DTA measure 2dta_pb_22 Date: 2024430:1217 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1728.52 s Mass = 966.200 mg data_number = 1075 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5090 -3.7168 405.8945 409.6113 400.9501 4.1150 -3.7205 406.0364 409.7569 400.9866 5.7076 -3.7213 406.1861 409.9074 400.9689 7.3170 -3.7238 406.3320 410.0558 400.9557 8.9263 -3.7226 406.4878 410.2104 400.9224 10.5394 -3.7320 406.6419 410.3739 400.8713 12.1376 -3.7386 406.7684 410.5070 400.8004 13.7374 -3.7398 406.9143 410.6541 400.7118 15.3386 -3.7404 407.0511 410.7915 400.6114 16.9528 -3.7449 407.1778 410.9227 400.4845 18.5690 -3.7472 407.3168 411.0639 400.3525 20.1711 -3.7525 407.4445 411.1970 400.2474 21.7725 -3.7517 407.5955 411.3472 400.1156 23.3865 -3.7552 407.7189 411.4740 399.9770 25.0005 -3.7569 407.8419 411.5989 399.8397 26.6145 -3.7615 407.9634 411.7249 399.6767 28.2144 -3.7611 408.0917 411.8528 399.5420 29.8159 -3.7609 408.1965 411.9575 399.3891 31.4308 -3.7634 408.3256 412.0890 399.2280 33.0265 -3.7626 408.4499 412.2125 399.0543 34.6471 -3.7678 408.5516 412.3194 398.9037 36.2381 -3.7688 408.6704 412.4392 398.7650 37.8446 -3.7750 408.7794 412.5544 398.6443 39.4383 -3.7754 408.8752 412.6506 398.5153 41.0640 -3.7790 408.9705 412.7495 398.4159 42.6603 -3.7815 409.0659 412.8474 398.2922 44.2593 -3.7815 409.1711 412.9525 398.1832 45.8748 -3.7827 409.2595 413.0422 398.0760 47.4736 -3.7827 409.3633 413.1460 397.9735 49.0726 -3.7861 409.4592 413.2453 397.8694 50.7019 -3.7861 409.5355 413.3216 397.7727 52.3006 -3.7891 409.6219 413.4110 397.6620 53.9146 -3.7940 409.7081 413.5020 397.5628 55.5136 -3.7965 409.7838 413.5803 397.4295 57.1290 -3.7993 409.8600 413.6592 397.3031 58.7438 -3.8034 409.9350 413.7384 397.1827 60.3436 -3.8066 410.0069 413.8135 397.0625 61.9591 -3.8071 410.0871 413.8942 396.9380 63.5615 -3.8093 410.1539 413.9632 396.8111 65.1599 -3.8063 410.2208 414.0271 396.6956 66.7835 -3.8117 410.2838 414.0955 396.5772 68.3746 -3.8147 410.3403 414.1550 396.4722 69.9664 -3.8212 410.4021 414.2233 396.3511 71.5771 -3.8251 410.4645 414.2896 396.2263 73.1724 -3.8246 410.5270 414.3516 396.1179 74.7981 -3.8257 410.5757 414.4015 396.0063 76.3976 -3.8280 410.6289 414.4568 395.8816 77.9965 -3.8315 410.6709 414.5024 395.7533 79.6105 -3.8349 410.7277 414.5626 395.6393 81.2095 -3.8405 410.7692 414.6097 395.5046 82.8233 -3.8441 410.8054 414.6495 395.3608 84.4374 -3.8465 410.8566 414.7032 395.2137 86.0359 -3.8475 410.8832 414.7307 395.0903 87.6348 -3.8533 410.9238 414.7771 394.9494 89.2486 -3.8550 410.9576 414.8126 394.8108 90.8635 -3.8580 410.9992 414.8572 394.6683 92.4780 -3.8626 411.0269 414.8895 394.5401 94.0776 -3.8642 411.0562 414.9204 394.4124 95.6766 -3.8665 411.0699 414.9364 394.2868 97.2903 -3.8689 411.0891 414.9580 394.1536 98.8981 -3.8714 411.1235 414.9950 394.0249 100.4893 -3.8743 411.1508 415.0251 393.8941 102.0835 -3.8754 411.1614 415.0368 393.7735 103.6926 -3.8807 411.1782 415.0590 393.6576 105.2861 -3.8818 411.1978 415.0796 393.5297 106.8946 -3.8876 411.2013 415.0889 393.4186 108.5066 -3.8912 411.2173 415.1085 393.2989 110.1055 -3.8916 411.2227 415.1143 393.1861 111.7058 -3.8939 411.2384 415.1323 393.0746 113.3206 -3.8993 411.2403 415.1397 392.9542 114.9195 -3.9044 411.2394 415.1438 392.8442 116.5335 -3.9084 411.2481 415.1565 392.7298 118.1475 -3.9075 411.2439 415.1515 392.6211 119.7465 -3.9128 411.2412 415.1541 392.5219 121.3455 -3.9121 411.2386 415.1507 392.4142 122.9595 -3.9180 411.2302 415.1482 392.2984 124.5738 -3.9186 411.2170 415.1357 392.1825 126.1879 -3.9222 411.2234 415.1456 392.0339 127.7868 -3.9253 411.2129 415.1381 391.9178 129.3849 -3.9335 411.2094 415.1429 391.7868 130.9928 -3.9370 411.1993 415.1364 391.6378 132.6033 -3.9368 411.1729 415.1098 391.5049 134.1969 -3.9438 411.1617 415.1055 391.3838 135.8031 -3.9436 411.1375 415.0810 391.2707 137.3955 -3.9466 411.1152 415.0618 391.1287 139.0063 -3.9502 411.1017 415.0520 390.9976 140.6329 -3.9505 411.0905 415.0409 390.8787 142.2459 -3.9501 411.0661 415.0162 390.7434 143.8451 -3.9519 411.0442 414.9961 390.6326 145.4448 -3.9611 410.9980 414.9591 390.5006 147.0588 -3.9640 410.9846 414.9486 390.3817 148.6728 -3.9665 410.9528 414.9194 390.2590 150.2750 -3.9689 410.9247 414.8936 390.1471 151.8796 -3.9708 410.8984 414.8692 390.0208 153.4786 -3.9744 410.8652 414.8396 389.9047 155.0925 -3.9767 410.8298 414.8065 389.7863 156.7065 -3.9795 410.8000 414.7795 389.6762 158.3205 -3.9807 410.7650 414.7456 389.5740 159.9195 -3.9857 410.7382 414.7240 389.4523 161.5321 -3.9846 410.6845 414.6691 389.3334 163.1245 -3.9869 410.6489 414.6358 389.1986 164.7315 -3.9837 410.6073 414.5910 389.0748 166.3380 -3.9886 410.5659 414.5544 388.9265 167.9333 -3.9905 410.5277 414.5182 388.7912 169.5294 -3.9970 410.4751 414.4721 388.6543 171.1304 -3.9989 410.4296 414.4285 388.5184 172.7876 -3.9994 410.3844 414.3838 388.3735 174.3865 -4.0022 410.3372 414.3393 388.2512 175.9855 -4.0056 410.2869 414.2925 388.0907 177.5995 -4.0048 410.2416 414.2464 387.9428 179.2135 -4.0060 410.1767 414.1828 387.7972 180.8275 -4.0066 410.1249 414.1315 387.6587 182.4265 -4.0090 410.0797 414.0887 387.5335 184.0250 -4.0121 410.0345 414.0466 387.4019 185.6388 -4.0145 409.9720 413.9865 387.2600 187.2679 -4.0154 409.9166 413.9320 387.1073 188.8676 -4.0171 409.8527 413.8698 386.9782 190.4669 -4.0184 409.7909 413.8093 386.8373 192.0816 -4.0183 409.7267 413.7450 386.7020 193.6956 -4.0183 409.6692 