DTA measure 1termo2 Test Date: 2023103:1155 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1201.29 s Mass = 1437.600 mg data_number = 1487 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1815 -2.1078 243.2279 245.3357 266.1582 1.9498 -2.1152 243.3164 245.4317 266.1374 2.7800 -2.1218 243.3981 245.5199 266.1181 3.5715 -2.1256 243.5064 245.6321 266.1122 4.3653 -2.1309 243.5905 245.7214 266.1148 5.1895 -2.1344 243.6840 245.8183 266.1414 5.9513 -2.1396 243.7506 245.8902 266.1372 6.8033 -2.1427 243.8611 246.0038 266.1595 7.5948 -2.1479 243.9415 246.0894 266.1693 8.3868 -2.1501 244.0244 246.1745 266.1796 9.2088 -2.1558 244.1078 246.2636 266.2223 9.9700 -2.1631 244.1973 246.3604 266.2658 10.8215 -2.1656 244.3022 246.4678 266.3190 11.5825 -2.1714 244.3809 246.5523 266.3575 12.4045 -2.1772 244.4757 246.6529 266.4113 13.2258 -2.1809 244.5542 246.7351 266.4645 13.9880 -2.1839 244.6338 246.8177 266.5333 14.8408 -2.1886 244.7457 246.9343 266.6219 15.6025 -2.1934 244.8405 247.0339 266.6881 16.4245 -2.1984 244.9202 247.1186 266.7749 17.2468 -2.1994 245.0146 247.2140 266.8763 18.0103 -2.2028 245.0987 247.3015 266.9663 18.8685 -2.2062 245.1906 247.3968 267.1022 19.6033 -2.2097 245.2651 247.4748 267.1971 20.4615 -2.2143 245.3644 247.5787 267.3337 21.2265 -2.2171 245.4623 247.6794 267.4392 22.0485 -2.2221 245.5503 247.7724 267.5739 22.8698 -2.2266 245.6352 247.8617 267.7020 23.6305 -2.2296 245.7470 247.9766 267.8404 24.4823 -2.2328 245.8263 248.0591 267.9905 25.2440 -2.2367 245.8980 248.1347 268.1207 26.0665 -2.2394 245.9823 248.2216 268.2801 26.8585 -2.2428 246.0993 248.3421 268.4229 27.6505 -2.2470 246.1889 248.4359 268.5814 28.5025 -2.2517 246.2691 248.5208 268.7472 29.2635 -2.2554 246.3543 248.6097 268.8818 30.0855 -2.2575 246.4516 248.7091 269.0336 30.8783 -2.2614 246.5436 248.8050 269.2030 31.6705 -2.2677 246.6323 248.9000 269.3714 32.4923 -2.2699 246.7322 249.0021 269.5440 33.2843 -2.2752 246.8136 249.0889 269.6928 34.1058 -2.2786 246.9259 249.2045 269.8473 34.8998 -2.2824 247.0120 249.2944 270.0051 35.6955 -2.2855 247.1009 249.3864 270.1652 36.5185 -2.2899 247.1876 249.4775 270.3212 37.2810 -2.2958 247.2791 249.5748 270.4676 38.1093 -2.3001 247.3743 249.6744 270.6271 38.9005 -2.3031 247.4637 249.7668 270.7606 39.7225 -2.3086 247.5565 249.8651 270.9224 40.5135 -2.3140 247.6567 249.9707 271.0479 41.3048 -2.3159 247.7484 250.0644 271.1723 42.1268 -2.3193 247.8439 250.1632 271.3360 42.9185 -2.3283 247.9381 250.2664 271.4703 43.7405 -2.3330 248.0247 250.3576 271.6041 44.5363 -2.3370 248.1286 250.4656 271.7194 45.3275 -2.3403 248.2197 250.5599 271.8446 46.1495 -2.3427 248.3310 250.6736 271.9891 46.9115 -2.3487 248.4074 250.7561 272.0861 47.7635 -2.3534 248.5154 250.8688 272.2177 48.5255 -2.3576 248.6124 250.9700 272.3265 49.3475 -2.3600 248.6998 251.0598 272.4491 50.1695 -2.3645 248.8055 251.1700 272.5713 50.9310 -2.3702 248.8986 251.2688 272.6749 51.7825 -2.3728 249.0056 251.3784 272.7893 52.5445 -2.3778 249.0969 251.4748 272.8684 53.3670 -2.3814 249.1768 251.5582 272.9684 54.1885 -2.3861 