DTA measure 11.ólom Date: 2024313:130 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.32 s Mass = 1386.900 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1413 -0.6400 272.3941 273.0341 267.3011 1.9308 -0.6413 272.4483 273.0896 267.2861 2.7493 -0.6422 272.4830 273.1252 267.2742 3.5375 -0.6467 272.5242 273.1709 267.2737 4.3278 -0.6537 272.5730 273.2267 267.2707 5.1775 -0.6575 272.5942 273.2517 267.2721 5.9390 -0.6645 272.6312 273.2957 267.2872 6.7613 -0.6728 272.6742 273.3469 267.2939 7.5530 -0.6713 272.7133 273.3846 267.3093 8.3448 -0.6725 272.7539 273.4264 267.3468 9.1670 -0.6709 272.7914 273.4624 267.3926 9.9290 -0.6756 272.8362 273.5118 267.4268 10.7820 -0.6822 272.8883 273.5705 267.4778 11.5738 -0.6877 272.9221 273.6098 267.5377 12.3655 -0.6919 272.9632 273.6551 267.6353 13.1878 -0.6920 272.9853 273.6773 267.6835 13.9495 -0.6955 273.0371 273.7326 267.7505 14.8018 -0.7035 273.0816 273.7851 267.8511 15.5938 -0.7190 273.1226 273.8416 267.9687 16.3855 -0.7245 273.1426 273.8672 268.0603 17.2078 -0.7301 273.1772 273.9074 268.1696 17.9695 -0.7328 273.2311 273.9639 268.2720 18.8218 -0.7353 273.2895 274.0249 268.4182 19.5835 -0.7285 273.3162 274.0446 268.5408 20.4058 -0.7297 273.3610 274.0907 268.6619 21.2278 -0.7314 273.3861 274.1175 268.8023 21.9895 -0.7430 273.4224 274.1654 268.9197 22.8415 -0.7536 273.4700 274.2236 269.0614 23.6335 -0.7566 273.5149 274.2715 269.2163 24.4255 -0.7514 273.5395 274.2909 269.3469 25.2480 -0.7472 273.5691 274.3163 269.5062 26.0105 -0.7309 273.6081 274.3390 269.6298 26.8630 -0.7217 273.6429 274.3646 269.7962 27.6555 -0.7308 273.6920 274.4228 269.9426 28.4483 -0.7459 273.7218 274.4677 270.0860 29.2670 -0.7533 273.7625 274.5158 270.2380 30.0250 -0.7547 273.8097 274.5645 270.3765 30.8730 -0.7595 273.8460 274.6054 270.5357 31.6610 -0.7669 273.8906 274.6575 270.6858 32.4490 -0.7733 273.9474 274.7208 270.8308 33.2673 -0.7796 273.9651 274.7447 270.9757 34.0560 -0.7818 274.0029 274.7847 271.1150 34.8753 -0.7860 274.0489 274.8350 271.2743 35.6643 -0.7914 274.0829 274.8742 271.4292 36.4540 -0.7972 274.1257 274.9229 271.5582 37.2728 -0.7972 274.1671 274.9644 271.7161 38.0635 -0.7987 274.2184 275.0171 271.8527 38.8855 -0.7934 274.2457 275.0391 272.0047 39.6775 -0.7924 274.2806 275.0730 272.1506 40.4695 -0.7974 274.3190 275.1164 272.2874 41.2915 -0.8045 274.3636 275.1681 272.4367 42.0835 -0.8122 274.4038 275.2160 272.5502 42.9055 -0.8150 274.4421 275.2570 272.6967 43.6975 -0.8204 274.4831 275.3034 272.8417 44.4895 -0.8247 274.5221 275.3468 272.9890 45.3115 -0.8354 274.5630 275.3984 273.1085 46.1035 -0.8465 274.6060 275.4526 273.2288 46.9253 -0.8547 274.6509 275.5055 273.3522 47.7175 -0.8628 274.6911 275.5539 273.4736 48.5095 -0.8685 274.7258 275.5942 273.6014 49.3325 -0.8739 274.7831 275.6570 273.7332 50.1253 -0.8785 274.8398 275.7184 273.8456 50.9480 -0.8837 