413.6875 386.5628 195.3061 -4.0208 409.6214 413.6422 386.4216 196.8980 -4.0205 409.5419 413.5624 386.3089 198.5048 -4.0209 409.4806 413.5015 386.1857 200.0966 -4.0213 409.4197 413.4409 386.0432 201.7044 -4.0242 409.3525 413.3766 385.9286 203.3128 -4.0246 409.2924 413.3170 385.8068 204.9136 -4.0269 409.2118 413.2387 385.6830 206.5286 -4.0275 409.1488 413.1763 385.5665 208.1275 -4.0253 409.0846 413.1099 385.4446 209.7415 -4.0267 409.0053 413.0319 385.3119 211.3556 -4.0292 408.9202 412.9493 385.1798 212.9545 -4.0298 408.8602 412.8900 385.0661 214.5685 -4.0306 408.8039 412.8345 384.9543 216.1675 -4.0317 408.7121 412.7438 384.8248 217.7815 -4.0308 408.6542 412.6850 384.7026 219.3964 -4.0297 408.5661 412.5958 384.5927 220.9955 -4.0321 408.4943 412.5264 384.4737 222.6096 -4.0322 408.4277 412.4598 384.3632 224.2091 -4.0335 408.3351 412.3685 384.2371 225.8236 -4.0336 408.2623 412.2960 384.1205 227.4331 -4.0336 408.1796 412.2132 383.9945 229.0244 -4.0328 408.1015 412.1343 383.8706 230.6314 -4.0305 408.0228 412.0533 383.7739 232.2223 -4.0273 407.9286 411.9559 383.6591 233.8216 -4.0283 407.8604 411.8888 383.5477 235.4493 -4.0263 407.7779 411.8042 383.4218 237.0455 -4.0298 407.7129 411.7427 383.2828 238.6438 -4.0281 407.6204 411.6484 383.1436 240.2429 -4.0257 407.5215 411.5472 383.0057 241.8568 -4.0312 407.4434 411.4746 382.8827 243.4708 -4.0279 407.3519 411.3797 382.7314 245.0848 -4.0287 407.2812 411.3099 382.6012 246.6839 -4.0281 407.1905 411.2186 382.4590 248.2836 -4.0272 407.1054 411.1325 382.3176 249.8826 -4.0276 407.0043 411.0319 382.1796 251.5116 -4.0266 406.9136 410.9401 382.0410 253.1116 -4.0258 406.8316 410.8574 381.9128 254.7265 -4.0214 406.7590 410.7804 381.7670 256.3255 -4.0208 406.6620 410.6829 381.6123 257.9249 -4.0241 406.5572 410.5813 381.5090 259.5350 -4.0205 406.4714 410.4919 381.3623 261.1409 -4.0230 406.3765 410.3995 381.2288 262.7324 -4.0209 406.2902 410.3111 381.1138 264.3404 -4.0205 406.1949 410.2154 380.9711 265.9329 -4.0203 406.1070 410.1274 380.8348 267.5280 -4.0223 406.0137 410.0360 380.7060 269.1565 -4.0234 405.9164 409.9398 380.5709 270.7555 -4.0210 405.8147 409.8357 380.4634 272.3545 -4.0215 405.7174 409.7389 380.3291 273.9535 -4.0197 405.6255 409.6452 380.1938 275.5675 -4.0194 405.5317 409.5511 380.0825 277.1815 -4.0172 405.4369 409.4542 379.9604 278.7954 -4.0173 405.3284 409.3457 379.8280 280.3943 -4.0157 405.2265 409.2422 379.7051 281.9928 -4.0172 405.1423 409.1595 379.5687 283.6068 -4.0146 405.0455 409.0602 379.4472 285.2206 -4.0124 404.9384 408.9508 379.3184 286.8349 -4.0133 404.8428 408.8561 379.2076 288.4346 -4.0157 404.7343 408.7500 379.0854 290.0335 -4.0136 404.6333 408.6470 378.9653 291.6420 -4.0124 404.5417 408.5541 