DTA measure 1dta_pb_1 Date: 2024430:1057 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 885.69 s Mass = 966.200 mg data_number = 1102 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1480 0.7227 224.0194 223.2968 265.6999 1.9673 0.7229 224.3010 223.5781 265.7208 2.7560 0.7248 224.5624 223.8376 265.7320 3.5768 0.7271 224.8169 224.0898 265.7433 4.3688 0.7235 225.0779 224.3544 265.7634 5.1605 0.7242 225.3359 224.6117 265.7864 5.9830 0.7231 225.5995 224.8763 265.8064 6.7445 0.7249 225.8588 225.1339 265.8409 7.5968 0.7249 226.1387 225.4137 265.8894 8.3890 0.7239 226.3869 225.6630 265.9190 9.1805 0.7242 226.6422 225.9181 265.9693 10.0028 0.7247 226.9071 226.1823 266.0262 10.7645 0.7238 227.1342 226.4103 266.0775 11.6168 0.7248 227.4038 226.6790 266.1526 12.4088 0.7257 227.6718 226.9461 266.2347 13.2005 0.7246 227.9274 227.2028 266.3249 14.0228 0.7233 228.1910 227.4677 266.4140 14.7845 0.7259 228.4354 227.7095 266.5026 15.6368 0.7247 228.6986 227.9739 266.6288 16.4288 0.7253 228.9581 228.2329 266.7630 17.2205 0.7221 229.1868 228.4647 266.8989 18.0425 0.7228 229.4322 228.7094 267.0375 18.8045 0.7212 229.6791 228.9579 267.1767 19.6565 0.7193 229.9578 229.2385 267.3065 20.4485 0.7190 230.1884 229.4695 267.4737 21.2415 0.7155 230.4346 229.7191 267.6349 22.0635 0.7163 230.6998 229.9834 267.8026 22.8255 0.7144 230.9233 230.2090 267.9566 23.6775 0.7135 231.1734 230.4598 268.1439 24.4695 0.7133 231.4122 230.6989 268.2972 25.2625 0.7096 231.6667 230.9571 268.4638 26.0845 0.7050 231.9002 231.1952 268.6431 26.8440 0.7035 232.1404 231.4369 268.8074 27.6925 0.7001 232.4218 231.7217 269.0007 28.4543 0.6999 232.6583 231.9584 269.1621 29.2740 0.6954 232.8904 232.1951 269.3344 30.0923 0.6939 233.1256 232.4317 269.5085 30.8510 0.6913 233.3529 232.6616 269.6614 31.6990 0.6883 233.6014 232.9131 269.8270 32.4870 0.6859 233.8271 233.1411 269.9829 33.2760 0.6840 234.0691 233.3851 270.1499 34.0958 0.6813 234.3000 233.6187 270.2981 34.8860 0.6781 234.5270 233.8489 270.4481 35.7065 0.6739 234.7778 234.1040 270.5879 36.4975 0.6699 235.0172 234.3473 270.7187 37.2895 0.6677 235.2565 234.5887 270.8622 38.1115 0.6660 235.5054 234.8395 271.0034 38.8735 0.6612 235.7299 235.0687 271.1242 39.7255 0.6597 235.9630 235.3033 271.2826 40.5175 0.6571 236.1884 235.5313 271.4056 41.3095 0.6545 236.4150 235.7605 271.5546 42.1315 0.6504 236.6678 236.0174 271.7121 42.8930 0.6474 236.8666 236.2192 271.8168 43.7453 0.6433 237.1171 236.4739 271.9555 44.5373 0.6412 237.3599 236.7187 272.0817 45.3288 0.6374 237.5782 236.9408 272.2009 46.1513 0.6346 237.8154 237.1808 272.3500 46.9425 0.6290 238.0424 237.4134 272.4859 47.7648 0.6274 238.2707 237.6433 272.6125 48.5570 0.6228 238.5090 237.8862 272.7416 