274.8892 275.7730 273.9875 51.7403 -0.8882 274.9107 275.7989 274.0977 52.5315 -0.8938 274.9598 275.8536 274.2175 53.3540 -0.8986 275.0041 275.9027 274.3303 54.1458 -0.9036 275.0578 275.9614 274.4428 54.9678 -0.9081 275.0882 275.9964 274.5432 55.7598 -0.9115 275.1314 276.0429 274.6527 56.5515 -0.9183 275.1755 276.0937 274.7717 57.4050 -0.9231 275.2393 276.1624 274.8945 58.1665 -0.9261 275.2687 276.1948 275.0070 58.9888 -0.9294 275.3096 276.2391 275.1281 59.8108 -0.9354 275.3587 276.2940 275.2671 60.5718 -0.9393 275.4175 276.3567 275.3928 61.4200 -0.9443 275.4551 276.3995 275.5149 62.1780 -0.9498 275.4882 276.4381 275.6283 62.9960 -0.9463 275.5407 276.4871 275.7480 63.7843 -0.9401 275.5933 276.5334 275.8756 64.5760 -0.9411 275.6426 276.5837 275.9976 65.4255 -0.9430 275.6933 276.6363 276.1161 66.1840 -0.9508 275.7273 276.6781 276.2383 67.0030 -0.9522 275.7821 276.7343 276.3789 67.7913 -0.9570 275.8349 276.7918 276.5031 68.5808 -0.9640 275.8770 276.8410 276.6159 69.4318 -0.9669 275.9370 276.9039 276.7272 70.1935 -0.9735 275.9761 276.9496 276.8826 71.0158 -0.9802 276.0284 277.0086 276.9995 71.8073 -0.9818 276.0874 277.0692 277.1107 72.5985 -0.9890 276.1478 277.1368 277.2447 73.4205 -1.0123 276.1980 277.2104 277.3752 74.2125 -1.0252 276.2439 277.2692 277.5155 75.0348 -1.0324 276.2776 277.3100 277.6660 75.8268 -1.0435 276.3439 277.3874 277.7810 76.6185 -1.0491 276.3793 277.4284 277.9126 77.4405 -1.0561 276.4205 277.4766 278.0515 78.2325 -1.0597 276.4853 277.5450 278.1914 79.0555 -1.0671 276.5447 277.6119 278.3244 79.8478 -1.0653 276.5860 277.6513 278.4633 80.6395 -1.0681 276.6642 277.7323 278.6129 81.4615 -1.0724 276.7030 277.7755 278.7609 82.2538 -1.0752 276.7480 277.8232 278.8794 83.0755 -1.0770 276.8214 277.8984 279.0224 83.8678 -1.0812 276.8715 277.9527 279.1684 84.6630 -1.0815 276.9248 278.0063 279.2912 85.4925 -1.0630 276.9923 278.0553 279.4234 86.2545 -1.0689 277.0340 278.1028 279.5551 87.1070 -1.0643 277.0868 278.1511 279.7154 87.8995 -1.0648 277.1424 278.2072 279.8548 88.6925 -1.0701 277.1990 278.2690 279.9863 89.5145 -1.0718 277.2689 278.3406 280.1409 90.2765 -1.0769 277.3262 278.4031 280.2693 91.1283 -1.0803 277.3754 278.4557 280.4335 91.9200 -1.0891 277.4198 278.5089 280.5550 92.7115 -1.1033 277.4730 278.5763 280.6984 93.5338 -1.0982 277.5423 278.6405 280.8274 94.2920 -1.0948 277.5980 278.6928 280.9496 95.1398 -1.0980 277.6626 278.7607 281.0872 95.8973 -1.1001 277.7368 278.8369 281.2329 96.7155 -1.1051 277.8093 278.9144 281.3649 97.5333 -1.1078 277.8684 278.9761 281.5135 98.2910 -1.1077 277.9099 279.0176 281.6260 99.1390 -1.1107 277.9764 279.0871 281.7600 99.8975 -1.1156 278.0468 279.1625 281.8765 100.7168 -1.1187 278.1027 279.2214 282.0213 101.5350 -1.1312 278.1673 279.2985 282.1700 102.3255 -1.1408 278.2239 279.3647 282.2996 103.1473 -1.1482 278.2884 279.4366 282.4096 