249.2759 251.6620 273.0862 54.9505 -2.3891 249.3809 251.7700 273.1810 55.8023 -2.3951 249.4751 251.8702 273.2839 56.5635 -2.3991 249.5690 251.9681 273.3665 57.3845 -2.4013 249.6591 252.0604 273.4469 58.1760 -2.4066 249.7488 252.1554 273.5211 58.9673 -2.4111 249.8481 252.2592 273.6123 59.8188 -2.4144 249.9417 252.3561 273.7211 60.5803 -2.4195 250.0334 252.4529 273.7858 61.4028 -2.4229 250.1324 252.5553 273.8770 62.1948 -2.4270 250.2472 252.6742 273.9385 62.9858 -2.4318 250.3507 252.7825 274.0175 63.8233 -2.4366 250.4430 252.8796 274.1002 64.5853 -2.4410 250.5190 252.9600 274.1769 65.4390 -2.4473 250.6234 253.0706 274.2547 66.2050 -2.4525 250.7271 253.1796 274.3328 67.0273 -2.4564 250.8196 253.2760 274.4125 67.8188 -2.4609 250.9247 253.3856 274.5053 68.6105 -2.4659 251.0167 253.4827 274.5651 69.4328 -2.4685 251.1092 253.5777 274.6497 70.1945 -2.4748 251.2069 253.6817 274.7345 71.0463 -2.4813 251.3099 253.7912 274.8279 71.8375 -2.4837 251.3957 253.8794 274.9139 72.6288 -2.4861 251.4912 253.9774 275.0024 73.4505 -2.4902 251.5950 254.0852 275.0777 74.2115 -2.4944 251.6676 254.1620 275.1654 75.0633 -2.4988 251.7805 254.2793 275.2545 75.8245 -2.5035 251.8725 254.3760 275.3376 76.6460 -2.5075 251.9600 254.4675 275.4229 77.4675 -2.5114 252.0603 254.5716 275.5204 78.2285 -2.5129 252.1646 254.6775 275.6008 79.0805 -2.5184 252.2656 254.7840 275.7103 79.8428 -2.5224 252.3506 254.8730 275.7966 80.6640 -2.5318 252.4455 254.9773 275.8795 81.4555 -2.5397 252.5440 255.0837 275.9746 82.2475 -2.5446 252.6274 255.1720 276.0652 83.0695 -2.5445 252.7356 255.2801 276.1833 83.8605 -2.5518 252.8432 255.3949 276.2963 84.6815 -2.5547 252.9339 255.4886 276.4235 85.4733 -2.5574 253.0199 255.5773 276.5017 86.2650 -2.5559 253.1231 255.6790 276.6148 87.0875 -2.5557 253.2156 255.7713 276.7386 87.8548 -2.5585 253.3065 255.8650 276.8418 88.7100 -2.5606 253.4205 255.9811 276.9659 89.4708 -2.5649 253.5076 256.0725 277.0678 90.2940 -2.5682 253.6112 256.1794 277.1812 91.0920 -2.5713 253.7033 256.2747 277.2903 91.8855 -2.5748 253.8017 256.3764 277.4108 92.7200 -2.5779 253.9049 256.4827 277.5396 93.4853 -2.5815 254.0042 256.5858 277.6628 94.3078 -2.5846 254.1050 256.6895 277.7758 95.1068 -2.5865 254.2085 256.7949 277.8950 95.9308 -2.5915 254.2974 256.8889 278.0249 96.6970 -2.5923 254.3899 256.9821 278.1440 97.5230 -2.5982 254.5027 257.1009 278.2651 98.3145 -2.6033 254.5836 257.1869 278.3866 99.1363 -2.6080 254.6834 257.2914 278.5025 99.9275 -2.6088 254.7815 257.3904 278.6305 100.7193 -2.6102 254.8622 257.4724 278.7419 101.5478 -2.6140 254.9717 257.5857 278.8717 102.3098 -2.6173 255.0709 257.6882 278.9884 103.1615 -2.6218 255.1760 257.7978 279.1048 103.9250 -2.6258 255.2486 257.8744 279.2281 104.7455 -2.6270 255.3546 257.9816 279.3482 105.5430 -2.6297 255.4549 258.0845 279.4613 106.3385 -2.6321 255.5565 258.1886 279.5784 107.1605 -2.6353 255.6627 258.2980 279.7025 107.9225 -2.6370 255.7428 258.3798 279.8008 108.7745 -2.6392 255.8588 258.4980 279.9199 109.5665 -2.6425 255.9603 258.6028 280.0354 110.3585 -2.6456 256.0507 