49.3485 0.6184 238.7174 238.0990 272.8712 50.1708 0.6149 238.9557 238.3409 272.9910 50.9625 0.6066 239.1883 238.5817 273.1159 51.7848 0.6045 239.4135 238.8089 273.2293 52.5768 0.6023 239.6300 239.0277 273.3646 53.3685 0.5977 239.8494 239.2517 273.4924 54.2213 0.5902 240.0935 239.5033 273.6187 54.9835 0.5883 240.3060 239.7177 273.7377 55.8065 0.5853 240.5323 239.9470 273.8511 56.5988 0.5800 240.7555 240.1755 273.9928 57.3915 0.5769 240.9784 240.4015 274.1257 58.2435 0.5720 241.2308 240.6588 274.2554 59.0055 0.5675 241.4233 240.8558 274.3621 59.8260 0.5628 241.6311 241.0683 274.4933 60.6140 0.5594 241.8539 241.2945 274.6249 61.4020 0.5540 242.0811 241.5270 274.7529 62.2500 0.5475 242.3116 241.7641 274.8896 63.0083 0.5431 242.5265 241.9834 275.0184 63.8270 0.5405 242.7490 242.2085 275.1386 64.6455 0.5377 242.9658 242.4280 275.2641 65.4040 0.5338 243.1769 242.6431 275.3778 66.2533 0.5280 243.4064 242.8783 275.5071 67.0420 0.5233 243.6100 243.0867 275.6293 67.8325 0.5181 243.8278 243.3097 275.7634 68.6533 0.5146 244.0492 243.5346 275.8995 69.4173 0.5089 244.2692 243.7603 276.0169 70.2695 0.5056 244.4898 243.9842 276.1558 71.0315 0.4997 244.7066 244.2068 276.2735 71.8535 0.4948 244.9531 244.4583 276.3901 72.6755 0.4892 245.1585 244.6694 276.5010 73.4375 0.4836 245.3485 244.8649 276.6176 74.2895 0.4795 245.5684 245.0889 276.7595 75.0515 0.4740 245.7718 245.2978 276.8696 75.8735 0.4697 245.9926 245.5229 277.0065 76.6655 0.4685 246.1934 245.7248 277.1180 77.4575 0.4629 246.4134 245.9505 277.2315 78.3095 0.4550 246.6207 246.1657 277.3748 79.0715 0.4498 246.8365 246.3867 277.4977 79.8935 0.4447 247.0367 246.5920 277.6472 80.6855 0.4398 247.2387 246.7989 277.7837 81.4775 0.4344 247.4697 247.0353 277.9223 82.3295 0.4336 247.6808 247.2472 278.0613 83.0915 0.4289 247.8612 247.4323 278.1899 83.9135 0.4218 248.0678 247.6461 278.3476 84.7358 0.4153 248.2951 247.8798 278.4868 85.4985 0.4093 248.4954 248.0861 278.6271 86.3503 0.4060 248.7247 248.3187 278.7948 87.1423 0.3991 248.9386 248.5395 278.9280 87.9345 0.3938 249.1378 248.7440 279.0806 88.7568 0.3888 249.3477 248.9589 279.2457 89.5198 0.3852 249.5345 249.1492 279.3828 90.3775 0.3801 249.7634 249.3833 279.5396 91.1395 0.3725 249.9596 249.5872 279.6875 91.9600 0.3679 250.1657 249.7978 279.8306 92.7785 0.3630 250.3734 250.0104 279.9708 93.5370 0.3578 250.5647 250.2069 280.1143 94.3863 0.3517 250.7788 250.4271 280.2574 95.1443 0.3452 250.9781 250.6329 280.3676 95.9620 0.3425 251.1879 250.8454 280.5051 96.7805 0.3387 251.3973 251.0586 280.6492 97.5380 0.3317 251.5780 251.2464 280.7786 98.3873 0.3269 251.7898 251.4629 280.9027 99.1765 0.3209 251.9966 251.6756 281.0376 99.9668 0.3177 252.1901 251.8724 281.1635 100.7875 