DTA measure 12_olom Date: 202436:1425 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1273.93 s Mass = 1138.400 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2518 -0.8316 248.4864 249.3180 266.3786 2.0445 -0.8255 248.6207 249.4462 266.3878 2.8668 -0.8217 248.7712 249.5929 266.4274 3.6585 -0.8156 248.9065 249.7221 266.4275 4.4808 -0.8025 249.0393 249.8418 266.4400 5.2728 -0.7990 249.1804 249.9794 266.4649 6.0645 -0.8019 249.3106 250.1125 266.4726 6.8868 -0.8017 249.4620 250.2637 266.4883 7.6785 -0.7986 249.5983 250.3969 266.5050 8.5008 -0.7909 249.7421 250.5330 266.5598 9.2925 -0.7906 249.8810 250.6716 266.5878 10.0845 -0.7861 250.0223 250.8084 266.6297 10.9370 -0.7828 250.1473 250.9301 266.6582 11.6995 -0.7796 250.2785 251.0581 266.7056 12.5200 -0.7739 250.4171 251.1911 266.7788 13.3078 -0.7691 250.5511 251.3203 266.8377 14.0948 -0.7679 250.7050 251.4728 266.8958 14.9130 -0.7640 250.8373 251.6013 266.9733 15.7010 -0.7623 250.9727 251.7350 267.0534 16.5193 -0.7598 251.1110 251.8709 267.1535 17.3080 -0.7557 251.2503 252.0061 267.2250 18.0960 -0.7539 251.3821 252.1360 267.3104 18.9448 -0.7742 251.5159 252.2901 267.4277 19.7043 -0.7795 251.6403 252.4198 267.5265 20.5238 -0.7718 251.7711 252.5430 267.6342 21.3128 -0.7540 251.9053 252.6593 267.7474 22.1020 -0.7392 252.0289 252.7681 267.8666 22.9515 -0.7339 252.1889 252.9228 267.9992 23.7135 -0.7322 252.3061 253.0384 268.1266 24.5358 -0.7311 252.4367 253.1678 268.2389 25.3275 -0.7295 252.5606 253.2901 268.3540 26.1195 -0.7253 252.6879 253.4132 268.4754 26.9443 -0.7223 252.8342 253.5565 268.6182 27.7065 -0.7222 252.9646 253.6868 268.7530 28.5585 -0.7202 253.1069 253.8271 268.9073 29.3505 -0.7185 253.2435 253.9620 269.0438 30.1425 -0.7158 253.3821 254.0979 269.1721 30.9645 -0.7194 253.5221 254.2415 269.3141 31.7265 -0.7159 253.6436 254.3595 269.4434 32.5785 -0.7127 253.7578 254.4705 269.5862 33.3705 -0.7120 253.8877 254.5997 269.7039 34.1625 -0.7134 254.0209 254.7343 269.8338 34.9845 -0.7114 254.1533 254.8648 269.9549 35.7520 -0.7108 254.2882 254.9990 270.0714 36.6045 -0.7093 254.4337 255.1429 270.2014 37.3665 -0.7108 254.5595 255.2702 270.3049 38.1878 -0.7084 254.6910 255.3993 270.4206 39.0105 -0.7086 254.8165 255.5250 270.5438 39.7725 -0.7071 254.9493 255.6564 270.6494 40.6248 -0.7048 255.0884 255.7932 270.7561 41.3865 -0.7065 255.2080 255.9145 270.8685 42.2088 -0.7037 255.3499 256.0536 270.9853 43.0310 -0.6971 255.4765 256.1737 271.0805 43.7925 -0.6969 255.5947 256.2916 271.1535 44.6453 -0.7145 255.7397 256.4542 271.2550 45.4060 -0.7254 255.8659 256.5914 271.3646 46.2240 -0.7314 256.0279 256.7593 271.4590 47.0420 -0.7312 256.1308 256.8620 271.5677 47.8000 -0.7302 256.2581 256.9883 271.6566 48.6480 -0.7312 256.3958 257.1270 271.7434 49.4060 -0.7278 256.5127 257.2405 271.8313 50.2240 -0.7276 256.6481 257.3757 271.9416 51.0420 -0.7224 256.7845 257.5069 272.0201 51.8000 -0.7172 256.8979 257.6151 272.1081 52.6485 -0.7119 257.0249 257.7368 272.2158 53.4373 -0.7120 257.1542 257.8662 272.3259 54.2273 -0.7098 257.2806 257.9904 272.4143 55.0480 -0.7165 257.4398 258.1563 272.4934 55.8095 -0.7179 257.5526 258.2705 272.5758 56.6618 -0.7138 257.6811 258.3949 272.6889 57.4235 -0.7208 257.7938 258.5146 272.7751 58.2458 -0.7187 257.9188 258.6375 272.8816 59.0678 -0.7113 258.0502 258.7615 272.9992 59.8295 -0.7137 258.1690 258.8828 273.0797 60.6818 -0.7188 258.3211 259.0399 273.1778 61.4435 -0.7192 258.4378 259.1570 273.2822 62.2658 -0.7218 258.5724 259.2941 273.3900 63.0610 -0.7205 258.7059 259.4264 273.5064 63.8535 -0.7195 258.8175 259.5369 273.6140 64.7058 -0.7203 258.9592 259.6795 273.7188 65.4675 -0.7226 259.0888 259.8114 273.8230 66.2898 -0.7220 259.2095 259.9315 273.9488 67.0820 -0.7235 259.3405 260.0640 274.0496 67.8755 -0.7299 259.4669 260.1969 274.1586 68.7278 -0.7316 259.6055 260.3371 274.2848 69.4895 -0.7322 259.7366 260.4688 274.3967 70.3115 -0.7251 259.8637 260.5887 274.5186 71.1058 -0.7249 259.9641 260.6890 274.6316 71.8995 -0.7256 260.0873 260.8130 274.7262 72.7515 -0.7257 260.2182 260.9439 274.8471 73.5148 -0.7261 260.3399 261.0660 274.9652 74.3415 -0.7222 260.4822 261.2045 275.0791 75.1335 -0.7250 260.6042 261.3292 275.1847 75.9255 -0.7263 260.7286 261.4548 275.2854 76.7773 -0.7356 260.8664 261.6020 275.4102 77.5363 -0.7375 260.9775 261.7151 275.5212 78.3535 -0.7268 261.1033 261.8301 275.6608 79.1413 -0.7167 261.2237 261.9404 275.7325 79.9293 -0.7142 261.3523 262.0665 275.8503 80.7478 -0.7151 261.4823 262.1974 275.9619 81.5368 -0.7161 261.6118 262.3279 276.0597 82.3568 -0.7181 261.7318 262.4498 276.1729 83.1450 -0.7222 261.8593 262.5815 276.2803 83.9348 -0.7231 261.9934 262.7165 276.3902 84.7838 -0.7142 262.1313 262.8454 276.5045 85.5453 -0.7138 262.2464 262.9601 276.6110 86.3665 -0.7175 262.3713 263.0888 276.7289 87.1585 -0.7220 262.4955 263.2175 276.8388 87.9505 -0.7208 262.6151 263.3359 276.9412 88.8025 -0.7228 262.7364 263.4592 277.0495 89.5645 -0.7206 262.8722 263.5927 277.1497 90.3865 -0.7213 262.9961 263.7174 277.2661 91.1785 -0.7198 263.1166 263.8364 277.3697 91.9705 -0.7200 263.2330 263.9531 277.4816 92.8225 -0.7204 263.3474 264.0679 277.5934 93.5845 -0.7219 263.4863 264.2082 277.6902 94.4063 -0.7252 263.6146 264.3398 277.8140 95.1985 -0.7276 263.7467 264.4742 277.9051 95.9903 -0.7252 263.8723 264.5975 278.0031 96.8430 -0.7294 263.9902 264.7196 278.1230 97.6048 -0.7332 264.1098 264.8430 278.2313 98.4275 -0.7331 264.2449 264.9779 278.3399 99.2200 -0.7327 264.3563 265.0890 278.4438 100.0115 -0.7356 264.4907 265.2263 278.5778 100.8340 -0.7372 264.6126 265.3499 278.6831 101.6255 -0.7386 264.7249 265.4635 278.7825 102.4485 -0.7397 264.8551 265.5948 278.8937 103.2408 -0.7404 264.9983 265.7387 278.9998 