258.6963 280.1515 111.1788 -2.6491 256.1540 258.8031 280.2593 111.9395 -2.6486 256.2416 258.8902 280.3552 112.7913 -2.6505 256.3423 258.9928 280.4693 113.5530 -2.6550 256.4498 259.1047 280.5710 114.3765 -2.6581 256.5534 259.2115 280.6905 115.1985 -2.6623 256.6540 259.3164 280.7910 115.9595 -2.6644 256.7459 259.4103 280.8913 116.8120 -2.6672 256.8453 259.5125 281.0005 117.5763 -2.6700 256.9463 259.6162 281.1130 118.3998 -2.6711 257.0430 259.7140 281.2146 119.1918 -2.6744 257.1360 259.8105 281.3009 120.1680 -2.6781 257.2705 259.9486 281.4349 120.9913 -2.6822 257.3747 260.0569 281.5353 121.8128 -2.6848 257.4687 260.1535 281.6370 122.6048 -2.6884 257.5775 260.2658 281.7245 123.3963 -2.6906 257.6656 260.3562 281.8364 124.1963 -2.6937 257.7780 260.4717 281.9444 124.9900 -2.6972 257.8634 260.5606 282.0253 125.8415 -2.7005 257.9736 260.6741 282.1499 126.6045 -2.7039 258.0705 260.7743 282.2350 127.4278 -2.7045 258.1894 260.8938 282.3236 128.2208 -2.7097 258.2902 260.9999 282.4301 129.0125 -2.7148 258.3716 261.0863 282.5272 129.8345 -2.7163 258.4665 261.1827 282.6158 130.5965 -2.7201 258.5697 261.2898 282.7300 131.4485 -2.7239 258.6883 261.4122 282.8096 132.2405 -2.7261 258.7801 261.5062 282.9156 133.0325 -2.7294 258.8650 261.5944 283.0155 133.8635 -2.7336 258.9538 261.6874 283.1078 134.6288 -2.7342 259.0635 261.7977 283.1797 135.4538 -2.7374 259.1715 261.9089 283.2825 136.2455 -2.7393 259.2644 262.0038 283.3823 137.0675 -2.7455 259.3535 262.0989 283.4838 137.8295 -2.7470 259.4510 262.1981 283.5725 138.6825 -2.7527 259.5570 262.3097 283.6689 139.4468 -2.7569 259.6449 262.4018 283.7477 140.2723 -2.7581 259.7566 262.5147 283.8504 141.0645 -2.7611 259.8512 262.6123 283.9406 141.8560 -2.7646 259.9374 262.7020 284.0326 142.6780 -2.7657 260.0560 262.8217 284.1207 143.4488 -2.7665 260.1536 262.9200 284.2133 144.3000 -2.7683 260.2627 263.0310 284.3237 145.0440 -2.7705 260.3589 263.1294 284.4076 145.8753 -2.7725 260.4582 263.2307 284.5193 146.6670 -2.7746 260.5611 263.3357 284.6215 147.5188 -2.7779 260.6754 263.4533 284.7234 148.2835 -2.7782 260.7580 263.5362 284.8113 149.1055 -2.7781 260.8611 263.6392 284.9134 149.9010 -2.7801 260.9574 263.7374 285.0177 150.6938 -2.7809 261.0462 263.8271 285.1160 151.5198 -2.7821 261.1622 263.9443 285.2372 152.2805 -2.7846 261.2628 264.0474 285.3303 153.1325 -2.7849 261.3496 264.1345 285.4423 153.8945 -2.7871 261.4524 264.2396 285.5414 154.7170 -2.7879 261.5713 264.3592 285.6569 155.4805 -2.7902 261.6688 264.4591 285.7468 156.3348 -2.7919 261.7682 264.5601 285.8537 157.0955 -2.7955 261.8679 264.6634 285.9561 157.9475 -2.7978 261.9674 264.7653 286.0604 158.7095 -2.7988 262.0667 264.8655 286.1571 159.5315 -2.7993 262.1565 264.9558 286.2711 160.3540 -2.8016 262.2745 265.0761 286.3698 161.1173 -2.8024 262.3717 265.1741 286.4787 161.9703 -2.8034 262.4752 265.2785 286.6071 162.7315 -2.8058 262.5622 265.3680 286.7053 163.5535 -2.8096 262.6688 265.4784 286.8167 164.3783 -2.8088 262.7838 265.5925 286.9289 165.1410 -2.8098 262.8795 265.6893 287.0159 165.9968 -2.8118 262.9745 