0.3132 252.3957 252.0824 281.2921 101.5485 0.3068 252.5877 252.2809 281.4055 102.4010 0.3023 252.7942 252.4919 281.5284 103.1633 0.2987 252.9938 252.6951 281.6415 103.9878 0.2929 253.2053 252.9125 281.7734 104.8098 0.2865 253.4057 253.1192 281.9113 105.5715 0.2820 253.5972 253.3151 282.0325 106.4238 0.2762 253.7991 253.5229 282.1616 107.1858 0.2731 253.9977 253.7246 282.2676 108.0078 0.2695 254.1950 253.9255 282.4110 108.7998 0.2619 254.3847 254.1228 282.5270 109.5915 0.2566 254.5857 254.3291 282.6524 110.4438 0.2511 254.8017 254.5506 282.7809 111.2055 0.2474 254.9898 254.7424 282.8791 112.0278 0.2391 255.1857 254.9465 282.9951 112.8198 0.2355 255.3846 255.1492 283.1119 113.6115 0.2319 255.5740 255.3421 283.2467 114.4338 0.2278 255.7825 255.5547 283.3910 115.2255 0.2227 255.9777 255.7550 283.5181 116.0485 0.2191 256.1622 255.9431 283.6616 116.8408 0.2116 256.3558 256.1442 283.7960 117.6325 0.2061 256.5518 256.3457 283.9318 118.4548 0.2007 256.7487 256.5479 284.0643 119.2175 0.1976 256.9254 256.7277 284.2149 120.0695 0.1924 257.1253 256.9329 284.3607 120.8615 0.1868 257.3307 257.1439 284.5010 121.6545 0.1854 257.5320 257.3466 284.6370 122.4765 0.1792 257.7170 257.5377 284.7937 123.2385 0.1754 257.8958 257.7204 284.9427 124.0888 0.1720 258.0960 257.9240 285.1017 124.8470 0.1660 258.2969 258.1309 285.2255 125.6658 0.1611 258.4724 258.3114 285.3769 126.4840 0.1585 258.6764 258.5179 285.5306 127.2420 0.1514 258.8697 258.7183 285.6679 128.0900 0.1457 259.0544 258.9087 285.8300 128.8480 0.1408 259.2338 259.0930 285.9502 129.6668 0.1358 259.4400 259.3042 286.1041 130.4883 0.1315 259.6452 259.5138 286.2536 131.2523 0.1260 259.8392 259.7133 286.3838 132.1015 0.1219 260.0316 259.9097 286.5341 132.8618 0.1183 260.1963 260.0780 286.6623 133.6825 0.1137 260.3941 260.2804 286.8019 134.4745 0.1070 260.5800 260.4730 286.9189 135.2665 0.1019 260.7601 260.6582 287.0511 136.1185 0.0968 260.9537 260.8568 287.2051 136.8805 0.0952 261.1303 261.0350 287.3084 137.7025 0.0858 261.3381 261.2522 287.4262 138.4945 0.0841 261.5171 261.4331 287.5506 139.2865 0.0802 261.7017 261.6215 287.6663 140.1085 0.0760 261.8893 261.8133 287.7876 140.8738 0.0718 262.0761 262.0043 287.9048 141.7305 0.0683 262.2612 262.1929 288.0312 142.4923 0.0614 262.4453 262.3840 288.1335 143.3155 0.0588 262.6517 262.5929 288.2447 144.1385 0.0569 262.8357 262.7788 288.3543 144.8998 0.0498 263.0150 262.9652 288.4625 145.7520 0.0485 263.2161 263.1675 288.6119 146.5135 0.0443 263.3942 263.3499 288.7130 147.3358 0.0410 263.5689 263.5279 288.8525 148.1278 0.0375 263.7604 263.7229 288.9759 148.9195 0.0320 263.9328 263.9008 289.0965 149.7723 0.0277 264.1309 264.1032 289.2281 150.5345 0.0254 264.3046 264.2792 289.3554 