DTA measure 1dta_pb_22 Date: 2024430:1146 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 975.91 s Mass = 966.200 mg data_number = 1214 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1615 -0.8120 250.8018 251.6138 266.2682 1.9835 -0.8070 250.9291 251.7362 266.2858 2.7455 -0.8042 251.0423 251.8465 266.3228 3.5975 -0.7961 251.1834 251.9796 266.3547 4.3595 -0.7921 251.2895 252.0815 266.3473 5.1835 -0.7853 251.4241 252.2094 266.3754 6.0055 -0.7806 251.5473 252.3279 266.4077 6.7675 -0.7788 251.6609 252.4397 266.4261 7.6195 -0.7720 251.7954 252.5674 266.4638 8.3815 -0.7674 251.9053 252.6728 266.4965 9.2033 -0.7605 252.0456 252.8060 266.5424 10.0255 -0.7547 252.1698 252.9245 266.5931 10.7875 -0.7495 252.2712 253.0207 266.6197 11.6390 -0.7450 252.3994 253.1443 266.6807 12.4008 -0.7414 252.5258 253.2671 266.7358 13.2228 -0.7365 252.6564 253.3929 266.8047 14.0448 -0.7328 252.7685 253.5013 266.8898 14.8065 -0.7280 252.8788 253.6068 266.9663 15.6593 -0.7240 253.0113 253.7353 267.0550 16.4518 -0.7184 253.1312 253.8496 267.1600 17.2445 -0.7139 253.2472 253.9611 267.2517 18.0668 -0.7076 253.3705 254.0781 267.3385 18.8293 -0.7041 253.4766 254.1807 267.4417 19.6818 -0.7010 253.6126 254.3136 267.5688 20.4728 -0.6970 253.7356 254.4326 267.6679 21.2610 -0.6930 253.8428 254.5358 267.7661 22.0790 -0.6892 253.9800 254.6692 267.8868 22.8370 -0.6850 254.1069 254.7919 267.9979 23.6850 -0.6803 254.2283 254.9086 268.1008 24.4733 -0.6771 254.3330 255.0101 268.2087 25.2628 -0.6735 254.4413 255.1148 268.3323 26.0820 -0.6683 254.5539 255.2222 268.4635 26.8428 -0.6680 254.6792 255.3472 268.5639 27.6918 -0.6640 254.8025 255.4666 268.6948 28.4810 -0.6607 254.9158 255.5765 268.8129 29.2725 -0.6601 255.0234 255.6834 268.9341 30.0948 -0.6570 255.1650 255.8221 269.0511 30.8565 -0.6549 255.2787 255.9336 269.1624 31.7090 -0.6507 255.3992 256.0499 269.2928 32.5008 -0.6484 255.5022 256.1506 269.4152 33.2925 -0.6439 255.6202 256.2641 269.5395 34.1188 -0.6412 255.7510 256.3922 269.6722 34.8833 -0.6314 255.8560 256.4875 269.7728 35.7355 -0.6320 255.9910 256.6229 269.8987 36.4980 -0.6332 256.1029 256.7361 270.0192 37.3205 -0.6330 256.2171 256.8502 270.1620 38.1125 -0.6311 256.3545 256.9857 270.2725 38.9045 -0.6245 256.4567 257.0812 270.3798 39.7565 -0.6246 256.5965 257.2211 270.5233 40.5185 -0.6218 256.6974 257.3192 270.6267 41.3415 -0.6178 256.8220 257.4398 270.7524 42.1335 -0.6188 256.9361 257.5549 270.8781 42.9255 -0.6209 257.0453 257.6663 271.0064 43.7793 -0.6173 257.1676 257.7849 271.1353 44.5415 -0.6200 257.2743 257.8943 271.2374 45.3635 -0.6185 257.3932 258.0117 271.3500 46.1555 -0.6176 257.5275 258.1451 271.4653 46.9475 -0.6167 257.6510 258.2677 271.5835 47.7995 -0.6136 257.7660 258.3796 271.7086 48.5615 -0.6147 257.8772 258.4919 271.8173 49.3835 -0.6103 257.9967 258.6070 271.9150 50.2050 -0.6102 258.1260 258.7362 