DTA measure 2termo1 Test Date: 2023103:111 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1019.00 s Mass = 1437.600 mg data_number = 1265 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2468 -5.9230 208.3044 214.2274 264.7415 2.0995 -5.9102 208.5884 214.4986 264.8032 2.8595 -5.8981 208.8203 214.7184 264.8594 3.6998 -5.8860 209.0601 214.9461 264.9078 4.4873 -5.8742 209.3149 215.1891 264.9599 5.2795 -5.8601 209.5598 215.4199 265.0174 6.0715 -5.8450 209.8126 215.6576 265.0816 6.9235 -5.8288 210.0587 215.8875 265.1430 7.6855 -5.8182 210.3037 216.1219 265.2185 8.5075 -5.8042 210.5677 216.3719 265.2922 9.2995 -5.7919 210.7986 216.5906 265.3739 10.0915 -5.7779 211.0440 216.8220 265.4701 10.9135 -5.7635 211.2984 217.0619 265.5643 11.6755 -5.7525 211.5181 217.2705 265.6516 12.5275 -5.7378 211.7600 217.4978 265.7926 13.3195 -5.7268 212.0178 217.7445 265.8997 14.1463 -5.7157 212.2700 217.9857 266.0024 14.9120 -5.7020 212.4981 218.2002 266.1253 15.7335 -5.6879 212.7420 218.4298 266.2506 16.4955 -5.6758 212.9859 218.6617 266.3938 17.3475 -5.6624 213.2228 218.8852 266.5313 18.1105 -5.6492 213.4550 219.1042 266.6577 18.9335 -5.6359 213.7014 219.3373 266.8016 19.7555 -5.6203 213.9536 219.5739 266.9540 20.5175 -5.6049 214.1926 219.7975 267.1195 21.3690 -5.5949 214.4319 220.0268 267.2705 22.1313 -5.5829 214.6414 220.2243 267.4358 22.9530 -5.5698 214.8862 220.4560 267.5831 23.7450 -5.5571 215.1252 220.6823 267.7699 24.5893 -5.5437 215.3808 220.9245 267.9290 25.3345 -5.5309 215.5970 221.1279 268.0833 26.1870 -5.5173 215.8392 221.3565 268.2594 26.9493 -5.5061 216.0821 221.5882 268.4132 27.7728 -5.4927 216.3086 221.8013 268.5824 28.5648 -5.4809 216.5424 222.0233 268.7704 29.3565 -5.4692 216.7779 222.2471 268.9699 30.1788 -5.4582 217.0012 222.4594 269.1514 30.9705 -5.4472 217.2311 222.6784 269.3281 31.7928 -5.4353 217.4773 222.9127 269.5029 32.5845 -5.4214 217.7103 223.1317 269.6775 33.3765 -5.4095 217.9529 223.3623 269.8590 34.1985 -5.3976 218.1944 223.5920 270.0425 35.1755 -5.3823 218.4649 223.8472 270.2283 35.9975 -5.3699 218.6968 224.0666 270.4006 36.7895 -5.3567 218.9284 224.2851 270.5748 37.5815 -5.3449 219.1508 224.4958 270.7429 38.4335 -5.3317 219.4089 224.7406 270.9281 39.1955 -5.3219 219.6090 224.9308 271.0900 40.0175 -5.3118 219.8481 225.1599 271.2602 40.8095 -5.2960 220.0809 225.3769 271.4193 41.6015 -5.2838 220.2906 225.5744 271.5666 42.4235 -5.2681 220.5247 225.7928 271.7164 43.2155 -5.2622 220.7578 226.0200 271.8830 44.0375 -5.2513 220.9984 226.2497 272.0334 44.8305 -5.2399 221.2243 226.4642 272.1866 45.6253 -5.2300 221.4285 226.6585 272.3486 46.4525 -5.2167 221.6552 226.8719 272.4868 47.2145 -5.2066 221.8738 227.0804 272.6064 48.0665 -5.1992 222.1206 227.3198 272.7631 48.8285 -5.1905 222.3506 227.5411 272.9027 49.6500 -5.1777 222.5773 227.7550 273.0346 50.4423 -5.1666 222.8025 227.9690 273.1625 51.2338 -5.1544 223.0160 228.1705 273.2829 52.0860 -5.1417 223.2534 228.3951 273.4139 52.8478 -5.1314 223.4673 228.5987 273.5241 53.6698 -5.1199 223.6815 228.8014 273.6730 54.4618 -5.1145 