378.8456 293.2481 -4.0117 404.4377 408.4494 378.7248 294.8549 -4.0126 404.3361 408.3487 378.6142 296.4463 -4.0090 404.2275 408.2365 378.4860 298.0535 -4.0081 404.1508 408.1589 378.3717 299.6636 -4.0083 404.0180 408.0263 378.2423 301.2780 -4.0074 403.9177 407.9251 378.1216 302.8786 -4.0044 403.8277 407.8321 377.9963 304.4776 -4.0055 403.7190 407.7245 377.8823 306.0916 -4.0049 403.6111 407.6160 377.7698 307.6906 -4.0065 403.5056 407.5121 377.6434 309.3198 -4.0030 403.3883 407.3912 377.5074 310.9195 -4.0019 403.2836 407.2855 377.3716 312.5185 -4.0008 403.1890 407.1897 377.2426 314.1325 -3.9994 403.0717 407.0712 377.1067 315.7465 -3.9979 402.9569 406.9548 376.9522 317.3605 -3.9972 402.8628 406.8600 376.8230 318.9595 -3.9942 402.7619 406.7561 376.6699 320.5730 -3.9932 402.6525 406.6457 376.5326 322.1720 -3.9917 402.5534 406.5451 376.4053 323.7996 -3.9902 402.4442 406.4344 376.2594 325.3915 -3.9882 402.3388 406.3270 376.1269 326.9973 -3.9870 402.2187 406.2057 375.9855 328.5891 -3.9862 402.1245 406.1107 375.8344 330.1966 -3.9825 402.0171 405.9996 375.7017 331.8200 -3.9789 401.9084 405.8873 375.5674 333.4154 -3.9791 401.8060 405.7851 375.4236 335.0134 -3.9786 401.6784 405.6570 375.2968 336.6271 -3.9768 401.5760 405.5528 375.1627 338.2258 -3.9756 401.4635 405.4391 375.0300 339.8549 -3.9712 401.3422 405.3134 374.8948 341.4536 -3.9716 401.2404 405.2120 374.7495 343.0526 -3.9706 401.1292 405.0998 374.6185 344.6666 -3.9649 401.0130 404.9779 374.4937 346.2806 -3.9621 400.9093 404.8714 374.3595 347.8948 -3.9631 400.7884 404.7515 374.2271 349.4936 -3.9620 400.6747 404.6367 374.0992 351.1079 -3.9585 400.5791 404.5377 373.9547 352.7075 -3.9565 400.4568 404.4133 373.8230 354.3365 -3.9559 400.3209 404.2768 373.6964 355.9338 -3.9524 400.2224 404.1747 373.5512 357.5399 -3.9499 400.1153 404.0652 373.4416 359.1313 -3.9490 399.9910 403.9400 373.2797 360.7235 -3.9455 399.8745 403.8199 373.1593 362.3458 -3.9426 399.7629 403.7055 373.0452 363.9401 -3.9420 399.6420 403.5840 372.8957 365.5524 -3.9381 399.5174 403.4555 372.7678 367.1505 -3.9350 399.4121 403.3471 372.6500 368.7495 -3.9342 399.3107 403.2449 372.5184 370.3640 -3.9300 399.1831 403.1131 372.3927 371.9785 -3.9288 399.0683 402.9971 372.2600 373.5775 -3.9284 398.9529 402.8812 372.1368 375.1915 -3.9264 398.8327 402.7590 372.0090 376.7903 -3.9217 398.7106 402.6322 371.8832 378.4040 -3.9181 398.5880 402.5060 371.7659 380.0178 -3.9164 398.4838 402.4002 371.6401 381.6176 -3.9152 398.3777 402.2928 371.5092 383.2166 -3.9142 398.2535 402.1677 371.3885 384.8311 -3.9089 398.1281 402.0371 371.2667 386.4313 -3.9049 397.9967 401.9016 371.1468 388.0424 -3.9018 397.8910 401.7928 371.0285 389.6480 -3.9019 397.7820 401.6839 370.9031 