104.0335 -0.7424 265.1117 265.8542 279.1143 104.8558 -0.7467 265.2239 265.9706 279.2091 105.6475 -0.7482 265.3545 266.1027 279.3242 106.4705 -0.7513 265.4801 266.2314 279.4292 107.2628 -0.7523 265.6012 266.3535 279.5295 108.0545 -0.7532 265.7351 266.4884 279.6296 108.8765 -0.7535 265.8537 266.6072 279.7432 109.6660 -0.7559 265.9685 266.7244 279.8579 110.4840 -0.7634 266.0919 266.8553 279.9793 111.2720 -0.7668 266.2104 266.9771 280.0833 112.0600 -0.7699 266.3250 267.0949 280.1688 112.8788 -0.7761 266.4686 267.2447 280.2700 113.6970 -0.7764 266.5898 267.3662 280.3723 114.4858 -0.7814 266.7185 267.4999 280.4614 115.3043 -0.7824 266.8307 267.6130 280.5836 116.0635 -0.7908 266.9345 267.7253 280.6908 116.9138 -0.7941 267.0718 267.8659 280.7963 117.6753 -0.7961 267.2052 268.0013 280.8931 118.4968 -0.7972 267.3161 268.1133 281.0088 119.3180 -0.7950 267.4451 268.2400 281.1188 120.0785 -0.7951 267.5612 268.3563 281.2237 120.9308 -0.7954 267.6874 268.4829 281.3390 121.6925 -0.7979 267.7994 268.5973 281.4251 122.5145 -0.7971 267.9183 268.7154 281.5306 123.3365 -0.8012 268.0538 268.8550 281.6318 124.0985 -0.8038 268.1856 268.9894 281.7368 124.9508 -0.8057 268.3167 269.1224 281.8461 125.7125 -0.8049 268.4185 269.2234 281.9421 126.5345 -0.8080 268.5515 269.3596 282.0390 127.3265 -0.8110 268.6704 269.4814 282.1422 128.1185 -0.8139 268.7805 269.5945 282.2458 128.9705 -0.8155 268.9160 269.7315 282.3533 129.7325 -0.8173 269.0385 269.8558 282.4512 130.5545 -0.8170 269.1711 269.9881 282.5436 131.3465 -0.8228 269.2862 270.1090 282.6545 132.1385 -0.8246 269.3896 270.2142 282.7401 132.9905 -0.8223 269.5255 270.3478 282.8526 133.7525 -0.8244 269.6461 270.4705 282.9372 134.5745 -0.8251 269.7610 270.5861 283.0328 135.3663 -0.8268 269.8930 270.7197 283.1436 136.1578 -0.8299 270.0291 270.8589 283.2393 137.0098 -0.8315 270.1411 270.9727 283.3352 137.7718 -0.8367 270.2547 271.0914 283.4345 138.5938 -0.8328 270.3643 271.1971 283.5449 139.3860 -0.8281 270.4998 271.3279 283.6497 140.1775 -0.8279 270.6371 271.4650 283.7426 141.0300 -0.8320 270.7356 271.5677 283.8423 141.7893 -0.8344 270.8465 271.6809 283.9407 142.6083 -0.8348 270.9868 271.8216 284.0303 143.4265 -0.8344 271.1047 271.9391 284.1386 144.1845 -0.8372 271.2251 272.0624 284.2258 145.0335 -0.8416 271.3376 272.1792 284.3328 145.7913 -0.8440 271.4595 272.3036 284.4429 146.6110 -0.8434 271.5802 272.4236 284.5427 147.4298 -0.8461 271.7004 272.5464 284.6453 148.1905 -0.8494 271.8297 272.6790 284.7475 149.0425 -0.8497 271.9480 272.7977 284.8285 149.8040 -0.8541 272.0561 272.9102 284.9230 150.6260 -0.8577 272.1813 273.0391 285.0176 151.4480 -0.8594 272.3023 273.1617 285.1240 152.2098 -0.8626 272.4219 273.2845 285.2249 153.0620 -0.8607 272.5454 273.4060 285.3157 153.8235 -0.8625 272.6632 273.5257 285.4168 154.6460 -0.8644 272.7880 273.6524 285.5200 155.4678 -0.8687 272.8974 273.7661 285.6178 156.2295 -0.8715 273.0155 273.8871 285.7196 157.0820 -0.8752 273.1454 274.0206 285.8204 157.8435 -0.8748 273.2744 274.1492 285.9253 158.6665 -0.8767 273.3780 274.2547 286.0381 159.4888 -0.8786 273.5120 274.3905 286.1359 160.2505 -0.8800 273.6206 274.5006 286.2453 161.1028 -0.8814 273.7688 274.6502 286.3572 161.8645 -0.8842 273.8704 274.7546 286.4641 162.6868 -0.8852 273.9933 274.8785 286.5810 163.5088 -0.8858 274.1220 275.0078 286.7027 164.2705 -0.8870 274.2388 275.1258 286.8099 165.1228 -0.8903 274.3402 275.2305 286.9298 165.9148 -0.8952 274.4790 275.3741 287.0499 166.7065 -0.8963 274.5838 275.4800 287.1738 167.5290 -0.8985 274.6992 275.5977 287.2913 168.2915 -0.9002 274.8068 275.7070 287.3976 169.1435 -0.9040 274.9439 275.8479 287.5181 169.9355 -0.9053 275.0546 275.9599 287.6349 170.7275 -0.9063 275.1776 276.0840 287.7619 171.5495 -0.9149 275.3159 276.2308 287.8842 172.3415 -0.9178 275.4181 276.3359 288.0010 173.1643 -0.9194 275.5282 276.4476 288.1224 173.9563 -0.9233 275.6479 276.5713 288.2481 174.7458 -0.9278 275.7660 276.6938 288.3538 175.5643 -0.9313 275.8885 276.8197 288.4641 176.3528 -0.9312 276.0176 276.9487 288.5594 177.1710 -0.9313 276.1338 277.0651 288.6660 177.9590 -0.9346 276.2513 277.1859 288.7808 178.7480 -0.9367 276.3786 277.3153 288.8851 179.5705 -0.9368 276.4858 277.4226 288.9837 180.3610 -0.9410 276.6006 277.5417 289.0817 181.1800 -0.9430 276.7310 277.6739 289.1749 181.9713 -0.9461 276.8498 277.7959 289.2729 182.7625 -0.9507 276.9739 277.9246 289.3871 183.5843 -0.9526 277.0956 278.0482 289.4705 184.3755 -0.9551 277.2105 278.1656 289.5656 185.1975 -0.9567 277.3218 278.2786 289.6586 185.9895 -0.9603 277.4450 278.4053 289.7690 186.7815 -0.9632 277.5599 278.5231 289.8601 187.6035 -0.9647 277.6745 278.6393 289.9469 188.3655 -0.9703 277.7885 278.7588 290.0345 189.2175 -0.9694 277.9189 278.8883 290.1388 190.0095 -0.9696 278.0386 279.0082 290.2152 190.8015 -0.9729 278.1612 279.1341 290.2944 191.6233 -0.9761 278.2772 279.2533 290.4071 192.3853 -0.9784 278.3899 279.3683 290.5036 193.2373 -0.9797 278.5198 279.4995 290.5950 194.0295 -0.9796 278.6312 279.6109 290.6851 194.8205 -0.9837 278.7294 279.7131 290.7887 195.6430 -0.9864 278.8594 279.8458 290.8930 196.4345 -0.9876 278.9776 279.9652 291.0098 197.2568 -0.9912 279.1000 280.0913 291.1235 198.0488 -1.0023 279.2113 280.2136 291.2340 198.8405 -1.0065 279.3296 280.3361 291.3473 199.6628 -1.0137 279.4410 280.4547 291.4720 200.4545 -1.0157 279.5597 280.5754 291.5669 201.2768 -1.0174 279.7013 280.7187 291.6926 202.0688 -1.0215 279.8094 280.8309 291.8023 202.8605 -1.0248 279.9350 280.9598 291.9140 203.7125 -1.0174 280.0654 281.0828 292.0290 204.4745 -1.0135 280.1699 281.1833 292.1324 205.2965 -1.0214 280.2789 281.3003 292.2697 206.0883 -1.0268 280.3989 281.4257 292.3808 206.8770 -1.0322 280.5152 