223.9121 229.0266 273.7750 55.3970 -5.1030 224.1708 229.2738 273.9014 56.2960 -5.0908 224.4040 229.4948 274.0238 57.0575 -5.0820 224.6281 229.7100 274.1439 57.8798 -5.0691 224.8381 229.9073 274.2720 58.6715 -5.0600 225.0555 230.1155 274.3620 59.4635 -5.0471 225.2676 230.3147 274.4745 60.2855 -5.0371 225.4835 230.5205 274.5841 61.0778 -5.0317 225.7097 230.7415 274.6881 61.8995 -5.0208 225.9345 230.9553 274.7930 62.6915 -5.0083 226.1734 231.1817 274.9026 63.4835 -4.9966 226.3909 231.3875 275.0225 64.3055 -4.9865 226.6054 231.5919 275.1379 65.0675 -4.9743 226.8026 231.7769 275.2566 65.9195 -4.9634 227.0380 232.0014 275.3548 66.7115 -4.9565 227.2425 232.1991 275.4745 67.5035 -4.9469 227.4565 232.4035 275.5848 68.3255 -4.9345 227.6730 232.6076 275.7109 69.0875 -4.9252 227.8734 232.7986 275.8115 69.9395 -4.9150 228.0931 233.0081 275.9312 70.7028 -4.9060 228.3033 233.2093 276.0428 71.5298 -4.8963 228.5296 233.4260 276.1734 72.3215 -4.8858 228.7280 233.6138 276.2947 73.1135 -4.8771 228.9471 233.8242 276.4243 73.9353 -4.8697 229.1592 234.0289 276.5390 74.6978 -4.8595 229.3694 234.2288 276.6553 75.6458 -4.8480 229.6051 234.4532 276.8054 76.5335 -4.8341 229.8477 234.6818 276.9457 77.3248 -4.8262 230.0385 234.8646 277.0714 78.1473 -4.8188 230.2626 235.0815 277.2029 78.9090 -4.8086 230.4631 235.2717 277.3225 79.7610 -4.7974 230.6887 235.4861 277.4637 80.5530 -4.7880 230.8870 235.6750 277.6130 81.3445 -4.7786 231.1148 235.8934 277.7073 82.1668 -4.7695 231.3350 236.1045 277.8296 82.9285 -4.7576 231.5166 236.2742 277.9659 83.7808 -4.7487 231.7334 236.4821 278.1181 84.5425 -4.7387 231.9364 236.6751 278.2360 85.3648 -4.7277 232.1345 236.8622 278.3643 86.1598 -4.7206 232.3437 237.0643 278.5058 86.9515 -4.7123 232.5363 237.2485 278.6527 87.7738 -4.7012 232.7491 237.4504 278.7882 88.5655 -4.6914 232.9585 237.6499 278.9072 89.3875 -4.6864 233.1747 237.8611 279.0576 90.1795 -4.6766 233.3845 238.0612 279.1901 90.9715 -4.6673 233.5697 238.2370 279.3219 91.7935 -4.6585 233.7719 238.4303 279.4737 92.5558 -4.6505 233.9624 238.6128 279.6051 93.4085 -4.6400 234.1887 238.8287 279.7468 94.1705 -4.6318 234.3731 239.0050 279.8955 94.9920 -4.6235 234.5856 239.2092 280.0402 95.8610 -4.6171 234.8205 239.4376 280.1816 96.7655 -4.6081 235.0608 239.6690 280.3236 97.6175 -4.5973 235.2586 239.8559 280.4730 98.3795 -4.5906 235.4532 240.0438 280.6294 99.2015 -4.5801 235.6396 240.2197 280.7637 100.0235 -4.5732 235.8440 240.4172 280.9255 100.7855 -4.5673 236.0200 240.5873 281.0559 101.6373 -4.5609 236.2562 240.8171 281.1995 102.3995 -4.5507 236.4517 241.0025 281.3281 103.2220 -4.5429 236.6502 241.1931 281.4674 104.0145 -4.5365 236.8623 241.3988 281.5954 104.8053 -4.5277 237.0359 241.5636 281.7320 105.6270 -4.5220 237.2549 241.7768 281.8668 106.4190 -4.5138 237.4491 241.9628 282.0093 107.2408 -4.5027 237.6481 242.1508 282.1656 108.0330 -4.4959 237.8373 242.3332 282.3073 108.8245 -4.4881 238.0235 242.5116 282.4387 109.6485 -4.4804 238.2196 242.7000 282.5777 110.4110 -4.4735 238.4202 242.8936 282.7114 111.2628 -4.4643 238.6388 