103.9385 -1.1447 278.3532 279.4978 282.5386 104.7300 -1.1459 278.4217 279.5677 282.6784 105.5523 -1.1548 278.4827 279.6375 282.8081 106.3143 -1.1592 278.5430 279.7022 282.9277 107.1665 -1.1621 278.6115 279.7735 283.0699 107.9583 -1.1641 278.6627 279.8269 283.1917 108.7495 -1.1695 278.7195 279.8889 283.3143 109.5723 -1.1728 278.7899 279.9627 283.4586 110.3338 -1.1798 278.8427 280.0225 283.5787 111.1860 -1.1836 278.9254 280.1090 283.7030 111.9783 -1.1794 278.9934 280.1728 283.8013 112.7715 -1.1754 279.0770 280.2524 283.9409 113.5938 -1.1775 279.1297 280.3072 284.0603 114.3555 -1.1766 279.1901 280.3667 284.1715 115.2078 -1.1671 279.2562 280.4233 284.2998 115.9998 -1.1634 279.3314 280.4949 284.4243 116.7915 -1.1684 279.4031 280.5715 284.5489 117.6138 -1.1736 279.4675 280.6410 284.6775 118.3755 -1.1732 279.5354 280.7086 284.7922 119.2278 -1.1756 279.6174 280.7930 284.9086 120.0198 -1.1770 279.6700 280.8470 285.0321 120.8125 -1.1790 279.7615 280.9405 285.1532 121.6348 -1.1826 279.8142 280.9968 285.2752 122.4265 -1.1840 279.8811 281.0652 285.3946 123.2495 -1.1848 279.9608 281.1456 285.5322 124.0418 -1.1859 280.0290 281.2149 285.6347 124.8335 -1.1888 280.1059 281.2947 285.7382 125.6553 -1.1905 280.1729 281.3634 285.8574 126.4435 -1.1923 280.2353 281.4276 285.9857 127.2620 -1.1953 280.3090 281.5043 286.1031 128.0500 -1.1986 280.3847 281.5833 286.2157 128.8390 -1.1982 280.4565 281.6547 286.3339 129.6573 -1.2001 280.5237 281.7238 286.4409 130.4460 -1.2019 280.5993 281.8012 286.5531 131.2648 -1.2038 280.6710 281.8748 286.6868 132.0530 -1.2050 280.7549 281.9599 286.8140 132.8420 -1.2082 280.8403 282.0485 286.9386 133.6908 -1.2126 280.9044 282.1170 287.0691 134.4518 -1.2155 280.9710 282.1866 287.1910 135.2733 -1.2168 281.0561 282.2729 287.3308 136.0948 -1.2179 281.1374 282.3553 287.4463 136.8565 -1.2172 281.2026 282.4198 287.5611 137.7088 -1.2196 281.2815 282.5011 287.7250 138.4705 -1.2235 281.3667 282.5902 287.8493 139.2925 -1.2255 281.4314 282.6569 287.9910 140.1148 -1.2275 281.5149 282.7424 288.1325 140.8765 -1.2279 281.5815 282.8094 288.2325 141.7285 -1.2295 281.6574 282.8869 288.3772 142.4905 -1.2302 281.7381 282.9683 288.5062 143.3125 -1.2320 281.8296 283.0615 288.6372 144.1345 -1.2343 281.8925 283.1268 288.7826 144.8965 -1.2359 281.9533 283.1892 288.8847 145.7485 -1.2394 282.0558 283.2952 289.0343 146.5405 -1.2445 282.1332 283.3777 289.1678 147.3323 -1.2475 282.2109 283.4585 289.2918 148.1545 -1.2535 282.2913 283.5448 289.4232 148.9163 -1.2588 282.3674 283.6262 289.5518 149.7680 -1.2592 282.4621 283.7214 289.6784 150.5603 -1.2618 282.5448 283.8066 289.8025 151.3528 -1.2645 282.6161 283.8806 289.9169 152.1750 -1.2661 282.6964 283.9626 290.0591 152.9365 -1.2712 282.7775 284.0487 290.1776 153.7888 -1.2705 282.8510 284.1215 290.3128 154.5808 -1.2647 282.9331 284.1978 290.4391 155.4028 -1.2640 