DTA measure 21.ólom Date: 2024313:1330 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.47 s Mass = 1386.900 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4898 -5.0410 440.9661 446.0071 424.5657 4.1186 -5.0480 440.9733 446.0212 424.5293 5.7328 -5.0552 440.9895 446.0448 424.4953 7.3316 -5.0628 441.0224 446.0852 424.4375 8.9310 -5.0699 441.0363 446.1062 424.3557 10.5476 -5.0798 441.0483 446.1281 424.2512 12.1766 -5.0858 441.0636 446.1493 424.1166 13.7766 -5.0933 441.0767 446.1700 423.9681 15.3765 -5.0980 441.0801 446.1780 423.7970 16.9755 -5.1023 441.1015 446.2038 423.6184 18.5885 -5.1075 441.1064 446.2139 423.4078 20.1958 -5.1108 441.1137 446.2245 423.1790 21.8020 -5.1164 441.1131 446.2295 422.9754 23.3933 -5.1192 441.1133 446.2325 422.7501 25.0005 -5.1223 441.1116 446.2338 422.5226 26.6089 -5.1260 441.1163 446.2423 422.2994 28.2196 -5.1275 441.1237 446.2512 422.0672 29.8083 -5.1311 441.1104 446.2415 421.8552 31.4315 -5.1334 441.1092 446.2426 421.6179 33.0305 -5.1365 441.1108 446.2473 421.3985 34.6295 -5.1378 441.0851 446.2228 421.1745 36.2585 -5.1378 441.0820 446.2198 420.9689 37.8575 -5.1409 441.0569 446.1977 420.7549 39.4716 -5.1414 441.0383 446.1797 420.5370 41.0711 -5.1442 441.0297 446.1739 420.3190 42.6698 -5.1477 441.0017 446.1495 420.1206 44.2836 -5.1485 440.9730 446.1214 419.8890 45.8979 -5.1462 440.9451 446.0914 419.6895 47.4966 -5.1491 440.9129 446.0620 419.4829 49.1110 -5.1510 440.8872 446.0381 419.2794 50.7161 -5.1505 440.8682 446.0187 419.0896 52.3100 -5.1504 440.8184 445.9688 418.9005 53.9161 -5.1524 440.7753 445.9277 418.7128 55.5241 -5.1539 440.7412 445.8951 418.5287 57.1173 -5.1526 440.7068 445.8593 418.3341 58.7110 -5.1527 440.6562 445.8089 418.1433 60.3234 -5.1527 440.6222 445.7750 417.9691 61.9348 -5.1524 440.5538 445.7062 417.7938 63.5338 -5.1572 440.5130 445.6703 417.5959 65.1476 -5.1575 440.4676 445.6252 417.4123 66.7466 -5.1567 440.4016 445.5583 417.2266 68.3456 -5.1596 440.3489 445.5085 417.0430 69.9746 -5.1627 440.3049 445.4676 416.8470 71.5736 -5.1610 440.2476 445.4086 416.6423 73.1878 -5.1592 440.1867 445.3459 416.4299 74.7875 -5.1607 440.1249 445.2856 416.2309 76.3865 -5.1620 440.0435 445.2055 416.0200 78.0154 -5.1620 439.9875 445.1496 415.8286 79.6145 -5.1577 439.9162 445.0740 415.6228 81.2174 -5.1590 439.8590 445.0180 415.4139 82.8346 -5.1611 439.7818 444.9430 415.2119 84.4286 -5.1602 439.7167 444.8768 415.0314 86.0350 -5.1606 439.6457 444.8063 414.8377 87.6414 -5.1589 439.5675 444.7264 414.6393 89.2480 -5.1594 439.5002 444.6596 414.4373 90.8401 -5.1588 439.4061 444.5648 414.2354 92.4498 -5.1603 439.3198 444.4802 414.0283 94.0624 -5.1617 439.2439 444.4056 413.8204 95.6761 -5.1583 439.1598 444.3181 413.5976 97.2750 -5.1588 439.0716 444.2304 413.3807 98.8736 -5.1589 438.9758 444.1347 413.1694 100.4879 -5.1560 438.8881 444.0440 412.9511 102.1018 -5.1577 438.8011 443.9589 412.7391 103.7158 -5.1554 