DTA measure 1gyors-futes Test Date: 2024227:1459 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.61 s Mass = 1.000 mg data_number = 1266 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1940 1.5469 231.8605 230.3136 265.9630 1.9310 1.5391 232.1397 230.6006 265.9706 2.7843 1.5458 232.4716 230.9258 265.8925 3.5758 1.5491 232.7047 231.1557 266.0268 4.3658 1.5565 232.9232 231.3667 266.0039 5.1855 1.5524 233.1925 231.6401 265.9923 5.9438 1.5531 233.4782 231.9250 266.0226 6.7920 1.5644 233.6322 232.0678 265.9760 7.5505 1.5613 233.9604 232.3991 266.0131 8.3708 1.5722 234.3111 232.7390 266.0870 9.1893 1.5600 234.4206 232.8606 266.0979 9.9480 1.5634 234.5744 233.0110 266.1695 10.7960 1.5771 234.7991 233.2220 266.2264 11.5850 1.5775 234.9929 233.4154 266.2496 12.3740 1.5755 235.1823 233.6068 266.2725 13.1928 1.5644 235.4155 233.8511 266.3176 13.9828 1.5548 235.5873 234.0325 266.4985 14.8030 1.5555 235.8822 234.3267 266.6128 15.5935 1.5532 236.0246 234.4714 266.6990 16.3855 1.5586 236.2198 234.6613 266.7549 17.2075 1.5591 236.5862 235.0271 266.8534 17.9995 1.5599 236.8212 235.2613 267.0270 18.8215 1.5489 237.2344 235.6855 267.2650 19.6135 1.5517 237.4548 235.9031 267.4621 20.4053 1.5545 237.6470 236.0925 267.5677 21.2273 1.5512 237.7730 236.2218 267.6218 22.0190 1.5545 237.9756 236.4210 267.8097 22.8413 1.5481 238.1707 236.6225 267.9837 23.6330 1.5377 238.3872 236.8495 268.2033 24.4245 1.5356 238.6010 237.0654 268.4398 25.2470 1.5300 238.7905 237.2606 268.5832 26.0385 1.5319 238.8918 237.3599 268.7802 26.8608 1.5385 239.0677 237.5291 268.8363 27.6528 1.5385 239.3329 237.7944 268.9991 28.4455 1.5158 239.5788 238.0629 269.2354 29.2680 1.5105 239.8124 238.3019 269.4545 30.0595 1.5129 240.0181 238.5052 269.6052 30.8818 1.5188 240.2141 238.6953 269.6824 31.6533 1.5021 240.3987 238.8966 269.8613 32.4848 1.5075 240.6307 239.1232 270.0462 33.2768 1.4954 240.8467 239.3514 270.1520 34.0685 1.4952 240.9913 239.4961 270.3084 34.9208 1.4922 241.1230 239.6308 270.3850 35.6823 1.4819 241.3465 239.8646 270.5294 36.5010 1.4756 241.5748 240.0992 270.6086 37.2890 1.4774 241.7632 240.2859 270.6704 38.0770 1.4720 241.9786 240.5067 270.8703 38.9250 1.4766 242.2365 240.7599 271.0294 39.6830 1.4626 242.4560 240.9934 271.2150 40.5020 1.4469 242.6904 241.2435 271.4377 41.2900 1.4621 242.9108 241.4488 271.6237 42.0790 1.4752 243.0551 241.5799 271.7896 42.9275 1.4514 243.2711 241.8198 272.0511 43.6860 1.4297 243.4551 242.0254 272.1541 44.5048 1.4288 243.7068 242.2780 272.3569 45.3235 1.4337 243.8591 242.4255 272.5056 46.0835 1.4271 243.9917 242.5646 272.5180 46.9345 1.4268 244.3316 242.9047 272.6305 47.6955 1.3971 244.4578 243.0607 272.7978 48.5175 1.3986 244.7466 243.3480 272.9333 49.3398 1.4036 244.9598 243.5561 272.9614 50.1015 1.3882 245.0962 243.7080 273.0045 50.9545 1.3842 245.2711 243.8869 273.2920 51.7165 1.3906 245.6142 244.2236 273.3831 