DTA measure 3Pb_4 Date: 2024416:1219 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1476.82 s Mass = 953.400 mg data_number = 1839 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2225 -4.1782 373.2197 377.3979 390.1432 2.0445 -4.1731 373.3197 377.4928 390.1288 2.8065 -4.1728 373.4095 377.5823 390.1365 3.6580 -4.1699 373.5139 377.6838 390.1299 4.4505 -4.1706 373.6077 377.7783 390.1240 5.2425 -4.1682 373.6960 377.8642 390.1234 6.0643 -4.1609 373.7947 377.9556 390.1359 6.8238 -4.1547 373.8700 378.0247 390.1294 7.6763 -4.1611 373.9751 378.1362 390.1464 8.4373 -4.1625 374.0609 378.2234 390.1238 9.2588 -4.1618 374.1547 378.3165 390.1215 10.0800 -4.1613 374.2437 378.4050 390.1441 10.8413 -4.1612 374.3296 378.4908 390.1247 11.6928 -4.1589 374.4119 378.5707 390.1304 12.4528 -4.1588 374.5103 378.6692 390.1102 13.2748 -4.1568 374.5849 378.7416 390.0987 14.0970 -4.1575 374.6849 378.8423 390.0939 14.8580 -4.1585 374.7727 378.9312 390.0653 15.7100 -4.1512 374.8665 379.0177 390.0416 16.5013 -4.1465 374.9612 379.1077 390.0313 17.2925 -4.1446 375.0375 379.1821 390.0112 18.1148 -4.1470 375.1341 379.2811 389.9868 18.8748 -4.1472 375.2072 379.3544 389.9653 19.7265 -4.1442 375.3011 379.4454 389.9510 20.4885 -4.1400 375.3678 379.5078 389.9119 21.3098 -4.1378 375.4623 379.6002 389.8751 22.1295 -4.1376 375.5529 379.6906 389.8372 22.8905 -4.1354 375.6212 379.7566 389.7970 23.7415 -4.1336 375.7180 379.8516 389.7483 24.5335 -4.1334 375.7982 379.9316 389.6975 25.3255 -4.1323 375.8810 380.0132 389.6532 26.1478 -4.1269 375.9792 380.1061 389.6103 26.9095 -4.1265 376.0476 380.1741 389.5726 27.7608 -4.1233 376.1323 380.2556 389.5100 28.5225 -4.1185 376.2065 380.3250 389.4548 29.3430 -4.1167 376.2779 380.3945 389.3918 30.1645 -4.1146 376.3589 380.4735 389.3529 30.9245 -4.1113 376.4366 380.5480 389.3031 31.7753 -4.1085 376.5220 380.6305 389.2277 32.5665 -4.1062 376.6018 380.7081 389.1712 33.3565 -4.1031 376.6789 380.7820 389.1120 34.1773 -4.1005 376.7655 380.8660 389.0376 34.9388 -4.0995 376.8252 380.9247 388.9928 35.7910 -4.0958 376.9135 381.0093 388.9265 36.5518 -4.0933 376.9855 381.0788 388.8691 37.3738 -4.0866 377.0529 381.1394 388.8021 38.1960 -4.0785 377.1228 381.2014 388.7539 38.9560 -4.0764 377.2024 381.2788 388.6807 39.8070 -4.0746 377.2863 381.3609 388.6005 40.5670 -4.0632 377.3629 381.4261 388.5443 41.3885 -4.0644 377.4353 381.4996 388.4653 42.1805 -4.0658 377.5000 381.5659 388.4011 42.9725 -4.0635 377.5565 381.6200 388.3420 43.8228 -4.0504 377.6339 381.6842 388.2613 44.5835 -4.0516 377.7084 381.7600 388.1820 45.4065 -4.0523 377.7884 381.8407 388.1093 46.1985 -4.0500 377.8625 381.9125 388.0417 46.9903 -4.0448 377.9257 381.9706 387.9520 47.8115 -4.0400 377.9972 