283.0295 284.2935 290.5885 156.3150 -1.2718 283.1145 284.3863 290.7240 157.0765 -1.2733 283.1786 284.4519 290.8304 157.9873 -1.2771 283.2843 284.5614 290.9740 158.8350 -1.2763 283.3702 284.6465 291.1196 159.7430 -1.2761 283.4678 284.7439 291.2660 160.5010 -1.2768 283.5592 284.8360 291.3829 161.3190 -1.2787 283.6472 284.9259 291.5080 162.1370 -1.2810 283.7370 285.0180 291.6621 162.8950 -1.2846 283.8207 285.1054 291.7850 163.7430 -1.2824 283.9154 285.1978 291.9177 164.5010 -1.2838 283.9854 285.2692 292.0493 165.3198 -1.2864 284.0577 285.3441 292.2000 166.1393 -1.2888 284.1434 285.4322 292.3399 166.9000 -1.2926 284.2312 285.5238 292.4903 167.7520 -1.2939 284.3280 285.6220 292.6249 168.5728 -1.2933 284.4214 285.7147 292.7862 169.4848 -1.2951 284.5253 285.8204 292.9564 170.3068 -1.2946 284.6148 285.9094 293.0941 171.1288 -1.2957 284.7132 286.0089 293.2502 171.8908 -1.2913 284.8058 286.0971 293.3805 172.7428 -1.2873 284.8954 286.1828 293.5456 173.5045 -1.2885 284.9622 286.2507 293.6861 174.3268 -1.2880 285.0424 286.3303 293.8347 175.1488 -1.2889 285.1190 286.4079 293.9895 175.9105 -1.2905 285.2128 286.5033 294.1169 176.7628 -1.2924 285.3093 286.6016 294.2549 177.5245 -1.2928 285.4091 286.7019 294.3856 178.3468 -1.2939 285.5145 286.8084 294.5113 179.1388 -1.2964 285.6035 286.8999 294.6394 179.9305 -1.2984 285.6818 286.9802 294.7500 180.7828 -1.2979 285.7794 287.0773 294.8932 181.5445 -1.2998 285.8736 287.1734 295.0051 182.3673 -1.3023 285.9640 287.2663 295.1327 183.1595 -1.3029 286.0610 287.3638 295.2401 183.9515 -1.3047 286.1606 287.4653 295.3677 184.8040 -1.3085 286.2487 287.5572 295.4913 185.5665 -1.3087 286.3278 287.6365 295.6065 186.3885 -1.3102 286.4136 287.7237 295.7281 187.1805 -1.3105 286.5113 287.8218 295.8364 187.9725 -1.3118 286.6131 287.9249 295.9496 188.8245 -1.3210 286.7355 288.0564 296.0666 189.5855 -1.3238 286.8130 288.1368 296.1731 190.4020 -1.3275 286.8879 288.2155 296.3089 191.1890 -1.3300 286.9710 288.3009 296.4266 192.0975 -1.3291 287.0866 288.4157 296.5730 193.0063 -1.3292 287.2012 288.5305 296.7252 193.8250 -1.3305 287.3102 288.6407 296.8627 194.6430 -1.3339 287.4140 288.7478 296.9788 195.4310 -1.3319 287.5026 288.8345 297.1061 196.2190 -1.3314 287.5839 288.9153 297.2361 197.0675 -1.3339 287.6834 289.0174 297.3624 197.8285 -1.3375 287.7782 289.1157 297.5048 198.7390 -1.3390 287.8886 289.2276 297.6586 199.5598 -1.3390 287.9973 289.3363 297.7835 200.3515 -1.3354 288.0912 289.4266 297.9416 201.1735 -1.3335 288.2044 289.5379 298.0848 201.9355 -1.3337 288.2867 289.6205 298.2107 202.7875 -1.3303 288.3871 289.7174 298.3557 203.5495 -1.3338 288.4884 289.8222 298.4789 204.3715 -1.3346 288.6031 289.9378 298.6181 205.1935 -1.3353 288.6757 290.0110 298.7557 205.9555 -1.3374 288.7774 290.1148 298.8829 206.8073 -1.3407 288.8820 290.2228 299.0155 207.5693 -1.3402 288.9746 