52.5593 1.3773 245.9291 244.5518 273.5289 53.3515 1.3702 246.0169 244.6467 273.7458 54.1435 1.3591 246.2255 244.8663 273.8727 54.9665 1.3485 246.4263 245.0777 274.0136 55.7285 1.3335 246.6476 245.3142 274.1264 56.5805 1.3354 246.9729 245.6374 274.2603 57.3430 1.3244 247.2228 245.8985 274.4462 58.1665 1.3198 247.4115 246.0917 274.5373 58.9885 1.3139 247.7309 246.4169 274.5982 59.7505 1.2997 247.8974 246.5977 274.8046 60.6025 1.2921 247.9999 246.7078 274.8135 61.3945 1.2968 248.0980 246.8011 274.8774 62.1873 1.2904 248.2338 246.9434 274.9344 63.0105 1.2721 248.4567 247.1847 275.1176 63.7728 1.2703 248.7245 247.4542 275.1305 64.6248 1.2620 248.9234 247.6614 275.2503 65.3873 1.2685 249.0357 247.7672 275.3443 66.2098 1.2486 249.1787 247.9300 275.4465 67.0318 1.2382 249.4255 248.1873 275.5930 67.7928 1.2344 249.5900 248.3557 275.6826 68.6428 1.2331 249.7568 248.5237 275.7958 69.4013 1.2270 249.9445 248.7175 275.9399 70.2193 1.2320 250.1975 248.9655 276.1259 71.0075 1.2193 250.3986 249.1793 276.1994 71.7953 1.2133 250.4806 249.2673 276.2893 72.6448 1.2005 250.6042 249.4037 276.4193 73.4035 1.1896 250.7791 249.5895 276.5432 74.2230 1.1655 250.9858 249.8203 276.7501 75.0420 1.1665 251.0791 249.9126 276.8783 75.8013 1.1721 251.2054 250.0333 277.0001 76.6508 1.1472 251.4186 250.2714 277.1703 77.4398 1.1340 251.5742 250.4402 277.3843 78.2308 1.1293 251.7820 250.6526 277.5395 79.0520 1.1296 251.9222 250.7926 277.7441 79.8135 1.1204 252.0681 250.9476 277.8563 80.6650 1.1178 252.3321 251.2142 278.0611 81.4270 1.0928 252.4760 251.3832 278.1626 82.2488 1.0922 252.6922 251.6000 278.3935 83.0498 1.0862 252.8676 251.7814 278.4926 83.8455 1.0889 253.1231 252.0342 278.7024 84.6680 1.0778 253.3925 252.3147 278.8304 85.4295 1.0760 253.5830 252.5070 278.8347 86.2820 1.0697 253.7124 252.6427 279.0465 87.0738 1.0531 253.9002 252.8470 279.2261 87.8655 1.0360 254.1161 253.0801 279.2700 88.6885 1.0343 254.3297 253.2954 279.4063 89.4515 1.0325 254.5557 253.5232 279.6101 90.3038 1.0091 254.7764 253.7672 279.7317 91.0958 1.0115 254.9881 253.9767 279.8893 91.8875 0.9982 255.1560 254.1577 279.9374 92.7098 0.9899 255.3376 254.3477 280.0383 93.5015 0.9872 255.5541 254.5669 280.2469 94.3235 0.9730 255.7358 254.7628 280.2992 95.1160 0.9784 255.8694 254.8910 280.3740 95.9095 0.9742 256.0034 255.0292 280.4870 96.7315 0.9624 256.1869 255.2245 280.6584 97.5235 0.9579 256.4333 255.4754 280.7329 98.3455 0.9530 256.5318 255.5788 280.8845 99.1378 0.9332 256.6076 255.6744 281.1367 99.9303 0.9207 256.7604 255.8397 281.2576 100.7520 0.9220 256.9893 256.0673 281.3159 101.5100 0.9221 257.2088 256.2867 281.4436 102.3618 0.9061 257.4134 256.5073 281.6786 103.1538 0.8915 257.6143 256.7228 281.7902 103.9538 0.8894 257.7468 256.8574 281.8314 104.7433 0.8705 257.8148 256.9442 281.9540 105.5340 0.8547 258.0443 257.1895 282.1767 106.3820 0.8574 258.2704 257.4130 282.2531 