281.5474 292.4754 207.6950 -1.0353 280.6316 281.6669 292.5883 208.4830 -1.0386 280.7445 281.7832 292.7052 209.3010 -1.0413 280.8732 281.9145 292.8168 210.0900 -1.0495 280.9902 282.0397 292.9233 210.8780 -1.0651 281.0970 282.1621 293.0531 211.6973 -1.0818 281.2103 282.2921 293.1587 212.4870 -1.0848 281.3214 282.4062 293.2667 213.3050 -1.0827 281.4595 282.5422 293.4031 214.0950 -1.0647 281.5715 282.6361 293.4969 214.8850 -1.0478 281.6797 282.7275 293.6094 215.7033 -1.0442 281.8008 282.8451 293.7393 216.4935 -1.0565 281.9184 282.9749 293.8504 217.3155 -1.0653 282.0435 283.1088 293.9648 218.1078 -1.0708 282.1677 283.2385 294.0685 218.8995 -1.0726 282.2876 283.3603 294.1804 219.7218 -1.0748 282.4098 283.4846 294.2821 220.4835 -1.0752 282.4951 283.5703 294.3955 221.3358 -1.0814 282.6270 283.7084 294.5189 222.1278 -1.0824 282.7436 283.8260 294.6378 222.9195 -1.0827 282.8576 283.9403 294.7523 223.7415 -1.0832 282.9864 284.0696 294.8478 224.5035 -1.0868 283.1062 284.1929 294.9435 225.3570 -1.0926 283.2229 284.3155 295.0560 226.1495 -1.0913 283.3444 284.4357 295.1573 226.9415 -1.0947 283.4597 284.5543 295.2609 227.7638 -1.0959 283.5707 284.6666 295.3498 228.5265 -1.0974 283.6757 284.7731 295.4308 229.3785 -1.1011 283.8143 284.9154 295.5399 230.1705 -1.1026 283.9415 285.0441 295.6083 230.9625 -1.1039 284.0504 285.1543 295.6968 231.7845 -1.1048 284.1557 285.2605 295.7906 232.5465 -1.1048 284.2760 285.3808 295.8763 233.3980 -1.1073 284.3986 285.5059 295.9833 234.1900 -1.1071 284.5143 285.6214 296.0762 234.9815 -1.1089 284.6409 285.7499 296.1642 235.8043 -1.1135 284.7540 285.8675 296.2637 236.5655 -1.1171 284.8702 285.9873 296.3480 237.4180 -1.1261 284.9867 286.1128 296.4467 238.2095 -1.1468 285.1042 286.2511 296.5586 238.9993 -1.1605 285.2170 286.3776 296.6662 239.8170 -1.1630 285.3411 286.5041 296.7594 240.5750 -1.1661 285.4486 286.6147 296.8685 241.4240 -1.1695 285.5852 286.7546 296.9727 242.2123 -1.1726 285.7004 286.8730 297.0846 243.0010 -1.1687 285.7997 286.9684 297.1813 243.7970 -1.1522 285.9266 287.0788 297.2963 244.5863 -1.1365 286.0470 287.1835 297.4030 245.4360 -1.1392 286.1577 287.2969 297.5232 246.1943 -1.1441 286.2728 287.4169 297.6109 247.0160 -1.1489 286.3941 287.5430 297.7181 247.8378 -1.1468 286.5256 287.6724 297.8118 248.5998 -1.1571 286.6224 287.7796 297.9157 249.4518 -1.1643 286.7492 287.9135 298.0602 250.2138 -1.1578 286.8544 288.0122 298.1518 251.0358 -1.1451 286.9777 288.1228 298.2553 251.8280 -1.1471 287.0929 288.2400 298.3631 252.6198 -1.1517 287.2073 288.3590 298.4763 253.4718 -1.1640 287.3309 288.4949 298.6008 254.2338 -1.1706 287.4246 288.5952 298.7059 255.0558 -1.1698 287.5500 288.7198 298.8144 255.8778 -1.1618 287.6956 288.8574 298.9078 256.6395 -1.1610 287.8078 288.9688 299.0177 257.4923 -1.1619 287.9222 289.0841 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