151.3568 0.0204 264.4924 264.4720 289.4890 152.1488 0.0153 264.6815 264.6662 289.6139 152.9405 0.0134 264.8793 264.8659 289.7338 153.7933 0.0095 265.0798 265.0703 289.8809 154.5555 0.0073 265.2533 265.2459 290.0124 155.3783 0.0031 265.4283 265.4253 290.1407 156.1670 0.0004 265.6040 265.6036 290.2935 156.9550 -0.0027 265.7940 265.7967 290.4317 157.8030 -0.0089 265.9833 265.9922 290.5701 158.5613 -0.0099 266.1451 266.1550 290.6911 159.3810 -0.0136 266.3475 266.3612 290.8623 160.1695 -0.0146 266.5175 266.5321 290.9722 160.9590 -0.0199 266.6933 266.7131 291.1162 161.8080 -0.0220 266.8821 266.9041 291.2538 162.5673 -0.0295 267.0612 267.0907 291.3892 163.3873 -0.0298 267.2563 267.2861 291.5373 164.1788 -0.0340 267.4349 267.4689 291.6874 164.9705 -0.0383 267.6021 267.6404 291.8216 165.8228 -0.0404 267.7713 267.8116 291.9703 166.5845 -0.0436 267.9488 267.9925 292.0982 167.4068 -0.0457 268.1424 268.1881 292.2544 168.1985 -0.0505 268.3371 268.3875 292.3945 168.9905 -0.0571 268.5038 268.5608 292.5336 169.8128 -0.0588 268.6745 268.7334 292.6600 170.6045 -0.0602 268.8662 268.9264 292.8036 171.4268 -0.0627 269.0559 269.1186 292.9616 172.2188 -0.0686 269.2350 269.3036 293.0928 173.0105 -0.0753 269.3955 269.4708 293.2237 173.8328 -0.0791 269.5773 269.6564 293.3665 174.6245 -0.0833 269.7589 269.8422 293.5069 175.4465 -0.0849 269.9380 270.0230 293.6621 176.2385 -0.0860 270.1300 270.2161 293.7859 177.0305 -0.0865 270.2886 270.3751 293.9395 177.8525 -0.0915 270.4823 270.5738 294.0510 178.6445 -0.0945 270.6608 270.7553 294.1768 179.4665 -0.0954 270.8398 270.9352 294.3277 180.2585 -0.0977 271.0133 271.1110 294.4647 181.0505 -0.1040 271.1924 271.2964 294.5893 181.9025 -0.1050 271.3725 271.4776 294.7460 182.6645 -0.1091 271.5364 271.6456 294.8663 183.4873 -0.1130 271.7156 271.8286 295.0264 184.2795 -0.1154 271.8907 272.0061 295.1437 185.0720 -0.1191 272.0729 272.1919 295.2838 185.9245 -0.1258 272.2721 272.3979 295.4174 186.6865 -0.1298 272.4411 272.5709 295.5401 187.5095 -0.1275 272.6182 272.7457 295.6768 188.3015 -0.1311 272.7875 272.9186 295.7958 189.0910 -0.1292 272.9680 273.0972 295.9161 189.9395 -0.1312 273.1353 273.2665 296.0658 190.6970 -0.1337 273.3124 273.4461 296.1863 191.5150 -0.1360 273.4892 273.6252 296.3297 192.3333 -0.1406 273.6644 273.8050 296.4600 193.0913 -0.1789 273.8303 274.0092 296.5738 193.9408 -0.2002 274.0322 274.2324 296.7107 194.7005 -0.2214 274.1978 274.4192 296.8323 195.5220 -0.2129 274.3681 274.5810 296.9610 196.3408 -0.2120 274.5429 274.7549 297.1007 197.1010 -0.2133 274.7084 274.9218 297.2370 197.9523 -0.2152 274.8948 275.1101 297.3576 198.7133 -0.2179 275.0685 275.2864 297.4734 199.5348 -0.2193 275.2426 275.4619 297.6027 200.3573 -0.2196 275.3984 