272.0395 50.9665 -0.6087 258.2358 258.8445 272.1214 51.8190 -0.6089 258.3547 258.9636 272.2318 52.5793 -0.6069 258.4609 259.0678 272.3270 53.3963 -0.6063 258.5884 259.1947 272.4288 54.2140 -0.6053 258.6987 259.3040 272.5305 54.9710 -0.6007 258.8190 259.4197 272.6252 55.8190 -0.5982 258.9485 259.5468 272.7366 56.5773 -0.5978 259.0598 259.6576 272.8206 57.3950 -0.5976 259.1709 259.7685 272.9201 58.2138 -0.5930 259.2955 259.8885 273.0228 58.9713 -0.5940 259.4041 259.9981 273.1240 59.8200 -0.5977 259.5231 260.1208 273.2226 60.6088 -0.5961 259.6661 260.2622 273.3240 61.3975 -0.5920 259.7719 260.3639 273.4140 62.2180 -0.5934 259.8786 260.4719 273.5114 63.0080 -0.5878 259.9905 260.5782 273.6120 63.8290 -0.5906 260.1242 260.7149 273.7150 64.6215 -0.5971 260.2464 260.8435 273.8104 65.4133 -0.5956 260.3444 260.9400 273.9065 66.2353 -0.5877 260.4530 261.0407 273.9994 67.0270 -0.5916 260.5795 261.1711 274.0951 67.8488 -0.5915 260.7005 261.2920 274.1952 68.6413 -0.5920 260.8290 261.4210 274.2853 69.4325 -0.5922 260.9356 261.5277 274.3963 70.2550 -0.5901 261.0495 261.6395 274.5033 71.0470 -0.5882 261.1620 261.7502 274.6057 71.8698 -0.5904 261.2943 261.8846 274.7105 72.6618 -0.5899 261.4198 262.0097 274.8149 73.4535 -0.5886 261.5229 262.1114 274.9284 74.3058 -0.5881 261.6328 262.2208 275.0503 75.0675 -0.5884 261.7490 262.3374 275.1495 75.8898 -0.5864 261.8686 262.4550 275.2723 76.6818 -0.5897 261.9950 262.5846 275.3743 77.4735 -0.5883 262.1081 262.6964 275.4962 78.3258 -0.5899 262.2217 262.8116 275.6175 79.0875 -0.5898 262.3309 262.9207 275.7294 79.9095 -0.5901 262.4461 263.0362 275.8407 80.7023 -0.5910 262.5674 263.1584 275.9492 81.4945 -0.5916 262.6909 263.2825 276.0598 82.3470 -0.5922 262.8054 263.3976 276.1908 83.1095 -0.5923 262.9249 263.5172 276.3180 83.9315 -0.5903 263.0369 263.6273 276.4429 84.7520 -0.5914 263.1476 263.7390 276.5399 85.5100 -0.5901 263.2736 263.8637 276.6604 86.3578 -0.5917 263.3930 263.9847 276.7756 87.1160 -0.5924 263.5097 264.1021 276.8891 87.9348 -0.5921 263.6311 264.2232 277.0092 88.7245 -0.5946 263.7501 264.3446 277.1218 89.5160 -0.5941 263.8491 264.4431 277.2348 90.3645 -0.5926 263.9471 264.5397 277.3495 91.1230 -0.5918 264.0711 264.6628 277.4470 91.9435 -0.5926 264.1980 264.7905 277.5653 92.7338 -0.5948 264.3171 264.9118 277.6694 93.5250 -0.5961 264.4315 265.0276 277.7738 94.3465 -0.5961 264.5487 265.1448 277.8705 95.1385 -0.5975 264.6639 265.2614 277.9498 95.9608 -0.5987 264.7835 265.3822 278.0611 96.7525 -0.6000 264.8953 265.4952 278.1656 97.5445 -0.5986 265.0120 265.6106 278.2570 98.3665 -0.5987 265.1286 265.7272 278.3466 99.1285 -0.6024 265.2347 265.8371 278.4390 99.9805 -0.6027 265.3561 265.9588 278.5374 100.7725 -0.6018 265.4776 266.0793 278.6207 101.5645 -0.6020 265.5958 266.1978 278.7230 102.3865 -0.6050 265.7182 266.3231 278.7887 103.1485 -0.6058 265.8416 