265.7863 287.1399 166.7305 -2.8142 263.0724 265.8866 287.2606 167.5843 -2.8170 263.1726 265.9896 287.3628 168.3813 -2.8176 263.2748 266.0924 287.4566 169.1785 -2.8201 263.3744 266.1945 287.5516 169.9713 -2.8221 263.4795 266.3016 287.6813 170.7630 -2.8229 263.5797 266.4026 287.7769 171.5860 -2.8233 263.6894 266.5127 287.8893 172.3778 -2.8253 263.7790 266.6043 288.0071 173.2033 -2.8260 263.8814 266.7074 288.1154 173.9958 -2.8257 263.9974 266.8231 288.2218 174.7868 -2.8277 264.0928 266.9205 288.3215 175.6090 -2.8301 264.1881 267.0182 288.4342 176.3725 -2.8296 264.2934 267.1230 288.5312 177.2300 -2.8301 264.4012 267.2313 288.6508 177.9918 -2.8321 264.4930 267.3251 288.7540 178.8135 -2.8353 264.6133 267.4486 288.8751 179.6100 -2.8320 264.7084 267.5404 288.9613 180.4110 -2.8336 264.8088 267.6425 289.0646 181.2325 -2.8335 264.9302 267.7636 289.1789 181.9948 -2.8338 265.0286 267.8624 289.2904 182.8465 -2.8387 265.1266 267.9653 289.3962 183.6095 -2.8381 265.2106 268.0487 289.4950 184.5518 -2.8387 265.3397 268.1784 289.6074 185.3135 -2.8404 265.4421 268.2824 289.7152 186.1355 -2.8417 265.5495 268.3911 289.8243 186.9275 -2.8410 265.6372 268.4783 289.9218 187.7195 -2.8389 265.7600 268.5988 290.0225 188.5715 -2.8408 265.8473 268.6880 290.1398 189.3335 -2.8439 265.9444 268.7883 290.2243 190.1555 -2.8433 266.0514 268.8947 290.3446 190.9475 -2.8443 266.1484 268.9927 290.4525 191.7395 -2.8454 266.2428 269.0882 290.5370 192.5615 -2.8457 266.3439 269.1896 290.6461 193.3233 -2.8473 266.4588 269.3061 290.7408 194.1750 -2.8455 266.5711 269.4165 290.8504 194.9675 -2.8475 266.6671 269.5147 290.9540 195.7590 -2.8477 266.7798 269.6276 291.0563 196.5813 -2.8502 266.8933 269.7435 291.1570 197.3425 -2.8521 266.9954 269.8475 291.2676 198.1948 -2.8530 267.0791 269.9321 291.3667 198.9570 -2.8550 267.1694 270.0244 291.4641 199.7793 -2.8552 267.2855 270.1407 291.5615 200.6028 -2.8557 267.3848 270.2404 291.6719 201.3635 -2.8560 267.4983 270.3543 291.7744 202.2158 -2.8586 267.6053 270.4638 291.8866 202.9785 -2.8585 267.6913 270.5498 291.9906 203.8018 -2.8571 267.8034 270.6605 292.0818 204.5940 -2.8580 267.9037 270.7616 292.2005 205.3855 -2.8549 268.0082 270.8631 292.3237 206.2075 -2.8573 268.1017 270.9590 292.4366 206.9695 -2.8597 268.2057 271.0654 292.5338 207.8223 -2.8611 268.3052 271.1662 292.6432 208.6155 -2.8619 268.4146 271.2765 292.7562 209.4075 -2.8598 268.5175 271.3773 292.8801 210.2295 -2.8628 268.6243 271.4871 292.9819 210.9915 -2.8647 268.7107 271.5753 293.0984 211.8435 -2.8648 268.8383 271.7031 293.2267 212.6055 -2.8645 268.9449 271.8094 293.3357 213.4275 -2.8672 269.0334 271.9006 293.4578 214.2195 -2.8686 269.1382 272.0069 293.5616 215.0115 -2.8701 269.2285 272.0986 293.6811 215.8635 -2.8688 269.3403 272.2091 293.7953 216.6255 -2.8709 269.4449 272.3157 293.9010 217.4475 -2.8718 269.5507 272.4225 294.0216 218.2395 -2.8719 269.6569 272.5288 294.1359 219.0315 -2.8753 269.7630 272.6384 294.2591 219.8543 -2.8752 269.8676 272.7428 294.4055 220.6163 -2.8749 269.9626 272.8375 294.4925 221.4683 -2.8771 270.0866 