382.0372 387.8782 48.6025 -4.0389 378.0633 382.1023 387.8009 49.4240 -4.0342 378.1309 382.1651 387.7219 50.2155 -4.0314 378.1804 382.2118 387.6562 51.0070 -4.0289 378.2509 382.2798 387.5817 51.8285 -4.0254 378.3159 382.3413 387.5015 52.6205 -4.0185 378.3839 382.4024 387.4203 53.4425 -4.0172 378.4774 382.4946 387.3443 54.2340 -4.0150 378.5033 382.5183 387.2675 55.0255 -4.0090 378.5658 382.5747 387.2025 55.8460 -4.0036 378.6334 382.6370 387.1184 56.6068 -4.0015 378.6880 382.6895 387.0351 57.4585 -3.9984 378.7640 382.7625 386.9650 58.2498 -3.9936 378.8324 382.8260 386.8818 59.0398 -3.9936 378.8804 382.8741 386.8300 59.8613 -3.9887 378.9426 382.9314 386.7727 60.6228 -3.9835 378.9793 382.9628 386.7079 61.4748 -3.9840 379.0470 383.0309 386.6413 62.2653 -3.9806 379.1059 383.0865 386.5660 63.0565 -3.9745 379.1731 383.1475 386.5184 63.8785 -3.9656 379.2213 383.1869 386.4449 64.6393 -3.9628 379.2867 383.2495 386.3980 65.4910 -3.9631 379.3382 383.3014 386.3549 66.2528 -3.9613 379.3973 383.3586 386.2982 67.0745 -3.9569 379.4401 383.3969 386.2290 67.8668 -3.9532 379.4825 383.4357 386.1794 68.6578 -3.9514 379.5380 383.4894 386.1431 69.5088 -3.9467 379.5998 383.5464 386.0910 70.2705 -3.9455 379.6480 383.5935 386.0554 71.0920 -3.9430 379.6867 383.6297 386.0059 71.8835 -3.9395 379.7434 383.6829 385.9534 72.6755 -3.9377 379.8044 383.7421 385.9189 73.4975 -3.9325 379.8655 383.7980 385.8511 74.2595 -3.9312 379.8947 383.8259 385.8074 75.1115 -3.9264 379.9597 383.8861 385.7517 75.9035 -3.9210 379.9949 383.9159 385.7077 76.6955 -3.9186 380.0543 383.9729 385.6590 77.5175 -3.9128 380.0961 384.0089 385.6109 78.2795 -3.9083 380.1345 384.0428 385.5579 79.1315 -3.9034 380.1992 384.1026 385.4940 79.8935 -3.9026 380.2339 384.1365 385.4459 80.7155 -3.9037 380.2875 384.1912 385.4106 81.5075 -3.8957 380.3150 384.2108 385.3381 82.2995 -3.8907 380.3577 384.2483 385.2852 83.1508 -3.8852 380.4074 384.2926 385.2177 83.9098 -3.8800 380.4405 384.3205 385.1733 84.7310 -3.8755 380.4913 384.3667 385.1261 85.5233 -3.8748 380.5403 384.4151 385.0741 86.3145 -3.8710 380.5913 384.4623 385.0155 87.1660 -3.8648 380.6236 384.4885 384.9471 87.9278 -3.8637 380.6683 384.5320 384.9237 88.7493 -3.8627 380.7127 384.5754 384.8674 89.5410 -3.8626 380.7367 384.5994 384.8310 90.3313 -3.8618 380.7920 384.6537 384.7712 91.1828 -3.8564 380.8176 384.6740 384.7065 91.9438 -3.8504 380.8579 384.7083 384.6466 92.7653 -3.8449 380.8900 384.7349 384.6094 93.5568 -3.8430 380.9251 384.7682 384.5460 94.3478 -3.8393 380.9683 384.8076 384.4880 95.1695 -3.8342 381.0077 384.8419 384.4376 95.9608 -3.8321 381.0430 384.8751 384.3688 96.7820 -3.8271 381.0972 384.9243 384.3029 97.5725 -3.8168 381.1102 384.9270 384.2523 98.3635 -3.8160 381.1411 384.9571 384.2054 99.1845 -3.8150 381.1798 384.9948 384.1378 99.9765 -3.8125 381.2190 385.0315 384.0804 100.7975 -3.8063 381.2426 385.0490 384.0390 101.5880 -3.7962 381.2914 385.0876 383.9753 102.3785 -3.7998 381.3135 385.1133 383.9095 103.2005 -3.7968 381.3375 385.1343 383.8611 103.9640 -3.7964 381.3731 385.1695 383.7984 104.8178 -3.7930 381.3951 385.1881 383.7288 105.6085 -3.7928 381.4176 385.2104 383.6628 106.3998 -3.7879 381.4578 385.2457 383.6074 107.2200 -3.7821 381.4796 385.2617 383.5540 107.9813 -3.7774 381.5075 385.2850 383.4908 108.8325 -3.7754 381.5608 385.3362 383.4293 109.6243 -3.7716 381.5722 385.3438 383.3578 110.4155 -3.7659 381.5973 385.3631 383.3113 111.2370 -3.7612 381.6274 385.3886 383.2720 111.9985 -3.7572 381.6478 385.4050 383.2058 112.8510 -3.7517 381.6851 385.4368 383.1484 113.6128 -3.7505 381.6918 385.4423 383.0790 114.4343 -3.7457 381.7331 385.4788 383.0117 115.2573 -3.7365 381.7644 385.5009 382.9660 116.0183 -3.7298 381.7889 385.5187 382.9071 116.8708 -3.7325 381.8193 385.5517 382.8507 117.6328 -3.7313 381.8285 385.5597 382.7853 118.4545 -3.7311 381.8551 385.5862 382.7308 119.2455 -3.7267 381.8787 385.6053 382.6745 120.0375 -3.7228 381.8985 385.6213 382.6064 120.8655 -3.7186 381.9187 385.6373 382.5601 121.6558 -3.7161 381.9333 385.6494 382.4971 122.4770 -3.7153 381.9600 385.6753 382.4427 123.2660 -3.7134 381.9770 385.6904 382.3801 124.0558 -3.7062 381.9970 385.7032 382.3349 124.8770 -3.7005 382.0157 385.7162 382.2931 125.6685 -3.7005 382.0376 385.7381 382.2380 126.4905 -3.6971 382.0510 385.7481 382.1863 127.2820 -3.6878 382.0728 385.7606 382.1102 128.0733 -3.6841 382.0929 385.7770 382.0550 128.8945 -3.6860 382.1096 385.7956 381.9889 129.6565 -3.6851 382.1147 385.7998 381.9295 130.5083 -3.6848 382.1511 385.8358 381.8796 131.2975 -3.6813 382.1633 385.8446 381.8144 132.0878 -3.6785 382.1809 385.8594 381.7514 132.9085 -3.6725 382.1951 385.8676 381.6784 133.6995 -3.6700 382.2261 385.8961 381.6127 134.5215 -3.6691 382.2319 385.9011 381.5565 135.3135 -3.6651 382.2314 385.8964 381.4885 136.1045 -3.6650 382.2268 385.8919 381.4286 136.9270 -3.6611 382.2447 385.9058 381.3606 137.6875 -3.6583 382.2564 385.9147 381.2853 138.5390 -3.6528 382.2804 385.9332 381.2245 139.3293 -3.6480 382.3017 385.9497 381.1681 140.1200 -3.6385 382.3158 385.9543 381.0990 140.9420 -3.6400 382.3256 385.9656 381.0513 141.7330 -3.6400 382.3428 385.9828 380.9817 142.5548 -3.6360 382.3475 385.9834 380.9250 143.3468 -3.6283 382.3694 385.9977 380.8510 144.1378 -3.6280 382.3666 385.9947 380.7964 144.9598 -3.6269 382.3924 386.0194 380.7349 145.7215 -3.6274 382.3865 386.0139 380.6547 146.5735 -3.6164 382.4033 386.0197 380.5846 147.3638 -3.6175 382.4024 