275.6179 297.7406 201.1185 -0.2199 275.5825 275.8023 297.8554 201.9710 -0.2259 275.7633 275.9892 298.0014 202.7340 -0.2253 275.9530 276.1783 298.1176 203.5578 -0.2284 276.1188 276.3472 298.2496 204.3798 -0.2335 276.2925 276.5261 298.3843 205.1415 -0.2359 276.4513 276.6872 298.5144 205.9938 -0.2389 276.6328 276.8717 298.6571 206.7555 -0.2409 276.7971 277.0380 298.7692 207.5778 -0.2424 276.9720 277.2144 298.9234 208.3998 -0.2426 277.1495 277.3920 299.0319 209.1615 -0.2430 277.3225 277.5655 299.1580 210.0138 -0.2412 277.4986 277.7399 299.3077 210.7755 -0.2408 277.6598 277.9006 299.4125 211.5978 -0.2419 277.8397 278.0816 299.5426 212.4200 -0.2427 278.0205 278.2631 299.6818 213.1825 -0.2449 278.1860 278.4308 299.7816 214.0345 -0.2485 278.3549 278.6033 299.9154 214.8268 -0.2454 278.5192 278.7646 300.0327 215.6185 -0.2292 278.7029 278.9321 300.1528 216.4405 -0.2093 278.8906 279.0999 300.2827 217.2025 -0.2164 279.0441 279.2605 300.4016 218.0545 -0.2230 279.2151 279.4381 300.5286 218.8465 -0.2340 279.3754 279.6094 300.6538 219.6395 -0.2553 279.5422 279.7976 300.7792 220.4613 -0.2724 279.7292 280.0017 300.9069 221.2495 -0.2768 279.9067 280.1835 301.0218 222.0670 -0.2846 280.0643 280.3489 301.1365 222.8348 -0.2741 280.2389 280.5130 301.2433 223.6638 -0.2383 280.4079 280.6462 301.3759 224.4520 -0.2204 280.5730 280.7934 301.5012 225.2400 -0.2215 280.7485 280.9699 301.6247 226.0605 -0.2205 280.9347 281.1552 301.7459 226.8510 -0.2201 281.0891 281.3093 301.8730 227.6705 -0.2216 281.2506 281.4722 302.0161 228.4608 -0.2299 281.4056 281.6355 302.1562 229.2513 -0.2709 281.5753 281.8463 302.2991 230.0725 -0.2689 281.7412 282.0101 302.4237 230.8638 -0.2754 281.9283 282.2037 302.5581 231.6855 -0.2694 282.1070 282.3764 302.7156 232.4775 -0.2640 282.2737 282.5377 302.8531 233.2695 -0.2817 282.4415 282.7232 302.9959 234.0915 -0.2793 282.6138 282.8931 303.1248 234.8535 -0.2763 282.7610 283.0372 303.2641 235.7055 -0.3000 282.9317 283.2317 303.4050 236.4975 -0.2812 283.0944 283.3756 303.5398 237.2895 -0.2568 283.2680 283.5248 303.6790 238.1115 -0.2499 283.4410 283.6909 303.8396 238.9035 -0.2628 283.6154 283.8782 303.9997 239.7255 -0.2757 283.7739 284.0496 304.1234 240.5175 -0.2825 283.9385 284.2210 304.2680 241.3093 -0.2867 284.1014 284.3881 304.4117 242.1313 -0.2788 284.2559 284.5347 304.5450 242.8930 -0.2572 284.4226 284.6798 304.6883 243.7600 -0.2520 284.6167 284.8687 304.8596 244.5218 -0.2540 284.7861 285.0401 305.0142 245.3445 -0.2538 284.9730 285.2267 305.1579 246.1378 -0.2539 285.1186 285.3726 305.2933 246.9295 -0.2550 285.2742 285.5292 305.4219 247.7823 -0.2567 285.4593 285.7161 305.5760 248.5445 -0.3366 285.6259 285.9624 305.7142 249.3668 -0.4293 285.7917 286.2210 