272.9636 294.5867 222.2603 -2.8744 270.1838 273.0582 294.7017 223.0520 -2.8756 270.2839 273.1595 294.8203 223.8740 -2.8762 270.3940 273.2701 294.9069 224.6373 -2.8778 270.4819 273.3597 295.0180 225.4920 -2.8778 270.6013 273.4791 295.1213 226.2593 -2.8799 270.7138 273.5937 295.2109 227.0818 -2.8801 270.8251 273.7052 295.3190 227.8740 -2.8810 270.9155 273.7966 295.4384 228.6655 -2.8806 271.0145 273.8951 295.5431 229.4930 -2.8795 271.1110 273.9905 295.6473 230.2545 -2.8800 271.2200 274.1000 295.7478 231.1068 -2.8819 271.3474 274.2294 295.8435 231.8688 -2.8827 271.4301 274.3129 295.9400 232.6908 -2.8788 271.5217 274.4005 296.0375 233.4828 -2.8839 271.6296 274.5136 296.1187 234.2745 -2.8850 271.7478 274.6328 296.2066 235.0965 -2.8848 271.8551 274.7399 296.3177 235.8885 -2.8850 271.9592 274.8442 296.4220 236.7105 -2.8840 272.0616 274.9457 296.5107 237.5030 -2.8848 272.1643 275.0491 296.6091 238.2965 -2.8838 272.2627 275.1466 296.7025 239.1185 -2.8851 272.3705 275.2556 296.8006 239.8805 -2.8852 272.4795 275.3647 296.8826 240.7325 -2.8845 272.5719 275.4563 296.9818 241.4945 -2.8872 272.6858 275.5730 297.0643 242.3165 -2.8880 272.7768 275.6647 297.1612 243.1385 -2.8862 272.9007 275.7869 297.2556 243.9008 -2.8858 273.0040 275.8898 297.3535 244.7535 -2.8856 273.1242 276.0098 297.4566 245.5160 -2.8873 273.2065 276.0938 297.5469 246.3378 -2.8868 273.3032 276.1900 297.6536 247.1590 -2.8881 273.4240 276.3121 297.7525 247.9210 -2.8890 273.5312 276.4202 297.8560 248.7730 -2.8899 273.6395 276.5294 297.9604 249.5350 -2.8892 273.7346 276.6238 298.0540 250.3570 -2.8894 273.8351 276.7246 298.1625 251.1490 -2.8879 273.9393 276.8272 298.2624 251.9410 -2.8879 274.0397 276.9276 298.3560 252.7628 -2.8871 274.1539 277.0410 298.4641 253.5548 -2.8892 274.2711 277.1603 298.5546 254.3768 -2.8866 274.3660 277.2526 298.6686 255.1688 -2.8871 274.4701 277.3571 298.7807 255.9605 -2.8876 274.5865 277.4741 298.8969 256.7838 -2.8874 274.6929 277.5804 298.9981 257.5455 -2.8877 274.7966 277.6843 299.1048 258.4040 -2.8848 274.9035 277.7884 299.2105 259.1665 -2.8849 274.9983 277.8832 299.3154 259.9885 -2.8864 275.0969 277.9833 299.4292 260.7805 -2.8854 275.2083 278.0936 299.5237 261.5725 -2.8867 275.3266 278.2133 299.6340 262.4245 -2.8883 275.4118 278.3001 299.7407 263.1865 -2.8881 275.5186 278.4067 299.8493 264.0095 -2.8881 275.6497 278.5379 299.9768 264.8015 -2.8899 275.7498 278.6397 300.0715 265.5935 -2.8895 275.8533 278.7428 300.1808 266.4158 -2.8917 275.9441 278.8358 300.2863 267.1810 -2.8927 276.0475 278.9403 300.4030 268.0340 -2.8936 276.1489 279.0425 300.5208 268.8265 -2.8927 276.2621 279.1548 300.6324 269.6185 -2.8945 276.3566 279.2511 300.7430 270.4405 -2.8916 276.4651 279.3566 300.8459 271.2025 -2.8927 276.5737 279.4664 300.9535 272.0545 -2.8924 276.6783 279.5707 301.0834 272.8165 -2.8936 276.7842 279.6778 301.1932 273.6385 -2.8946 276.8846 279.7792 301.2870 274.4303 -2.8935 276.9864 279.8799 301.3943 275.2225 -2.8947 277.0879 279.9826 301.5026 276.0753 -2.8962 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