243.1030 282.8669 112.0548 -4.4579 238.8201 243.2779 283.0130 112.8465 -4.4487 239.0073 243.4559 283.1337 113.6688 -4.4428 239.2315 243.6743 283.2890 114.4305 -4.4390 239.4087 243.8477 283.4351 115.2828 -4.4290 239.5966 244.0257 283.5844 116.0445 -4.4231 239.7943 244.2175 283.6999 117.0668 -4.4113 240.0337 244.4450 283.9124 117.8885 -4.4035 240.2345 244.6380 284.0417 118.6505 -4.3986 240.4458 244.8444 284.1686 119.5025 -4.3896 240.6593 245.0490 284.3355 120.2393 -4.3848 240.8119 245.1968 284.4516 121.0948 -4.3768 241.0547 245.4315 284.5863 121.8895 -4.3707 241.2238 245.5945 284.7333 122.6815 -4.3641 241.4111 245.7752 284.8822 123.5035 -4.3558 241.5996 245.9553 285.0333 124.2655 -4.3498 241.7953 246.1450 285.1733 125.1175 -4.3451 242.0081 246.3532 285.3236 125.8795 -4.3390 242.1746 246.5136 285.4469 126.7015 -4.3293 242.3731 246.7024 285.6106 127.4935 -4.3244 242.5639 246.8883 285.7469 128.2855 -4.3163 242.7383 247.0546 285.8768 129.1085 -4.3094 242.9369 247.2463 286.0132 129.9005 -4.3030 243.1391 247.4421 286.1431 130.7225 -4.2984 243.3398 247.6381 286.2940 131.4893 -4.2909 243.5211 247.8119 286.4311 132.3130 -4.2832 243.7047 247.9879 286.5815 133.1353 -4.2772 243.8813 248.1585 286.7136 133.8968 -4.2710 244.0677 248.3387 286.8356 134.7490 -4.2648 244.2725 248.5372 286.9570 135.5113 -4.2559 244.4641 248.7200 287.0866 136.4233 -4.2480 244.6697 248.9177 287.2352 137.2288 -4.2431 244.8414 249.0845 287.3556 138.0028 -4.2388 245.0138 249.2525 287.4784 138.8248 -4.2353 245.2185 249.4538 287.5885 139.6168 -4.2290 245.4056 249.6346 287.7176 140.4085 -4.2239 245.5844 249.8084 287.8464 141.2308 -4.2198 245.7907 250.0105 287.9660 141.9925 -4.2126 245.9624 250.1750 288.0751 142.8453 -4.2045 246.1724 250.3769 288.2129 143.6375 -4.1981 246.3585 250.5566 288.3250 144.4295 -4.1939 246.5445 250.7384 288.4503 145.2533 -4.1874 246.7326 250.9200 288.5617 146.0165 -4.1811 246.9043 251.0854 288.6803 146.8698 -4.1762 247.1094 251.2856 288.8038 147.6630 -4.1713 247.2946 251.4660 288.9319 148.4555 -4.1644 247.4878 251.6522 289.0543 149.2475 -4.1553 247.6567 251.8120 289.1595 150.0695 -4.1479 247.8367 251.9846 289.2978 150.8338 -4.1435 248.0205 252.1640 289.4248 151.6875 -4.1376 248.2129 252.3505 289.5486 152.4495 -4.1313 248.3846 252.5158 289.6684 153.2715 -4.1273 248.5808 252.7081 289.7849 154.0635 -4.1214 248.7642 252.8856 289.9219 154.8555 -4.1159 248.9368 253.0527 290.0597 155.7075 -4.1132 249.1278 253.2410 290.1846 156.4690 -4.1067 249.3170 253.4237 290.3062 157.3068 -4.1003 249.5006 253.6010 290.4516 158.0875 -4.0924 249.6558 253.7482 290.5831 158.8803 -4.0881 249.8298 253.9179 290.7046 159.6718 -4.0802 250.0100 254.0902 290.8392 160.5240 -4.0768 250.2234 254.3002 290.9676 161.3453 -4.0717 250.4205 254.4922 291.1113 162.1070 -4.0673 250.6043 254.6716 291.2317 162.9590 -4.0582 250.7614 254.8195 291.3817 163.7205 -4.0530 250.9569 255.0099 291.4968 164.5428 -4.0458 251.1456 255.1915 291.6493 165.3348 -4.0392 251.3059 255.3451 291.7673 166.1268 -4.0344 251.4701 255.5044 291.8965 166.9788 -4.0315 251.6787 