438.7190 443.8743 412.5204 105.3146 -5.1545 438.6210 443.7755 412.3059 106.9136 -5.1532 438.5315 443.6847 412.0969 108.5276 -5.1522 438.4306 443.5828 411.8870 110.1568 -5.1532 438.3071 443.4603 411.6898 111.7575 -5.1524 438.2133 443.3656 411.4889 113.3565 -5.1495 438.1120 443.2615 411.2690 114.9704 -5.1504 438.0130 443.1634 411.0771 116.5691 -5.1452 437.9074 443.0527 410.8790 118.1760 -5.1440 437.8272 442.9711 410.6813 119.7821 -5.1423 437.6986 442.8409 410.4910 121.3744 -5.1423 437.5836 442.7259 410.3057 122.9703 -5.1409 437.4673 442.6082 410.1073 124.5796 -5.1408 437.3714 442.5122 409.9213 126.1925 -5.1398 437.2514 442.3912 409.7376 127.7915 -5.1386 437.1331 442.2718 409.5609 129.4056 -5.1390 437.0145 442.1535 409.3731 131.0045 -5.1365 436.9073 442.0438 409.1694 132.6104 -5.1361 436.7703 441.9064 408.9589 134.2115 -5.1359 436.6602 441.7961 408.7589 135.8254 -5.1305 436.5406 441.6711 408.5532 137.4393 -5.1298 436.4294 441.5592 408.3561 139.0381 -5.1283 436.3168 441.4451 408.1519 140.6368 -5.1271 436.1931 441.3202 407.9311 142.2509 -5.1258 436.0564 441.1822 407.7139 143.8654 -5.1217 435.9278 441.0496 407.4923 145.4648 -5.1222 435.8059 440.9281 407.2907 147.0785 -5.1210 435.6726 440.7935 407.0910 148.6721 -5.1194 435.5321 440.6515 406.8925 150.2630 -5.1169 435.3924 440.5093 406.7048 151.8840 -5.1139 435.2713 440.3852 406.4891 153.4771 -5.1137 435.1385 440.2522 406.2796 155.0855 -5.1121 435.0225 440.1346 406.0850 156.6818 -5.1085 434.8823 439.9908 405.8817 158.2798 -5.1056 434.7328 439.8384 405.6827 159.9086 -5.1024 434.5920 439.6944 405.4942 161.5078 -5.1006 434.4704 439.5711 405.2968 163.1114 -5.0994 434.3356 439.4351 405.0934 164.7146 -5.0993 434.2032 439.3025 404.9090 166.3286 -5.0970 434.0513 439.1483 404.7013 167.9276 -5.0936 433.9076 439.0012 404.4976 169.5566 -5.0909 433.7636 438.8545 404.3007 171.1565 -5.0891 433.6162 438.7054 404.0789 172.7555 -5.0878 433.4855 438.5733 403.8696 174.3700 -5.0856 433.3463 438.4319 403.6609 175.9695 -5.0836 433.2003 438.2838 403.4500 177.5991 -5.0793 433.0501 438.1294 403.2135 179.1976 -5.0763 432.8908 437.9671 402.9866 180.8053 -5.0726 432.7381 437.8108 402.7692 182.3963 -5.0690 432.5991 437.6680 402.5582 184.0029 -5.0660 432.4515 437.5175 402.3310 185.6088 -5.0613 432.3061 437.3674 402.1239 187.2173 -5.0601 432.1419 437.2020 401.9100 188.8145 -5.0577 431.9895 437.0472 401.6772 190.4135 -5.0549 431.8568 436.9117 401.4804 192.0425 -5.0500 431.6876 436.7377 401.2589 193.6451 -5.0469 431.5306 436.5775 401.0565 195.2503 -5.0454 431.3777 436.4231 400.8476 196.8638 -5.0424 431.2059 436.2483 400.6392 198.4629 -5.0377 431.0502 436.0879 400.4348 200.0768 -5.0342 430.8742 435.9084 400.2277 201.6909 -5.0305 430.7358 435.7663 400.0261 203.3046 -5.0277 430.5756 435.6033 399.8090 204.9036 -5.0239 430.4086 435.4325 399.6159 206.5026 -5.0226 430.2535 435.2761 399.4160 208.1166 -5.0176 430.0893 435.1070 399.2109 209.7306 -5.0135 429.9156 434.9291 399.0077 211.3448 -5.0113 429.7475 434.7588 398.8085 212.9419 -5.0076 429.5910 434.5986 398.6017 214.5330 -5.0027 429.4434 434.4461 398.4169 216.1401 -4.9999 429.2761 434.2759 398.2164 217.7480 -4.9993 429.0987 434.0981 398.0378 219.3405 -4.9966 428.9498 433.9464 397.8447 220.9339 -4.9928 428.7807 433.7735 397.6548 222.5466 -4.9917 428.6123 433.6040 397.4595 224.1456 -4.9916 428.4312 433.4228 397.2889 225.7596 -4.9855 428.2612 433.2467 397.0842 227.3585 -4.9836 428.0959 433.0795 396.8827 228.9725 -4.9813 427.9336 432.9148 396.6963 230.5715 -4.9773 427.7576 432.7348 396.4827 232.1705 -4.9742 427.5962 432.5703 396.2765 233.7845 -4.9723 427.4159 432.3882 396.0624 235.3985 -4.9659 427.2474 432.2133 395.8482 236.9973 -4.9628 427.0747 432.0376 395.6349 238.6108 -4.9598 426.9086 431.8684 395.4233 240.2101 -4.9554 426.7424 431.6978 395.2236 241.8103 -4.9511 426.5633 431.5144 395.0296 243.4405 -4.9474 426.3774 431.3248 394.8014 245.0371 -4.9434 426.2091 431.1525 394.5880 246.6289 -4.9377 426.0363 430.9740 394.3842 248.2216 -4.9382 425.8764 430.8145 394.1752 249.8288 -4.9336 425.7096 430.6431 393.9721 251.4525 -4.9285 425.5280 430.4565 393.7748 253.0474 -4.9247 425.3566 430.2813 393.5694 254.6459 -4.9204 425.1630 430.0834 393.3610 256.2448 -4.9115 424.9852 429.8967 393.1568 257.8586 -4.9089 424.8190 429.7279 392.9495 259.4726 -4.9057 424.6391 429.5448 392.7438 261.0868 -4.9042 424.4665 429.3707 392.5419 262.6856 -4.8977 424.2812 429.1789 392.3471 264.2846 -4.8939 424.1050 428.9988 392.1621 265.8986 -4.8856 423.9255 428.8111 391.9579 267.5126 -4.8836 423.7457 428.6294 391.7423 269.1265 -4.8800 423.5576 428.4376 391.5315 270.7255 -4.8768 423.3836 428.2603 391.2973 272.3245 -4.8716 423.2025 428.0742 391.0855 273.9385 -4.8694 423.0213 427.8907 390.8633 275.5675 -4.8629 422.8406 427.7035 390.6385 277.1625 -4.8570 422.6576 427.5146 390.4118 278.7535 -4.8512 422.4768 427.3280 390.1841 280.3596 -4.8485 422.2882 427.1367 389.9578 281.9668 -4.8453 422.1084 426.9537 389.7347 283.5744 -4.8396 421.9321 426.7717 389.5177 285.1851 -4.8351 421.7399 426.5750 389.2844 286.7745 -4.8301 421.5576 426.3877 389.0664 288.3885 -4.8273 421.3774 426.2048 388.8450 289.9875 -4.8232 421.1931 426.0164 388.6321 291.6165 -4.8163 420.9983 425.8146 388.4166 293.2153 -4.8141 420.8054 425.6194 388.2116 294.8138 -4.8106 420.6230 425.4336 388.0026 296.4290 -4.7984 420.4463 425.2447 387.8059 298.0286 -4.7943 420.2584 425.0528 387.6194 299.6578 -4.7910 420.0609 424.8519 387.4252 301.2566 -4.7834 419.8781 424.6615 387.2544 302.8706 -4.7774 419.6858 424.4631 387.0506 304.4696 -4.7756 419.5114 424.2870 386.8748 306.0843 -4.7704 419.3187 424.0891 386.6745 307.6988 -4.7670 419.1223 423.8893 386.4806 309.2941 -4.7612 418.9455 423.7067 386.2883 310.8860 -4.7548 418.7427 423.4976 386.0930 312.4920 -4.7515 418.5668 423.3183 385.8899 314.0986 -4.7453 418.3860 423.1313 385.6915 