290.3148 299.1385 208.3908 -1.3405 289.0689 290.4094 299.2819 209.2128 -1.3415 289.1786 290.5201 299.4136 209.9745 -1.3395 289.2884 290.6279 299.5425 210.8268 -1.3400 289.3895 290.7295 299.6805 211.5885 -1.3429 289.4979 290.8408 299.8144 212.4108 -1.3415 289.5771 290.9186 299.9368 213.2328 -1.3465 289.6797 291.0263 300.0845 213.9945 -1.3462 289.7715 291.1176 300.2095 214.8468 -1.3469 289.8839 291.2308 300.3404 215.6085 -1.3458 289.9728 291.3186 300.4668 216.4308 -1.3453 290.0882 291.4334 300.6271 217.2528 -1.3475 290.1950 291.5425 300.7450 218.0150 -1.3493 290.2796 291.6288 300.8756 218.8678 -1.3516 290.3961 291.7477 300.9893 219.6598 -1.3510 290.4922 291.8432 301.1134 220.4525 -1.3532 290.6042 291.9575 301.2418 221.2748 -1.3538 290.7055 292.0593 301.3825 222.0365 -1.3519 290.8022 292.1541 301.5037 222.8878 -1.3527 290.9215 292.2742 301.6293 223.6760 -1.3551 291.0161 292.3712 301.7487 224.4640 -1.3586 291.1168 292.4754 301.8871 225.2820 -1.3600 291.2313 292.5914 302.0078 226.0700 -1.3641 291.3290 292.6931 302.1458 226.8888 -1.3664 291.4373 292.8038 302.2596 227.6770 -1.3672 291.5396 292.9067 302.3889 228.4660 -1.3718 291.6573 293.0291 302.5051 229.2848 -1.3732 291.7564 293.1296 302.6345 230.0743 -1.3713 291.8603 293.2316 302.7543 230.8945 -1.3713 291.9623 293.3336 302.8865 231.6848 -1.3725 292.0720 293.4445 303.0117 232.4755 -1.3736 292.1777 293.5512 303.1324 233.3278 -1.3729 292.2892 293.6620 303.2599 234.0895 -1.3755 292.3888 293.7643 303.3711 234.9115 -1.3771 292.4930 293.8702 303.5179 235.7038 -1.3748 292.6051 293.9799 303.6283 236.4955 -1.3742 292.7130 294.0871 303.7511 237.3175 -1.3796 292.8297 294.2093 303.8825 238.1095 -1.3802 292.9479 294.3281 304.0142 238.9315 -1.3804 293.0448 294.4252 304.1449 239.7235 -1.3834 293.1370 294.5204 304.2868 240.5155 -1.3829 293.2425 294.6254 304.4268 241.3375 -1.3851 293.3472 294.7323 304.5724 242.1295 -1.3862 293.4663 294.8525 304.7104 242.9515 -1.3885 293.5780 294.9666 304.8565 243.7435 -1.3886 293.6838 295.0725 304.9934 244.5355 -1.3897 293.8010 295.1907 305.1231 245.3575 -1.3914 293.9038 295.2951 305.2822 246.1495 -1.3938 294.0095 295.4033 305.4264 246.9715 -1.3950 294.1155 295.5105 305.5455 247.7635 -1.3943 294.2288 295.6231 305.6718 248.5553 -1.3980 294.3345 295.7324 305.8203 249.3775 -1.3983 294.4373 295.8356 305.9796 250.1688 -1.3979 294.5448 295.9427 306.1156 250.9915 -1.3996 294.6671 296.0667 306.2630 251.7838 -1.4015 294.7847 296.1863 306.4024 252.5755 -1.4011 294.8812 296.2823 306.5399 253.3978 -1.4048 295.0049 296.4097 306.6834 254.1895 -1.4077 295.1076 296.5154 306.8143 255.0090 -1.4074 295.2373 296.6447 306.9772 255.7973 -1.4098 295.3442 296.7539 307.1111 256.5850 -1.4091 295.4460 296.8551 307.2397 257.4030 -1.4096 295.5640 296.9736 307.3830 258.1910 -1.4135 295.6987 297.1122 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