255.7102 292.0636 167.7440 -4.0268 251.8467 255.8736 292.1819 168.5410 -4.0213 252.0239 256.0451 292.3243 169.3648 -4.0169 252.2078 256.2248 292.4626 170.1570 -4.0135 252.3941 256.4076 292.5987 170.9485 -4.0082 252.5521 256.5603 292.7305 171.7705 -4.0003 252.7212 256.7215 292.8768 172.5625 -3.9944 252.9051 256.8995 293.0066 173.4158 -3.9923 253.1125 257.1048 293.1536 174.2388 -3.9823 253.3053 257.2875 293.2858 175.0305 -3.9797 253.4877 257.4675 293.4399 175.8225 -3.9768 253.6406 257.6175 293.5740 176.6445 -3.9729 253.8268 257.7997 293.7221 177.4065 -3.9680 253.9949 257.9629 293.8501 178.2585 -3.9607 254.1815 258.1422 294.0113 179.0505 -3.9561 254.3525 258.3086 294.1300 179.8425 -3.9529 254.5258 258.4787 294.2631 180.6710 -3.9461 254.7014 258.6475 294.4078 181.4335 -3.9419 254.8803 258.8222 294.5449 182.2855 -3.9381 255.0574 258.9956 294.6820 183.0475 -3.9319 255.2257 259.1576 294.7954 183.8695 -3.9269 255.4112 259.3381 294.9397 184.6615 -3.9231 255.5890 259.5120 295.0736 185.4523 -3.9161 255.7659 259.6820 295.2232 186.2760 -3.9128 255.9407 259.8535 295.3676 187.0678 -3.9094 256.1137 260.0231 295.4974 187.8910 -3.9064 256.3118 260.2182 295.6430 188.6868 -3.9018 256.4802 260.3820 295.7774 189.4785 -3.9000 256.6395 260.5394 295.9067 190.3050 -3.8973 256.8366 260.7340 296.0404 191.0665 -3.8950 256.9944 260.8894 296.1668 191.9223 -3.8855 257.1761 261.0616 296.3131 192.6835 -3.8835 257.3357 261.2191 296.4518 193.5058 -3.8748 257.5170 261.3918 296.5968 194.3005 -3.8725 257.6873 261.5598 296.7300 195.0940 -3.8696 257.8633 261.7329 296.8581 195.9155 -3.8645 258.0372 261.9017 296.9934 196.6775 -3.8603 258.2078 262.0681 297.1231 197.5295 -3.8574 258.3980 262.2554 297.2772 198.2740 -3.8542 258.5391 262.3933 297.4006 199.1325 -3.8509 258.7297 262.5806 297.5464 199.8945 -3.8473 258.8843 262.7316 297.6591 200.7465 -3.8445 259.0795 262.9240 297.7964 201.5085 -3.8395 259.2295 263.0690 297.9230 202.3308 -3.8345 259.4109 263.2454 298.0750 203.1225 -3.8298 259.5844 263.4143 298.1935 203.9145 -3.8267 259.7410 263.5677 298.3235 204.7365 -3.8222 259.9420 263.7642 298.4627 205.5275 -3.8198 260.1203 263.9401 298.6015 206.3495 -3.8141 260.2938 264.1079 298.7335 207.1415 -3.8127 260.4712 264.2839 298.8669 207.9335 -3.8069 260.6265 264.4335 299.0098 208.7555 -3.8013 260.7773 264.5786 299.1520 209.5175 -3.7992 260.9442 264.7433 299.2617 210.3695 -3.7983 261.1426 264.9409 299.4000 211.1325 -3.7954 261.2955 265.0909 299.5232 211.9545 -3.7898 261.4665 265.2563 299.6723 212.7795 -3.7867 261.6419 265.4285 299.8080 213.6323 -3.7815 261.8267 265.6082 299.9619 214.3943 -3.7792 261.9969 265.7761 300.0830 215.2460 -3.7746 262.1693 265.9439 300.1966 216.0085 -3.7697 262.3388 266.1085 300.3309 216.8300 -3.7671 262.4999 266.2670 300.4808 217.6220 -3.7641 262.6731 266.4372 300.6061 218.4135 -3.7586 262.8456 266.6042 300.7374 219.2663 -3.7577 263.0234 266.7812 300.8791 220.0275 -3.7546 263.1633 266.9178 301.0138 220.8498 -3.7526 263.3361 267.0887 301.1398 221.6415 -3.7475 263.4949 267.2424 301.2767 222.4335 -3.7445 263.6701 