107.1400 0.8417 258.4840 257.6423 282.3597 107.9598 0.8296 258.7259 257.8964 282.4615 108.7783 0.8313 258.8379 258.0066 282.6128 109.5370 0.8341 258.9782 258.1441 282.7774 110.3880 0.8268 259.1225 258.2956 282.8411 111.1483 0.8167 259.2682 258.4515 282.8957 111.9695 0.8036 259.5178 258.7141 283.1083 112.7910 0.7892 259.7015 258.9123 283.2182 113.5525 0.7975 259.8316 259.0342 283.3590 114.4055 0.7847 259.9930 259.2083 283.5262 115.1675 0.7675 260.1638 259.3963 283.5989 115.9895 0.7688 260.3847 259.6159 283.6874 116.8115 0.7655 260.6229 259.8574 283.8336 117.5735 0.7522 260.7432 259.9910 283.9796 118.4265 0.7452 261.0351 260.2898 284.1972 119.1883 0.7348 261.2447 260.5098 284.2677 120.0103 0.7302 261.2936 260.5634 284.3698 120.8033 0.7148 261.4208 260.7061 284.4265 121.5958 0.7098 261.6360 260.9263 284.7015 122.4480 0.7075 261.7785 261.0710 284.7715 123.2095 0.6890 261.9610 261.2720 284.9115 124.0318 0.6809 262.1719 261.4910 284.9907 124.8245 0.6740 262.3541 261.6801 285.0476 125.6165 0.6671 262.4354 261.7683 285.1018 126.4688 0.6624 262.6609 261.9985 285.3011 127.2305 0.6692 262.8065 262.1373 285.4358 128.0528 0.6568 263.0437 262.3868 285.5317 128.8748 0.6432 263.2040 262.5609 285.6382 129.6365 0.6378 263.3989 262.7611 285.7508 130.4893 0.6284 263.5942 262.9658 285.8978 131.2515 0.6160 263.7153 263.0993 286.0461 132.0738 0.6176 263.8516 263.2341 286.2919 132.8953 0.6079 264.0966 263.4886 286.4449 133.6540 0.5919 264.1771 263.5852 286.5739 134.4828 0.5702 264.3645 263.7943 286.8052 135.2710 0.5760 264.5846 264.0085 286.9941 136.0890 0.5700 264.7805 264.2105 287.1686 136.8770 0.5557 264.9254 264.3697 287.3445 137.6650 0.5452 265.1511 264.6059 287.5388 138.5138 0.5300 265.2918 264.7619 287.5750 139.2723 0.5383 265.4955 264.9572 287.8151 140.0910 0.5375 265.6727 265.1352 287.9328 140.9095 0.5229 265.8540 265.3311 288.0594 141.6680 0.5091 265.9631 265.4540 288.1988 142.5168 0.5143 266.1126 265.5984 288.4904 143.3070 0.4957 266.2648 265.7691 288.6598 144.0975 0.4957 266.5045 266.0087 288.5923 144.9205 0.4901 266.6921 266.2019 288.7350 145.6825 0.4814 266.8145 266.3331 288.8626 146.5348 0.4751 266.9818 266.5068 289.0434 147.2965 0.4795 267.1607 266.6812 289.0957 148.1188 0.4654 267.3221 266.8567 289.2407 148.9405 0.4585 267.4749 267.0165 289.3979 149.7025 0.4425 267.7014 267.2589 289.5360 150.5548 0.4438 267.8622 267.4184 289.6340 151.3165 0.4337 268.0185 267.5848 289.7564 152.1385 0.4339 268.0936 267.6597 289.8945 152.9605 0.4168 268.2151 267.7984 290.0658 153.7225 0.3994 268.5220 268.1225 290.1529 154.5753 0.3964 268.7060 268.3096 290.2215 155.3375 0.3883 268.8270 268.4387 290.3453 156.1595 0.3761 269.0072 268.6311 290.5348 156.9815 0.3776 269.2493 268.8717 290.6716 157.7435 0.3766 269.3277 268.9510 290.8169 158.5973 0.3707 269.4951 269.1244 290.9178 159.3593 0.3663 269.6374 269.2711 290.9766 160.1808 0.3561 269.8210 