386.0199 380.5304 148.1548 -3.6146 382.4046 386.0192 380.4772 148.9755 -3.6113 382.4008 386.0122 380.4030 149.7370 -3.6075 382.4232 386.0307 380.3560 150.5878 -3.6051 382.4277 386.0328 380.2851 151.3785 -3.5989 382.4306 386.0295 380.2311 152.1693 -3.6011 382.4367 386.0378 380.1692 152.9950 -3.5960 382.4319 386.0279 380.0945 153.7560 -3.5931 382.4420 386.0351 380.0168 154.6073 -3.5805 382.4562 386.0367 379.9735 155.3973 -3.5762 382.4564 386.0325 379.8966 156.1883 -3.5798 382.4546 386.0345 379.8382 157.0090 -3.5798 382.4696 386.0494 379.8098 157.7705 -3.5795 382.4744 386.0540 379.7337 158.6225 -3.5793 382.4862 386.0655 379.6658 159.4145 -3.5751 382.4814 386.0565 379.6022 160.2063 -3.5665 382.4731 386.0397 379.5421 161.0288 -3.5588 382.4683 386.0271 379.4816 161.7905 -3.5625 382.4841 386.0466 379.4306 162.6423 -3.5623 382.4971 386.0594 379.3514 163.4030 -3.5594 382.4904 386.0498 379.3015 164.2248 -3.5545 382.4962 386.0507 379.2617 165.0470 -3.5547 382.4792 386.0339 379.1867 165.8085 -3.5506 382.4759 386.0266 379.1399 166.6610 -3.5478 382.4800 386.0278 379.0754 167.4228 -3.5469 382.4802 386.0271 379.0222 168.2448 -3.5398 382.4799 386.0197 378.9559 169.0370 -3.5394 382.4732 386.0126 378.9151 169.8283 -3.5366 382.4758 386.0124 378.8519 170.6795 -3.5303 382.4740 386.0043 378.7829 171.4400 -3.5312 382.4703 386.0015 378.7510 172.2608 -3.5270 382.4752 386.0022 378.6964 173.0513 -3.5178 382.4832 386.0010 378.6309 173.8418 -3.5117 382.4725 385.9842 378.5802 174.6935 -3.5185 382.4643 385.9828 378.5138 175.4545 -3.5199 382.4574 385.9773 378.4529 176.2765 -3.5178 382.4379 385.9557 378.3996 177.0685 -3.5118 382.4366 385.9484 378.3495 177.8605 -3.5096 382.4362 385.9459 378.2769 178.6835 -3.5076 382.4341 385.9417 378.2391 179.4760 -3.5027 382.4285 385.9311 378.1741 180.2975 -3.4991 382.4139 385.9130 378.1114 181.0888 -3.4952 382.4071 385.9023 378.0489 181.8790 -3.4934 382.3941 385.8875 377.9873 182.6985 -3.4935 382.3976 385.8911 377.9384 183.4898 -3.4906 382.3835 385.8742 377.8700 184.3105 -3.4876 382.3832 385.8708 377.8068 185.1025 -3.4864 382.3687 385.8551 377.7381 185.8943 -3.4831 382.3660 385.8492 377.6778 186.7163 -3.4792 382.3692 385.8484 377.6235 187.4778 -3.4760 382.3583 385.8344 377.5496 188.3300 -3.4735 382.3465 385.8200 377.4808 189.0908 -3.4725 382.3521 385.8246 377.4413 189.9128 -3.4674 382.3189 385.7863 377.3907 190.7350 -3.4631 382.3192 385.7824 377.3013 191.4965 -3.4624 382.3305 385.7929 377.2257 192.3490 -3.4607 382.2964 385.7572 377.1583 193.1098 -3.4570 382.2711 385.7281 377.1037 193.9318 -3.4540 382.2663 385.7203 377.0412 194.7238 -3.4536 382.2570 385.7106 376.9859 195.5155 -3.4543 382.2434 385.6977 376.9295 196.3673 -3.4515 382.2300 385.6815 