315.7066 -4.7385 418.1753 422.9138 385.4819 317.3016 -4.7339 417.9853 422.7192 385.2825 318.8996 -4.7324 417.8187 422.5511 385.1028 320.5136 -4.7273 417.6247 422.3520 384.9034 322.1125 -4.7217 417.4310 422.1527 384.7045 323.7266 -4.7184 417.2377 421.9561 384.5069 325.3258 -4.7122 417.0439 421.7560 384.3004 326.9405 -4.7084 416.8665 421.5748 384.0812 328.5395 -4.7050 416.6563 421.3613 383.8639 330.1385 -4.6981 416.4781 421.1762 383.6446 331.7525 -4.6902 416.2870 420.9772 383.4321 333.3665 -4.6876 416.0874 420.7749 383.2196 334.9651 -4.6816 415.9054 420.5871 383.0075 336.5786 -4.6773 415.7135 420.3908 382.7751 338.1776 -4.6752 415.5236 420.1988 382.5584 339.7918 -4.6682 415.3338 420.0020 382.3441 341.4050 -4.6608 415.1448 419.8055 382.1327 342.9973 -4.6566 414.9460 419.6026 381.8960 344.6031 -4.6518 414.7487 419.4005 381.6855 346.1948 -4.6486 414.5603 419.2089 381.4607 347.8041 -4.6428 414.3588 419.0016 381.2595 349.4134 -4.6394 414.1696 418.8090 381.0520 351.0103 -4.6341 413.9842 418.6183 380.8286 352.6236 -4.6282 413.7856 418.4138 380.5998 354.2239 -4.6258 413.5995 418.2254 380.3905 355.8236 -4.6201 413.3988 418.0189 380.1854 357.4529 -4.6147 413.1989 417.8136 379.9615 359.0516 -4.6090 412.9936 417.6026 379.7592 360.6506 -4.6012 412.8151 417.4163 379.5446 362.2646 -4.5962 412.6174 417.2135 379.3295 363.8636 -4.5904 412.4375 417.0279 379.1164 365.4928 -4.5847 412.2303 416.8150 378.9078 367.0916 -4.5794 412.0242 416.6035 378.6970 368.6915 -4.5727 411.8300 416.4027 378.4825 370.3068 -4.5673 411.6268 416.1942 378.2844 371.9065 -4.5602 411.4358 415.9960 378.0924 373.5340 -4.5580 411.2379 415.7959 377.8812 375.1261 -4.5528 411.0319 415.5846 377.6677 376.7183 -4.5446 410.8584 415.4030 377.4709 378.3250 -4.5403 410.6484 415.1887 377.2730 379.9316 -4.5348 410.4489 414.9837 377.0783 381.5396 -4.5312 410.2581 414.7893 376.8763 383.1525 -4.5260 410.0590 414.5850 376.6775 384.7515 -4.5213 409.8651 414.3863 376.4697 386.3505 -4.5193 409.6552 414.1745 376.2620 387.9645 -4.5158 409.4610 413.9768 376.0641 389.5785 -4.5094 409.2646 413.7740 375.8597 391.1925 -4.5065 409.0778 413.5843 375.6564 392.7909 -4.5011 408.8749 413.3761 375.4860 394.3899 -4.4928 408.6723 413.1652 375.2954 396.0186 -4.4898 408.4742 412.9640 375.0975 397.6178 -4.4844 408.2816 412.7659 374.8926 399.2319 -4.4789 408.0837 412.5626 374.7056 400.8316 -4.4725 407.8746 412.3471 374.4904 402.4464 -4.4690 407.6777 412.1467 374.2729 404.0606 -4.4646 407.4701 411.9347 374.0693 405.6725 -4.4581 407.2800 411.7381 373.8685 407.2631 -4.4559 407.0859 411.5417 373.6556 408.8561 -4.4508 406.8893 411.3401 373.4451 410.4638 -4.4440 406.6763 411.1202 373.2189 412.0881 -4.4374 406.4837 410.9211 372.9958 413.6838 -4.4339 406.2812 410.7151 372.7920 415.2803 -4.4265 406.0923 410.5188 372.5891 416.8936 -4.4224 405.8803 410.3026 372.3634 418.4940 -4.4146 405.6873 410.1018 372.1399 420.1146 -4.4082 405.4860 