.1022 255.9467 258.0489 285.0134 185.7965 -2.1065 256.0638 258.1703 285.1306 186.6180 -2.1061 256.1646 258.2707 285.2328 187.4095 -2.1020 256.2770 258.3790 285.3131 188.2000 -2.0980 256.3938 258.4918 285.4211 189.0193 -2.0948 256.5049 258.5998 285.5017 189.8105 -2.0993 256.6295 258.7287 285.6074 190.6320 -2.0974 256.7288 258.8262 285.7250 191.4235 -2.1069 256.8360 258.9429 285.8220 192.2155 -2.1172 256.9574 259.0746 285.9277 193.0368 -2.1177 257.0925 259.2101 286.0190 193.7965 -2.1176 257.1852 259.3028 286.1305 194.6473 -2.1194 257.3130 259.4324 286.2425 195.4375 -2.1232 257.4271 259.5503 286.3582 196.2283 -2.1250 257.5298 259.6548 286.4603 197.0495 -2.1295 257.6436 259.7731 286.5807 197.8093 -2.1301 257.7479 259.8780 286.6882 198.6585 -2.1295 257.8765 260.0060 286.8134 199.4485 -2.1327 257.9861 260.1188 286.9023 200.2385 -2.1345 258.1115 260.2460 287.0108 201.0588 -2.1360 258.2117 260.3478 287.1309 201.8480 -2.1341 258.3302 260.4643 287.2280 202.6693 -2.1390 258.4579 260.5969 287.3577 203.4485 -2.1418 258.5606 260.7024 287.4666 204.2698 -2.1412 258.6705 260.8118 287.5779 205.0620 -2.1439 258.7790 260.9229 287.6898 205.8535 -2.1461 258.8878 261.0338 287.7916 206.6760 -2.1477 258.9996 261.1473 287.9187 207.4368 -2.1499 259.1078 261.2577 288.0331 208.2890 -2.1515 259.2551 261.4066 288.1376 209.0795 -2.1549 259.3506 261.5055 288.2672 209.8705 -2.1557 259.4501 261.6058 288.3888 210.6915 -2.1575 259.5523 261.7097 288.5012 211.4530 -2.1587 259.6694 261.8281 288.6111 212.3043 -2.1589 259.8140 261.9729 288.7375 213.0638 -2.1600 259.9269 262.0870 288.8553 213.8848 -2.1598 260.0240 262.1838 288.9674 214.7045 -2.1628 260.1410 262.3038 289.0880 215.4655 -2.1658 260.2595 262.4253 289.1946 216.3175 -2.1684 260.3632 262.5316 289.3294 217.0778 -2.1704 260.4923 262.6627 289.4327 217.8988 -2.1702 260.5927 262.7630 289.5674 218.7185 -2.1767 260.7006 262.8773 289.6684 219.4788 -2.1805 260.8165 262.9970 289.7719 220.3293 -2.1819 260.9387 263.1206 289.8871 221.0890 -2.1786 261.0451 263.2238 289.9998 221.9098 -2.1837 261.1525 263.3362 290.1085 222.7300 -2.1859 261.2656 263.4515 290.2180 223.4908 -2.1905 261.3862 263.5767 290.3218 224.3410 -2.1919 261.5130 263.7048 290.4387 225.1020 -2.1956 261.6105 263.8061 290.5252 225.9230 -2.1971 261.7135 263.9106 290.6244 226.7440 -2.1986 261.8549 264.0535 290.7337 227.5035 -2.1980 261.9402 264.1382 290.8456 228.3548 -2.2005 262.0695 264.2700 290.9413 229.1140 -2.2033 262.1738 264.3771 291.0123 229.9350 -2.2056 262.2820 264.4877 291.1054 230.7560 -2.2060 262.4183 264.6243 291.2059 231.5150 -2.2083 262.5303 264.7386 291.3052 232.3655 -2.2098 262.6413 264.8511 291.4042 233.1250 -2.2113 262.7564 264.9677 291.4866 233.9460 -2.2149 262.8741 265.0890 291.5898 234.7658 -2.2137 262.9689 265.1826 291.6880 235.5253 -2.2174 263.0794 265.2968 291.7793 236.3763 -2.2193 263.1987 265.4180 291.8715 237.1358 -2.2218 263.2964 265.5182 291.9543 237.9563 -2.2124 263.4292 265.6416 292.0475 238.7765 -2.2015 263.5380 265.7395 292.1392 239.5363 -2.2003 263.6336 265.8340 292.2322 240.3873 -2.2005 263.7773 265.9778 292.3229 241.1768 -2.2049 263.8693 266.0741 292.4123 241.9670 -2.2093 263.9876 266.1969 292.5120 242.7875 -2.2096 264.0815 266.2911 292.6204 243.5473 -2.2115 264.2148 266.4264 292.7148 244.3983 -2.2102 264.3338 266.5440 292.8278 245.1878 -2.2114 264.4298 266.6412 292.9237 245.9788 -2.2128 264.5516 266.7643 293.0286 246.7995 -2.2142 264.6635 266.8777 293.1175 247.5898 -2.2148 264.7880 267.0028 293.2244 248.4100 -2.2189 264.9153 267.1342 293.3207 249.2015 -2.2230 265.0135 267.2365 293.4312 249.9925 -2.2228 265.1215 267.3442 293.5242 250.8143 -2.2249 265.2338 267.4587 293.6246 251.6043 -2.2262 265.3325 267.5587 293.7222 252.4250 -2.2335 265.4543 267.6878 293.8224 253.2143 -2.2353 265.5664 267.8017 293.9385 254.0030 -2.2394 265.6673 267.9067 294.0443 254.8538 -2.2382 265.7940 268.0323 294.1545 255.6140 -2.2414 265.9222 268.1637 294.2422 256.4350 -2.2441 266.0433 268.2875 294.3517 257.2265 -2.2483 266.1480 268.3963 294.4690 258.0173 -2.2485 266.2572 268.5057 294.5904 258.8678 -2.2505 266.3568 268.6073 294.6992 259.6263 -2.2533 266.4597 268.7130 294.7776 260.4463 -2.2543 266.5739 268.8281 294.8939 261.2675 -2.2539 266.6968 268.9507 295.0038 262.0290 -2.2532 266.8212 269.0744 295.1194 262.8803 -2.2546 266.9291 269.1837 295.2432 263.6398 -2.2552 267.0131 269.2683 295.3294 264.4615 -2.2602 267.1484 269.4086 295.4398 265.2825 -2.2619 267.2510 269.5129 295.5409 266.0428 -2.2635 267.3730 269.6365 295.6700 266.8935 -2.2638 267.5084 269.7722 295.7819 267.6548 -2.2668 267.5936 269.8604 295.8727 268.4758 -2.2673 267.6945 269.9618 295.9732 269.2955 -2.2703 267.8094 270.0797 296.0936 270.0553 -2.2744 267.9299 270.2043 296.1969 270.9063 -2.2764 268.0612 270.3376 296.3241 271.6968 -2.2755 268.1806 270.4561 296.4253 272.4870 -2.2753 268.2625 270.5378 296.5231 273.3075 -2.2767 268.3749 270.6516 296.6317 274.0980 -2.2803 268.5057 270.7860 296.7396 274.9188 -2.2810 268.6185 270.8994 296.8473 275.7095 -2.2828 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