376.8646 197.1285 -3.4496 382.2224 385.6720 376.8004 197.9505 -3.4466 382.2055 385.6522 376.7327 198.7425 -3.4433 382.1957 385.6390 376.6817 199.5345 -3.4384 382.1827 385.6212 376.6098 200.3565 -3.4367 382.1762 385.6129 376.5610 201.1485 -3.4340 382.1589 385.5929 376.5097 201.9703 -3.4311 382.1367 385.5679 376.4393 202.7408 -3.4304 382.1266 385.5570 376.3858 203.5625 -3.4258 382.1230 385.5488 376.3135 204.3545 -3.4227 382.0960 385.5187 376.2517 205.1465 -3.4220 382.0904 385.5124 376.2032 205.9975 -3.4189 382.0623 385.4811 376.1340 206.7585 -3.4165 382.0604 385.4769 376.0815 207.5805 -3.4169 382.0338 385.4508 376.0105 208.3725 -3.4151 382.0100 385.4251 375.9544 209.1640 -3.4095 381.9773 385.3868 375.9051 209.9845 -3.4102 381.9756 385.3857 375.8493 210.7765 -3.4232 381.9585 385.3817 375.7810 211.5985 -3.4220 381.9408 385.3628 375.7236 212.3903 -3.4087 381.9306 385.3394 375.6463 213.1808 -3.3995 381.9274 385.3269 375.6075 214.0013 -3.3954 381.8903 385.2857 375.5451 214.7625 -3.3917 381.8749 385.2666 375.4971 215.6148 -3.3921 381.8616 385.2537 375.4392 216.4060 -3.3962 381.8421 385.2383 375.3864 217.1975 -3.3956 381.8278 385.2234 375.3216 218.0200 -3.3932 381.8126 385.2058 375.2507 218.7805 -3.3933 381.7923 385.1856 375.1993 219.6328 -3.3829 381.7712 385.1541 375.1396 220.3920 -3.3777 381.7536 385.1313 375.0805 221.2130 -3.3739 381.7251 385.0990 375.0247 222.0328 -3.3725 381.6936 385.0661 374.9823 222.8063 -3.3682 381.6836 385.0518 374.9279 223.6410 -3.3678 381.6623 385.0302 374.8434 224.4325 -3.3708 381.6422 385.0130 374.7735 225.2543 -3.3716 381.6139 384.9855 374.7242 226.0455 -3.3696 381.5979 384.9675 374.6381 226.8370 -3.3681 381.5822 384.9504 374.5897 227.6585 -3.3646 381.5556 384.9203 374.5275 228.4205 -3.3613 381.5311 384.8925 374.4548 229.2723 -3.3505 381.5006 384.8512 374.3924 230.0335 -3.3491 381.4963 384.8454 374.3334 230.8553 -3.3450 381.4744 384.8194 374.2682 231.6765 -3.3415 381.4554 384.7969 374.1973 232.4375 -3.3377 381.4002 384.7378 374.1349 233.2893 -3.3347 381.3826 384.7173 374.0645 234.0488 -3.3333 381.3638 384.6971 374.0057 234.8705 -3.3301 381.3444 384.6746 373.9283 235.6925 -3.3307 381.3232 384.6539 373.8686 236.4538 -3.3284 381.2896 384.6180 373.8054 237.3048 -3.3239 381.2592 384.5830 373.7298 238.0648 -3.3218 381.2294 384.5512 373.6716 238.8868 -3.3213 381.2076 384.5290 373.6075 239.6793 -3.3183 381.1836 384.5020 373.5406 240.4705 -3.3156 381.1419 384.4576 373.4998 241.3228 -3.3134 381.1193 384.4327 373.4258 242.0820 -3.3120 381.1129 384.4249 373.3618 242.9030 -3.3090 381.0906 384.3996 373.3004 243.6848 -3.3092 381.0544 384.3635 373.2140 244.5068 -3.3048 381.0230 384.3278 373.1371 245.2990 -3.3008 381.0174 384.3183 373.0866 