266.4474 278.8814 104.0005 -0.6064 265.9412 266.5476 278.9815 104.7925 -0.6067 266.0634 266.6701 279.0864 105.5845 -0.6074 266.1724 266.7798 279.1873 106.4065 -0.6075 266.2918 266.8994 279.2856 107.1685 -0.6092 266.4079 267.0171 279.3655 108.0205 -0.6079 266.5254 267.1334 279.4838 108.7820 -0.6106 266.6425 267.2531 279.5870 109.6038 -0.6121 266.7702 267.3823 279.6929 110.4265 -0.6122 266.8825 267.4947 279.7975 111.1885 -0.6131 266.9890 267.6021 279.8995 112.0410 -0.6143 267.1166 267.7309 280.0015 112.8025 -0.6155 267.2251 267.8405 280.1308 113.6248 -0.6152 267.3470 267.9622 280.2252 114.4168 -0.6155 267.4588 268.0744 280.3278 115.2095 -0.6181 267.5797 268.1977 280.4263 116.0618 -0.6203 267.6932 268.3135 280.5541 116.8210 -0.6227 267.7904 268.4132 280.6585 117.6380 -0.6212 267.9056 268.5267 280.7691 118.4270 -0.6216 268.0295 268.6511 280.8688 119.2160 -0.6266 268.1492 268.7758 280.9749 120.0640 -0.6274 268.2849 268.9124 281.1004 120.8220 -0.6247 268.3770 269.0017 281.1975 121.6405 -0.6266 268.4967 269.1233 281.2988 122.4315 -0.6277 268.6080 269.2357 281.4086 123.2220 -0.6336 268.7330 269.3666 281.5167 124.0723 -0.6253 268.8582 269.4835 281.6240 124.8313 -0.6270 268.9763 269.6033 281.7343 125.6523 -0.6342 269.0791 269.7133 281.8395 126.4458 -0.6373 269.2066 269.8439 281.9466 127.2405 -0.6410 269.3128 269.9538 282.0554 128.0628 -0.6399 269.4287 270.0685 282.1630 128.8245 -0.6428 269.5430 270.1858 282.2752 129.6768 -0.6428 269.6522 270.2950 282.3778 130.4688 -0.6464 269.7743 270.4207 282.4827 131.2605 -0.6485 269.8960 270.5445 282.6025 132.0828 -0.6505 270.0176 270.6681 282.7075 132.8445 -0.6479 270.1148 270.7626 282.8188 133.6968 -0.6472 270.2262 270.8734 282.9282 134.4585 -0.6493 270.3361 270.9854 283.0333 135.2808 -0.6506 270.4597 271.1103 283.1410 136.1025 -0.6516 270.5829 271.2345 283.2557 136.8645 -0.6534 270.6935 271.3470 283.3500 137.7165 -0.6532 270.8074 271.4606 283.4620 138.4785 -0.6553 270.9219 271.5773 283.5658 139.3005 -0.6554 271.0403 271.6957 283.6629 140.1225 -0.6587 271.1687 271.8274 283.7668 140.8845 -0.6576 271.2624 271.9199 283.8756 141.7365 -0.6605 271.3848 272.0454 283.9949 142.4985 -0.6625 271.4979 272.1604 284.0940 143.3205 -0.6620 271.6161 272.2781 284.2056 144.1425 -0.6632 271.7458 272.4091 284.3052 144.9045 -0.6659 271.8418 272.5077 284.4116 145.7563 -0.6691 271.9630 272.6320 284.5150 146.5195 -0.6739 272.0750 272.7488 284.6268 147.3438 -0.6730 272.2038 272.8768 284.7337 148.1660 -0.6760 272.3195 272.9955 284.8481 148.9275 -0.6699 272.4246 273.0946 284.9535 149.7775 -0.6777 272.5495 273.2272 285.0506 150.5350 -0.6785 272.6494 273.3279 285.1538 151.3523 -0.6735 272.7626 273.4361 285.2564 152.1700 -0.6794 272.8812 273.5605 285.3731 152.9288 -0.6835 272.9882 273.6716 285.4683 153.7770 -0.6869 273.1161 273.8031 285.5633 154.5355 -0.6865 273.2404 273.9269 285.6726 