267.4146 301.4115 223.2555 -3.7402 263.8561 267.5963 301.5252 224.0475 -3.7364 264.0302 267.7666 301.6569 224.8695 -3.7349 264.1973 267.9322 301.7906 225.6615 -3.7326 264.3494 268.0820 301.9215 226.4528 -3.7311 264.5005 268.2316 302.0563 227.2745 -3.7280 264.6902 268.4182 302.1961 228.0365 -3.7262 264.8582 268.5844 302.3164 228.8898 -3.7219 265.0404 268.7623 302.4667 229.6808 -3.7188 265.1844 268.9031 302.5960 230.4725 -3.7133 265.3631 269.0764 302.7195 231.2945 -3.7110 265.5211 269.2321 302.8484 232.0565 -3.7114 265.6961 269.4074 302.9675 232.9085 -3.7087 265.8610 269.5696 303.0795 233.6710 -3.7052 266.0117 269.7170 303.2134 234.4945 -3.7049 266.1850 269.8898 303.3399 235.2883 -3.7009 266.3555 270.0563 303.4700 236.0848 -3.6986 266.5081 270.2067 303.6092 236.9095 -3.6930 266.6914 270.3844 303.7391 237.6755 -3.6893 266.8600 270.5493 303.8538 238.5065 -3.6866 267.0211 270.7076 303.9779 239.3765 -3.6868 267.2149 270.9017 304.1135 240.2105 -3.6824 267.3697 271.0521 304.2344 241.0018 -3.6784 267.5202 271.1985 304.3500 241.8250 -3.6766 267.7132 271.3897 304.4855 242.6170 -3.6746 267.8888 271.5634 304.6109 243.4388 -3.6695 268.0375 271.7070 304.7386 244.2310 -3.6682 268.1971 271.8653 304.8603 245.0225 -3.6658 268.3585 272.0243 304.9704 245.8450 -3.6628 268.5346 272.1974 305.0944 246.6065 -3.6607 268.6808 272.3415 305.2153 247.4588 -3.6576 268.8750 272.5326 305.3305 248.2205 -3.6533 269.0181 272.6713 305.4615 249.0428 -3.6518 269.1907 272.8425 305.5942 249.8350 -3.6500 269.3303 272.9803 305.7122 250.6265 -3.6498 269.4921 273.1419 305.8280 251.4788 -3.6491 269.6799 273.3290 305.9632 252.2405 -3.6462 269.8319 273.4781 306.0812 253.0628 -3.6405 269.9915 273.6320 306.2331 253.8545 -3.6381 270.1515 273.7897 306.3759 254.6465 -3.6370 270.3048 273.9418 306.5023 255.4685 -3.6331 270.4754 274.1086 306.6312 256.2605 -3.6311 270.6509 274.2820 306.7593 257.0850 -3.6276 270.8288 274.4564 306.9069 257.8775 -3.6245 270.9891 274.6136 307.0446 258.6695 -3.6218 271.1512 274.7730 307.1842 259.4915 -3.6182 271.3050 274.9232 307.3145 260.3043 -3.6166 271.4691 275.0857 307.4454 261.0665 -3.6168 271.6046 275.2214 307.5679 261.8885 -3.6123 271.7708 275.3830 307.7153 262.7105 -3.6094 271.9487 275.5582 307.8628 263.4725 -3.6073 272.0901 275.6974 307.9887 264.3245 -3.6057 272.2670 275.8727 308.1499 265.0865 -3.6056 272.4178 276.0234 308.2987 265.9085 -3.6034 272.5874 276.1907 308.4255 266.7005 -3.6023 272.7605 276.3628 308.5751 267.4923 -3.6002 272.9201 276.5203 308.7187 268.3450 -3.5985 273.0890 276.6875 308.8645 269.1073 -3.5960 273.2530 276.8490 308.9784 269.9483 -3.5937 273.4082 277.0018 309.1390 270.7240 -3.5910 273.5532 277.1443 309.2789 271.5460 -3.5875 273.7292 277.3167 309.4198 272.3075 -3.5865 273.8946 277.4811 309.5653 273.1595 -3.5847 274.0553 277.6400 309.7183 273.9210 -3.5859 274.1879 277.7738 309.8554 274.7430 -3.5828 274.3505 277.9333 309.9864 275.5650 -3.5786 274.5254 278.1040 310.1396 276.3265 -3.5768 274.6754 278.2522 310.2758 277.1788 -3.5734 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