391.2390 -3.8999 397.6628 401.5627 370.7947 392.8310 -3.8984 397.5396 401.4380 370.6898 394.4388 -3.8932 397.4131 401.3063 370.5674 396.0639 -3.8903 397.2983 401.1886 370.4455 397.6606 -3.8908 397.1820 401.0728 370.3313 399.2596 -3.8866 397.0585 400.9451 370.2090 400.8586 -3.8619 396.9372 400.7990 370.1055 402.4584 -3.8578 396.8233 400.6811 369.9975 404.0876 -3.8631 396.7090 400.5721 369.8614 405.7019 -3.8518 396.5943 400.4461 369.7343 407.3019 -3.8647 396.4710 400.3357 369.6086 408.9016 -3.8664 396.3657 400.2321 369.4716 410.5056 -3.8542 396.2388 400.0930 369.3420 412.1355 -3.8681 396.1162 399.9843 369.1887 413.7495 -3.8673 396.0001 399.8673 369.0452 415.3488 -3.8625 395.8685 399.7309 368.9081 416.9484 -3.8581 395.7517 399.6098 368.7663 418.5619 -3.8589 395.6400 399.4988 368.6207 420.1880 -3.8567 395.5104 399.3671 368.4505 421.7793 -3.8506 395.3919 399.2424 368.2831 423.3721 -3.8384 395.2690 399.1074 368.1543 424.9651 -3.8267 395.1549 398.9816 368.0161 426.5729 -3.8287 395.0332 398.8619 367.8873 428.1994 -3.8322 394.9168 398.7490 367.7563 429.7971 -3.8310 394.7820 398.6130 367.6493 431.3955 -3.8341 394.6676 398.5018 367.5169 432.9943 -3.8316 394.5441 398.3758 367.4069 434.6085 -3.8300 394.4162 398.2463 367.3000 436.2230 -3.8253 394.2948 398.1201 367.1913 437.8393 -3.8265 394.1865 398.0130 367.0784 439.4446 -3.8240 394.0551 397.8791 366.9544 441.0440 -3.8199 393.9250 397.7450 366.8364 442.6436 -3.8170 393.8097 397.6267 366.6964 444.2726 -3.8147 393.6735 397.4882 366.5775 445.8726 -3.7964 393.5557 397.3521 366.4415 447.4869 -3.8057 393.4472 397.2530 366.2953 449.0869 -3.8042 393.3267 397.1309 366.1675 450.6865 -3.7984 393.1917 396.9902 366.0367 452.3149 -3.7881 393.0601 396.8482 365.8964 453.9079 -3.7946 392.9712 396.7658 365.7598 455.5145 -3.7917 392.8360 396.6277 365.6234 457.1079 -3.7914 392.7007 396.4920 365.4917 458.7011 -3.7851 392.5835 396.3686 365.3615 460.3249 -3.7837 392.4539 396.2377 365.2157 461.9215 -3.7819 392.3404 396.1222 365.0894 463.5355 -3.7775 392.2125 395.9900 364.9568 465.1345 -3.7634 392.0875 395.8509 364.8290 466.7341 -3.7422 391.9561 395.6984 364.6894 468.3485 -3.7605 391.8438 395.6043 364.5573 469.9625 -3.7500 391.7271 395.4771 364.4253 471.5615 -3.7306 391.5924 395.3230 364.3001 473.1755 -3.7353 391.4624 395.1976 364.1691 474.7744 -3.7386 391.3464 395.0850 364.0432 476.3880 -3.7511 391.2130 394.9640 363.9185 478.0018 -3.7527 391.0919 394.8446 363.7802 479.6006 -3.7422 390.9683 394.7105 363.6459 481.2150 -3.7336 390.8437 394.5773 363.5208 482.8146 -3.7433 390.7170 394.4604 363.4117 484.4285 -3.7412 390.5954 394.3367 363.2660 486.0360 -3.7376 390.4701 394.2077 363.1467 487.6273 -3.7359 390.3406 394.0765 363.0318 489.2336 -3.7303 390.2122 393.9425 362.8946 490.8281 -3.7289 390.0934 393.8224 362.7701 492.4535 -3.7267 389.9591 393.6858 362.6441 494.0493 -3.7223 389.8435 393.5658 362.5277 495.6626 -3.7195 389.7100 393.4295 362.4083 497.2621 -3.7188 389.5938 393.3125 362.2914 498.8626 -3.7151 389.4626 393.1778 362.1746 500.4773 -3.7143 389.3310 393.0452 362.0362 502.0918 -3.7105 389.2121 392.9226 361.9116 503.6906 -3.7072 389.0832 392.7903 361.8017 505.3054 -3.7032 388.9515 392.6547 361.6675 506.9046 -3.7009 388.8356 392.5365 361.5504 508.5185 -3.6995 388.7047 392.4041 361.4216 510.1325 -3.6943 388.5830 392.2773 361.2958 511.7325 -3.6938 388.4550 392.1488 361.1530 513.3465 -3.6910 388.3297 392.0207 361.0083 514.9453 -3.6851 388.2045 391.8895 360.8751 516.5728 -3.6863 388.0804 391.7668 360.7281 518.1654 -3.6815 387.9370 391.6185 360.5854 519.7568 -3.6779 387.8292 391.5071 360.4333 521.3635 -3.6773 387.6920 391.3692 360.2783 522.9578 -3.6740 387.5755 391.2495 360.1439 524.5835 -3.6708 387.4494 391.1201 359.9858 526.1790 -3.6664 387.3361 391.0025 359.8390 527.7775 -3.6622 387.2045 390.8667 359.7012 529.3914 -3.6569 387.0722 390.7291 359.5653 530.9901 -3.6539 386.9446 390.5985 359.4376 532.6038 -3.6505 386.8126 390.4631 359.3156 534.2180 -3.6482 386.6841 390.3323 359.1927 535.8166 -3.6471 386.5756 390.2227 359.0714 537.4306 -3.6427 386.4341 390.0768 358.9640 539.0296 -3.6392 386.3044 389.9435 358.8426 540.6604 -3.6344 386.1636 389.7980 358.7468 542.2625 -3.6326 386.0506 389.6832 358.6363 543.8616 -3.6317 385.9291 389.5608 358.5012 545.4760 -3.6289 385.7965 389.4254 358.3851 547.0755 -3.6243 385.6735 389.2978 358.2602 548.6876 -3.6215 385.5363 389.1578 358.1365 550.2949 -3.6180 385.4122 389.0302 357.9951 551.8873 -3.6147 385.3077 388.9224 357.8568 553.4948 -3.6135 385.1712 388.7847 357.7155 555.0889 -3.6094 385.0442 388.6535 357.5983 556.7154 -3.6047 384.9008 388.5055 357.4437 558.3136 -3.6013 384.7813 388.3825 357.3066 559.9276 -3.5959 384.6606 388.2565 357.1796 561.5296 -3.5957 384.5307 388.1264 357.0370 563.1305 -3.5932 384.3890 387.9822 356.8909 564.7295 -3.5899 384.2797 387.8696 356.7602 566.3585 -3.5839 384.1514 387.7352 356.6233 567.9575 -3.5823 384.0103 387.5926 356.4980 569.5715 -3.5788 383.8869 387.4658 356.3511 571.1705 -3.5792 383.7606 387.3398 356.2243 572.7841 -3.5760 383.6226 387.1986 356.1055 574.3979 -3.5648 383.4998 387.0646 355.9623 576.0116 -3.5639 383.3777 386.9416 355.8120 577.6110 -3.5604 383.2378 386.7982 355.6944 579.2111 -3.5590 383.1162 386.6752 355.5708 580.8406 -3.5511 382.9764 386.5275 355.4324 582.4411 -3.5099 382.8578 386.3677 355.2971 584.0473 -3.5445 382.7438 386.2883 355.1751 585.6395 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