155.3538 -0.6892 273.3535 274.0427 285.7875 156.1728 -0.6917 273.4778 274.1695 285.8819 156.9330 -0.6917 273.5874 274.2792 285.9830 157.7825 -0.6923 273.6951 274.3873 286.0982 158.5725 -0.6922 273.8156 274.5078 286.1919 159.3645 -0.6969 273.9277 274.6246 286.2986 160.1863 -0.6981 274.0573 274.7554 286.4134 160.9480 -0.7011 274.1695 274.8705 286.5014 161.8000 -0.6955 274.2741 274.9696 286.5997 162.5623 -0.6987 274.3908 275.0895 286.7024 163.3838 -0.7017 274.5063 275.2080 286.8028 164.2065 -0.7067 274.6322 275.3390 286.9163 164.9675 -0.7051 274.7368 275.4419 287.0063 165.8203 -0.7131 274.8605 275.5736 287.1216 166.5818 -0.7164 274.9692 275.6856 287.2069 167.4038 -0.7139 275.0939 275.8078 287.3008 168.2260 -0.7137 275.2049 275.9186 287.4226 168.9875 -0.7146 275.3029 276.0175 287.5135 169.8398 -0.7186 275.4503 276.1689 287.6208 170.6015 -0.7217 275.5508 276.2725 287.7229 171.4238 -0.7258 275.6584 276.3843 287.8247 172.2460 -0.7248 275.7845 276.5093 287.9396 173.0075 -0.7230 275.8924 276.6153 288.0209 173.8598 -0.7261 276.0015 276.7275 288.1306 174.6518 -0.7287 276.1316 276.8603 288.2343 175.4445 -0.7254 276.2555 276.9810 288.3123 176.2668 -0.7297 276.3600 277.0898 288.4272 177.0285 -0.7317 276.4672 277.1989 288.5237 177.8808 -0.7341 276.5970 277.3311 288.6335 178.6425 -0.7376 276.7055 277.4431 288.7333 179.4653 -0.7307 276.8264 277.5570 288.8270 180.2880 -0.7369 276.9417 277.6785 288.9418 181.0505 -0.7344 277.0454 277.7797 289.0434 181.8988 -0.7353 277.1567 277.8920 289.1444 182.6865 -0.7400 277.2815 278.0214 289.2649 183.4768 -0.7409 277.3966 278.1375 289.3665 184.2950 -0.7466 277.5051 278.2517 289.4773 185.0538 -0.7493 277.6109 278.3602 289.5809 185.9058 -0.7442 277.7399 278.4841 289.7198 186.6645 -0.7490 277.8493 278.5983 289.8232 187.4840 -0.7545 277.9658 278.7203 289.9397 188.3028 -0.7577 278.0867 278.8444 290.0704 189.0620 -0.7605 278.1826 278.9431 290.2015 189.9118 -0.7609 278.3058 279.0667 290.3245 190.6725 -0.7628 278.4237 279.1865 290.4517 191.4933 -0.7609 278.5427 279.3036 290.5696 192.3145 -0.7635 278.6442 279.4077 290.6938 193.0768 -0.7677 278.7775 279.5452 290.8119 193.9295 -0.7682 278.8939 279.6620 290.9203 194.6915 -0.7734 278.9924 279.7657 291.0297 195.5135 -0.7771 279.1051 279.8822 291.1516 196.3055 -0.7799 279.2291 280.0090 291.2701 197.1023 -0.7761 279.3364 280.1124 291.3707 197.9265 -0.7778 279.4629 280.2408 291.4804 198.7185 -0.7765 279.5572 280.3337 291.5846 199.5415 -0.7843 279.6747 280.4590 291.6922 200.3335 -0.7885 279.8034 280.5919 291.8005 201.1255 -0.7885 279.9149 280.7034 291.9042 201.9478 -0.7919 280.0333 280.8252 292.0123 202.7215 -0.7908 280.1503 280.9411 292.0942 203.5780 -0.7902 280.2735 281.0637 292.2087 204.3408 -0.7952 280.3697 281.1649 292.3023 205.1643 -0.7971 280.4885 281.2855 292.3973 205.9560 -0.8012 280.6063 281.4075 292.4777 206.7475 -0.8077 280.7185 