269.4649 291.1004 161.0030 0.3511 269.9607 269.6095 291.2852 161.7645 0.3485 270.1576 269.8091 291.3788 162.6190 0.3326 270.3663 270.0337 291.5521 163.3805 0.3391 270.4858 270.1468 291.6921 164.2028 0.3306 270.6753 270.3447 291.6910 165.0230 0.3327 270.6732 270.3405 291.8134 165.7803 0.3249 270.9191 270.5942 291.9703 166.6330 0.3118 271.1970 270.8852 292.0406 167.3915 0.2940 271.2987 271.0047 292.1250 168.2113 0.2879 271.4118 271.1239 292.3408 168.9990 0.2831 271.6247 271.3416 292.5647 169.7870 0.2814 271.9105 271.6291 292.6670 170.6368 0.2729 271.9877 271.7148 292.8515 171.3953 0.2777 272.2527 271.9750 293.0078 172.2140 0.2597 272.3436 272.0839 293.0789 173.0328 0.2584 272.6135 272.3551 293.1986 173.7910 0.2540 272.7842 272.5302 293.2927 174.6408 0.2531 272.8588 272.6057 293.4867 175.4300 0.2419 273.1459 272.9039 293.6786 176.2200 0.2413 273.2752 273.0339 293.8575 177.0430 0.2242 273.4589 273.2347 293.8262 177.8053 0.2170 273.6164 273.3995 293.9597 178.6570 0.2094 273.8166 273.6072 294.1692 179.4488 0.2034 274.0068 273.8034 294.2181 180.2405 0.2051 274.1301 273.9250 294.2471 181.0628 0.1951 274.3792 274.1841 294.3814 181.8245 0.1939 274.5495 274.3556 294.6721 182.6780 0.1800 274.7486 274.5687 294.8179 183.4405 0.1789 274.9507 274.7717 294.9048 184.2628 0.1676 275.1684 275.0007 295.0249 185.0848 0.1617 275.2356 275.0739 295.1312 185.8465 0.1456 275.2478 275.1022 295.3256 186.6988 0.1499 275.4349 275.2850 295.4451 187.4605 0.1250 275.5395 275.4144 295.6166 188.2828 0.1132 275.7127 275.5995 295.7262 189.1048 0.1109 275.8888 275.7778 295.8670 189.8665 0.1182 276.0230 275.9047 295.9569 190.7193 0.1061 276.2158 276.1097 296.0839 191.4815 0.0955 276.3299 276.2344 296.1802 192.3050 0.0786 276.5637 276.4851 296.3543 193.0985 0.0865 276.6347 276.5482 296.5091 193.8915 0.0806 276.8717 276.7912 296.6541 194.7435 0.0701 276.9960 276.9259 296.7376 195.5055 0.0704 277.0403 276.9699 296.9601 196.3285 0.0514 277.2858 277.2345 296.9936 197.1453 0.0679 277.4247 277.3568 297.1849 197.9038 0.0562 277.6496 277.5934 297.3247 198.7520 0.0519 277.8712 277.8193 297.4310 199.5098 0.0430 277.9783 277.9354 297.5868 200.3280 0.0324 278.1239 278.0915 297.7116 201.1460 0.0310 278.2703 278.2393 297.8905 201.9048 0.0191 278.3582 278.3391 297.9932 202.7568 0.0108 278.5622 278.5514 298.0242 203.5150 0.0096 278.7854 278.7759 298.2099 204.3338 -0.0011 278.8535 278.8545 298.3497 205.1523 -0.0028 279.0707 279.0735 298.4498 205.9110 -0.0117 279.1819 279.1935 298.5768 206.7595 -0.0214 279.3775 279.3989 298.7551 207.5488 -0.0274 279.4912 279.5186 298.9641 208.3405 -0.0393 279.6773 279.7167 299.0492 209.1625 -0.0425 279.8230 279.8654 299.1718 209.9255 -0.0376 279.8393 279.8769 299.3746 210.7775 -0.0429 280.0320 280.0749 299.4571 211.5398 -0.0550 280.2618 280.3168 299.6073 212.3625 -0.0709 280.3993 280.4702 299.7145 213.1845 -0.0698 280.5627 280.6326 299.8953 