305.8576 250.1588 -0.4560 285.9688 286.4248 305.9867 250.9515 -0.4612 286.1317 286.5929 306.1063 251.7738 -0.4618 286.2957 286.7575 306.2584 252.5650 -0.4601 286.4399 286.9001 306.3859 253.3840 -0.4582 286.6380 287.0962 306.5049 254.1720 -0.4599 286.7917 287.2516 306.6540 254.9600 -0.4590 286.9629 287.4219 306.7804 255.7788 -0.4580 287.1178 287.5758 306.8985 256.5370 -0.4483 287.2814 287.7297 307.0313 257.3865 -0.4517 287.4608 287.9126 307.1468 258.1753 -0.4687 287.6291 288.0978 307.2586 258.9640 -0.4679 287.7856 288.2534 307.3796 259.7825 -0.4240 287.9494 288.3734 307.5110 260.5430 -0.2970 288.1202 288.4172 307.6421 261.3968 -0.2562 288.2771 288.5333 307.7841 262.1588 -0.2491 288.4347 288.6838 307.8959 262.9808 -0.2470 288.6037 288.8507 308.0001 263.7730 -0.2474 288.7723 289.0197 308.1272 264.5655 -0.2466 288.9465 289.1931 308.2418 265.4178 -0.2473 289.1071 289.3544 308.3706 266.1795 -0.2462 289.2658 289.5121 308.4812 267.0018 -0.2460 289.4395 289.6855 308.6085 267.7938 -0.2466 289.5982 289.8448 308.7292 268.5855 -0.2456 289.7539 289.9995 308.8431 269.4078 -0.2445 289.9211 290.1656 308.9699 270.1695 -0.2447 290.0719 290.3166 309.1014 271.0218 -0.2421 290.2648 290.5069 309.2359 271.8138 -0.2430 290.4140 290.6570 309.3510 272.6055 -0.2435 290.5729 290.8163 309.4907 273.4280 -0.2484 290.7397 290.9881 309.6223 274.1905 -0.2507 290.8965 291.1472 309.7654 275.0425 -0.2600 291.0696 291.3297 309.9117 275.8345 -0.2781 291.2377 291.5158 310.0434 276.6275 -0.2894 291.4024 291.6918 310.1788 277.4498 -0.2881 291.5629 291.8510 310.3195 278.2125 -0.3002 291.7221 292.0222 310.4508 279.0645 -0.3255 291.8987 292.2242 310.6098 279.8265 -0.3291 292.0333 292.3624 310.7480 280.6493 -0.3487 292.1927 292.5414 310.8799 281.4715 -0.3838 292.3810 292.7649 311.0355 282.2333 -0.3894 292.5500 292.9394 311.1724 283.0855 -0.3138 292.7040 293.0177 311.3048 283.8480 -0.2619 292.8475 293.1093 311.4523 284.6698 -0.2457 293.0173 293.2630 311.5801 285.4860 -0.2440 293.1853 293.4294 311.7403 286.2440 -0.2445 293.3261 293.5706 311.8756 287.0925 -0.2481 293.5126 293.7607 312.0135 287.8503 -0.2587 293.6650 293.9237 312.1633 288.7295 -0.2607 293.8443 294.1050 312.3175 289.6078 -0.2609 294.0336 294.2945 312.4680 290.3958 -0.2605 294.1740 294.4345 312.5940 291.2153 -0.2602 294.3396 294.5997 312.7216 292.0045 -0.2631 294.5013 294.7644 312.8591 292.7953 -0.2631 294.6474 294.9106 312.9998 293.6165 -0.2626 294.8252 295.0878 313.1416 294.3890 -0.2531 294.9747 295.2277 313.2729 295.2225 -0.2527 295.1446 295.3973 313.4033 296.0145 -0.2599 295.3248 295.5847 313.5294 296.8365 -0.2612 295.4687 295.7299 313.6779 297.6285 -0.2593 295.6156 295.8749 313.7926 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