281.5262 292.5780 207.6000 -0.8088 280.8376 281.6464 292.6886 208.3618 -0.8132 280.9401 281.7533 292.7657 209.1838 -0.8148 281.0691 281.8839 292.8661 210.0058 -0.8180 281.1874 282.0053 292.9686 210.7675 -0.8179 281.2921 282.1101 293.0648 211.6198 -0.8203 281.4159 282.2362 293.1595 212.3815 -0.8236 281.5247 282.3483 293.2460 213.2035 -0.8207 281.6347 282.4554 293.3378 214.0220 -0.8242 281.7689 282.5931 293.4257 214.7800 -0.8282 281.8682 282.6965 293.5192 215.6298 -0.8301 281.9971 282.8272 293.6277 216.3890 -0.8329 282.0939 282.9268 293.7155 217.2070 -0.8326 282.2132 283.0458 293.8190 217.9955 -0.8337 282.3353 283.1690 293.9257 218.7848 -0.8359 282.4420 283.2779 294.0402 219.6338 -0.8383 282.5688 283.4071 294.1604 220.3933 -0.8418 282.6705 283.5123 294.2645 221.2130 -0.8429 282.7830 283.6258 294.3663 222.0338 -0.8446 282.8980 283.7427 294.4774 222.7955 -0.8453 283.0023 283.8477 294.5835 223.6490 -0.8481 283.1277 283.9759 294.7055 224.4108 -0.8514 283.2480 284.0994 294.7980 225.2328 -0.8524 283.3600 284.2125 294.9306 226.0248 -0.8561 283.4717 284.3278 295.0566 226.8165 -0.8566 283.5930 284.4496 295.1671 227.6388 -0.8571 283.7210 284.5781 295.2864 228.4305 -0.8605 283.8224 284.6829 295.3834 229.2528 -0.8557 283.9397 284.7954 295.5094 230.0448 -0.8598 284.0426 284.9024 295.6292 230.8365 -0.8616 284.1617 285.0233 295.7419 231.6588 -0.8648 284.2796 285.1443 295.8648 232.4505 -0.8685 284.3821 285.2506 295.9809 233.2728 -0.8703 284.5042 285.3745 296.1016 234.0685 -0.8734 284.6274 285.5009 296.2310 234.8615 -0.8763 284.7462 285.6224 296.3566 235.6835 -0.8779 284.8657 285.7437 296.4664 236.4455 -0.8806 284.9634 285.8440 296.5803 237.2975 -0.8858 285.0918 285.9776 296.6997 238.0895 -0.8890 285.2161 286.1051 296.8117 238.8815 -0.8913 285.3183 286.2096 296.9092 239.7035 -0.8889 285.4470 286.3359 297.0094 240.4655 -0.8946 285.5477 286.4422 297.1216 241.3183 -0.8897 285.6539 286.5435 297.2184 242.0805 -0.8917 285.7571 286.6488 297.3279 242.9025 -0.8965 285.8973 286.7938 297.4182 243.7245 -0.8930 286.0060 286.8989 297.5090 244.4863 -0.8959 286.1148 287.0107 297.6032 245.3380 -0.8914 286.2237 287.1151 297.7080 246.0960 -0.8897 286.3349 287.2246 297.7824 246.9133 -0.8863 286.4520 287.3384 297.8751 247.7323 -0.8894 286.5799 287.4693 297.9847 248.4910 -0.8958 286.6976 287.5934 298.0677 249.3393 -0.8949 286.8170 287.7119 298.1503 250.0975 -0.9014 286.9225 287.8239 298.2314 250.9158 -0.9093 287.0284 287.9376 298.3159 251.7343 -0.9090 287.1599 288.0689 298.4194 252.4925 -0.9139 287.2746 288.1885 298.5050 253.3418 -0.9162 287.3977 288.3139 298.6121 254.1020 -0.9163 287.4900 288.4063 298.7093 254.9235 -0.9136 287.6056 288.5192 298.8044 255.7165 -0.8908 287.7187 288.6095 298.9036 256.5085 -0.9059 287.8514 288.7574 299.0070 257.3605 -0.9267 287.9731 288.8998 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