213.9465 -0.0667 280.7399 280.8066 300.0927 214.7985 -0.0734 280.9219 280.9953 300.1281 215.5605 -0.0841 280.9551 281.0392 300.1935 216.3823 -0.0918 281.1943 281.2861 300.3518 217.2043 -0.1034 281.2872 281.3906 300.5440 217.9660 -0.1035 281.4458 281.5493 300.6571 218.8195 -0.1108 281.6072 281.7180 300.7879 219.5820 -0.1201 281.8101 281.9303 300.8376 220.4038 -0.1190 281.9537 282.0727 301.0517 221.2260 -0.1222 282.0377 282.1599 301.2124 221.9875 -0.1275 282.2237 282.3512 301.3813 222.8405 -0.1369 282.4354 282.5723 301.4810 223.6025 -0.1431 282.5734 282.7166 301.5877 224.4248 -0.1549 282.6479 282.8028 301.7377 225.2468 -0.1578 282.8743 283.0321 301.8793 226.0098 -0.1687 282.9742 283.1429 302.0722 226.8648 -0.1747 283.1520 283.3268 302.0965 227.6265 -0.1621 283.4006 283.5627 302.1999 228.4488 -0.1754 283.4897 283.6651 302.3363 229.2705 -0.1777 283.6466 283.8243 302.4971 230.0310 -0.1938 283.7949 283.9887 302.6345 230.8810 -0.2071 283.9882 284.1953 302.8185 231.6390 -0.2069 284.1318 284.3388 302.9756 232.4610 -0.1905 284.2867 284.4771 303.0862 233.2493 -0.2004 284.4622 284.6626 303.1007 234.0380 -0.2212 284.5566 284.7779 303.2245 234.8580 -0.2317 284.6927 284.9243 303.4417 235.6470 -0.2426 284.8222 285.0648 303.5177 236.4660 -0.2475 285.0148 285.2624 303.5781 237.2543 -0.2432 285.0928 285.3360 303.6515 238.0430 -0.2517 285.2692 285.5209 303.8425 238.8918 -0.2590 285.4169 285.6759 304.0024 239.6500 -0.2579 285.4956 285.7535 304.1442 240.4700 -0.2600 285.6711 285.9311 304.2595 241.2908 -0.2814 285.8733 286.1546 304.3753 242.0505 -0.2835 285.9609 286.2444 304.4788 242.9015 -0.2883 286.0766 286.3649 304.5609 243.6635 -0.2949 286.2071 286.5020 304.7481 244.4855 -0.3236 286.3831 286.7067 304.9123 245.2835 -0.3258 286.5124 286.8383 304.9782 246.0755 -0.3266 286.7307 287.0573 305.1296 246.8870 -0.3341 286.8955 287.2296 305.2988 247.6865 -0.3423 287.0905 287.4328 305.3882 248.5085 -0.3513 287.2464 287.5977 305.4795 249.2705 -0.3417 287.4457 287.7875 305.6372 250.1235 -0.3599 287.5476 287.9075 305.7885 250.9155 -0.3715 287.7530 288.1244 305.8813 251.7075 -0.3793 287.9046 288.2839 306.0567 252.5300 -0.3905 288.0563 288.4468 306.1890 253.2925 -0.3879 288.3070 288.6950 306.3104 254.1445 -0.4035 288.4839 288.8875 306.4707 254.9365 -0.4096 288.6117 289.0213 306.6577 255.7285 -0.4135 288.6808 289.0943 306.7600 256.5513 -0.4048 288.8607 289.2655 306.9457 257.3128 -0.4011 289.0832 289.4843 307.0897 258.1670 -0.4214 289.2001 289.6215 307.3022 258.9590 -0.4214 289.3582 289.7795 307.4446 259.7505 -0.4220 289.4492 289.8712 307.5902 260.5728 -0.4294 289.6451 290.0745 307.7099 261.3645 -0.4135 289.8382 290.2518 307.9120 262.1843 -0.4341 290.0903 290.5244 308.0930 262.9723 -0.4373 290.2270 290.6643 308.2119 263.7605 -0.4352 290.3463 290.7815 308.3040 264.5785 -0.4372 290.5263 290.9635 308.4329 265.3365 -0.4472 290.6450 291.0922 308.5020 