246.0905 -3.2983 380.9851 384.2834 373.0264 246.9128 -3.2945 380.9703 384.2648 372.9521 247.7045 -3.2932 380.9369 384.2301 372.9001 248.5263 -3.2922 380.9065 384.1987 372.8340 249.3175 -3.2896 380.8687 384.1583 372.7558 250.1095 -3.2861 380.8504 384.1365 372.6984 250.9315 -3.2815 380.8194 384.1009 372.6391 251.7213 -3.2812 380.7766 384.0578 372.5792 252.5408 -3.2788 380.7684 384.0472 372.5005 253.3305 -3.2779 380.7412 384.0192 372.4426 254.1208 -3.2747 380.6947 383.9693 372.3871 254.9415 -3.2732 380.6576 383.9308 372.3400 255.7335 -3.2704 380.6400 383.9104 372.2790 256.5555 -3.2688 380.6135 383.8824 372.1948 257.3473 -3.2675 380.5827 383.8502 372.1424 258.1385 -3.2631 380.5480 383.8111 372.0739 258.9605 -3.2685 380.5104 383.7788 372.0127 259.7525 -3.2699 380.4783 383.7482 371.9502 260.5745 -3.2693 380.4512 383.7205 371.8998 261.3665 -3.2717 380.4164 383.6881 371.8323 262.1578 -3.2686 380.3809 383.6495 371.7642 262.9793 -3.2670 380.3606 383.6277 371.7227 263.7500 -3.2624 380.3392 383.6016 371.6782 264.5823 -3.2627 380.3093 383.5719 371.5892 265.3430 -3.2595 380.2622 383.5217 371.5273 266.1950 -3.2443 380.2233 383.4675 371.4737 266.9870 -3.2363 380.1933 383.4296 371.4011 267.7778 -3.2349 380.1615 383.3964 371.3434 268.5990 -3.2332 380.1412 383.3744 371.2956 269.3593 -3.2276 380.1065 383.3341 371.2348 270.2115 -3.2280 380.0696 383.2976 371.2030 271.0023 -3.2397 380.0395 383.2792 371.1245 271.7935 -3.2626 380.0014 383.2640 371.0671 272.6150 -3.2682 379.9622 383.2304 371.0003 273.3760 -3.2538 379.9269 383.1807 370.9260 274.2275 -3.2275 379.8890 383.1165 370.8745 275.0168 -3.2195 379.8601 383.0796 370.8312 275.8085 -3.2185 379.8180 383.0365 370.7768 276.6305 -3.2183 379.7986 383.0169 370.7333 277.3925 -3.2143 379.7792 382.9936 370.6813 278.2445 -3.2126 379.7327 382.9453 370.6023 279.0365 -3.2119 379.7010 382.9129 370.5304 279.8285 -3.2089 379.6673 382.8762 370.4919 280.6505 -3.2051 379.6231 382.8282 370.4383 281.4125 -3.2071 379.6188 382.8259 370.3898 282.2635 -3.2031 379.5591 382.7622 370.3062 283.0233 -3.2002 379.5252 382.7253 370.2426 283.8435 -3.1982 379.4820 382.6801 370.1790 284.6655 -3.1964 379.4469 382.6432 370.0986 285.4275 -3.1946 379.4137 382.6083 370.0564 286.2795 -3.1932 379.3759 382.5690 369.9860 287.0415 -3.1924 379.3500 382.5424 369.9152 287.8635 -3.1869 379.3008 382.4877 369.8494 288.6855 -3.1865 379.2675 382.4540 369.7882 289.4468 -3.1844 379.2419 382.4263 369.7183 290.2990 -3.1814 379.1895 382.3710 369.6574 291.0608 -3.1760 379.1542 382.3302 369.5819 291.8828 -3.1729 379.1131 382.2861 369.5141 292.6750 -3.1717 379.0758 382.2475 369.4477 293.4663 -3.1671 379.0459 382.2130 369.3843 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