266.1868 -0.4572 290.9663 291.4235 308.6753 266.9753 -0.4648 291.1294 291.5942 308.8757 267.7638 -0.4602 291.2200 291.6802 308.9428 268.5823 -0.4641 291.2715 291.7356 309.0642 269.3708 -0.4717 291.4012 291.8728 309.2133 270.1898 -0.4792 291.5413 292.0205 309.3396 270.9780 -0.4809 291.7362 292.2171 309.4214 271.7700 -0.4905 291.9334 292.4239 309.5941 272.5933 -0.4905 292.0320 292.5224 309.7238 273.3848 -0.4924 292.1291 292.6215 309.7911 274.2058 -0.5004 292.2386 292.7390 309.9450 274.9980 -0.5139 292.4864 293.0003 310.0719 275.7890 -0.5203 292.6216 293.1419 310.1393 276.6108 -0.5210 292.7862 293.3072 310.3463 277.4025 -0.5131 292.8783 293.3915 310.5196 278.2248 -0.5239 293.1370 293.6608 310.6681 279.0168 -0.5365 293.3002 293.8368 310.6928 279.8085 -0.5527 293.4635 294.0162 310.8404 280.6308 -0.5534 293.5974 294.1509 311.0161 281.3925 -0.5486 293.7216 294.2702 311.0547 282.2463 -0.5541 293.8316 294.3857 311.1650 283.0388 -0.5470 294.0392 294.5862 311.3104 283.8305 -0.5563 294.1736 294.7299 311.4649 284.6538 -0.5749 294.2387 294.8136 311.5307 285.4155 -0.5829 294.4989 295.0819 311.7555 286.2678 -0.5882 294.6659 295.2541 311.8737 287.0598 -0.5841 294.7786 295.3627 311.9672 287.8515 -0.6007 294.9397 295.5404 312.0973 288.6735 -0.6047 295.0464 295.6511 312.2286 289.4655 -0.6052 295.1648 295.7700 312.3378 290.2875 -0.6044 295.3721 295.9765 312.4488 291.0798 -0.6181 295.4961 296.1142 312.5718 291.8725 -0.6136 295.6476 296.2613 312.7002 292.6945 -0.6173 295.8329 296.4502 312.8326 293.4865 -0.6219 295.9362 296.5581 312.9623 294.3053 -0.6229 296.1136 296.7365 313.0939 295.0933 -0.6296 296.2413 296.8709 313.2489 295.8820 -0.6377 296.4593 297.0970 313.4619 296.7000 -0.6411 296.5719 297.2130 313.5517 297.4880 -0.6413 296.6364 297.2777 313.6533 298.3060 -0.6556 296.8246 297.4802 313.8339 299.0943 -0.6563 297.0319 297.6882 313.9471 299.8830 -0.6752 297.1456 297.8208 314.0802 300.7018 -0.6721 297.3618 298.0338 314.2804 301.4910 -0.6814 297.5669 298.2483 314.3963 302.3100 -0.6735 297.7183 298.3918 314.5421 303.0980 -0.6866 297.8157 298.5023 314.6687 303.8878 -0.6864 297.9310 298.6174 314.7306 304.7385 -0.6964 298.0550 298.7514 314.8457 305.4995 -0.7017 298.2325 298.9343 314.9936 306.3200 -0.7054 298.4455 299.1509 315.1189 307.1120 -0.7268 298.6794 299.4062 315.2922 307.9045 -0.7328 298.8029 299.5357 315.4160 308.7588 -0.7250 298.8651 299.5901 315.5239 309.5215 -0.7196 299.0198 299.7393 315.6686 310.3435 -0.7236 299.1923 299.9159 315.8259 311.1355 -0.7179 299.2890 300.0069 315.9013 311.9275 -0.7178 299.4866 300.2044 316.0071 312.7505 -0.7307 299.5720 300.3027 316.0813 313.5425 -0.7394 299.7252 300.4646 316.2589 314.3645 -0.7461 299.8661 300.6121 316.4534 315.1585 -0.7497 300.0110 300.7607 316.6176 315.9518 -0.7571 300.1370 300.8942 316.7914 316.7740 -0.7726 300.3977 301.1703 316.9614 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