409.8943 371.9209 421.7138 -4.4043 405.2924 409.6967 371.7111 423.3276 -4.4006 405.0886 409.4893 371.5009 424.9265 -4.3918 404.9025 409.2943 371.2732 426.5405 -4.3785 404.6951 409.0736 371.0710 428.1545 -4.3738 404.4983 408.8721 370.8601 429.7685 -4.3716 404.2954 408.6670 370.6282 431.3674 -4.3664 404.0898 408.4562 370.4207 432.9663 -4.3608 403.8850 408.2458 370.2077 434.5798 -4.3551 403.6919 408.0470 370.0058 436.2088 -4.3482 403.4974 407.8457 369.7995 437.8060 -4.3414 403.2966 407.6380 369.5942 439.3983 -4.3395 403.0889 407.4285 369.3845 441.0053 -4.3336 402.8960 407.2296 369.1773 442.5983 -4.3292 402.6844 407.0136 368.9604 444.2234 -4.3224 402.4949 406.8173 368.7663 445.8210 -4.3161 402.2859 406.6020 368.5629 447.4190 -4.3116 402.0770 406.3886 368.3585 449.0179 -4.3052 401.8751 406.1803 368.1678 450.6336 -4.3007 401.6868 405.9875 367.9543 452.2498 -4.2969 401.4740 405.7709 367.7399 453.8488 -4.2905 401.2845 405.5750 367.5427 455.4626 -4.2865 401.0699 405.3564 367.3470 457.0616 -4.2824 400.8744 405.1567 367.1367 458.6606 -4.2764 400.6822 404.9586 366.9364 460.2834 -4.2703 400.4644 404.7347 366.7436 461.9019 -4.2651 400.2522 404.5173 366.5350 463.5008 -4.2600 400.0587 404.3187 366.3407 465.1010 -4.2543 399.8671 404.1214 366.1603 466.7155 -4.2462 399.6530 403.8992 365.9627 468.3295 -4.2411 399.4565 403.6976 365.7676 469.9434 -4.2363 399.2519 403.4882 365.5666 471.5378 -4.2284 399.0484 403.2768 365.3662 473.1444 -4.2244 398.8561 403.0805 365.1492 474.7360 -4.2210 398.6505 402.8716 364.9411 476.3434 -4.2168 398.4460 402.6628 364.7176 477.9524 -4.2133 398.2529 402.4662 364.5059 479.5640 -4.2073 398.0520 402.2594 364.2835 481.1619 -4.2013 397.8472 402.0485 364.0811 482.7605 -4.1970 397.6310 401.8280 363.8554 484.3745 -4.1917 397.4405 401.6322 363.6428 485.9890 -4.1854 397.2369 401.4223 363.4337 487.5885 -4.1793 397.0454 401.2247 363.2181 489.2023 -4.1742 396.8412 401.0154 363.0011 490.8018 -4.1670 396.6255 400.7926 362.7975 492.4159 -4.1601 396.4148 400.5750 362.5865 494.0298 -4.1543 396.2160 400.3703 362.3660 495.6300 -4.1500 396.0203 400.1704 362.1627 497.2456 -4.1402 395.8016 399.9418 361.9447 498.8446 -4.1329 395.6060 399.7388 361.7348 500.4605 -4.1276 395.4041 399.5317 361.5361 502.0875 -4.1247 395.1999 399.3246 361.3267 503.6810 -4.1172 394.9871 399.1043 361.1138 505.2726 -4.1107 394.7901 398.9008 360.9072 506.8806 -4.1075 394.5973 398.7048 360.6971 508.4878 -4.1041 394.3953 398.4994 360.4989 510.0968 -4.0996 394.2015 398.3011 360.2999 511.6953 -4.0947 393.9783 398.0730 360.0932 513.2956 -4.0886 393.7946 397.8831 359.8972 514.9096 -4.0841 393.5789 397.6631 359.6969 516.5086 -4.0800 393.3787 397.4588 359.4866 518.1378 -4.0734 393.1630 397.2364 359.2947 519.7366 -4.0681 392.9685 397.0367 359.0815 521.3505 -4.0637 392.7734 396.8370 358.8844 522.9495 -4.0573 392.5710 396.6283 358.6929 524.5635 -4.0519 392.3491 396.4010 358.4940 526.1775 -4.0467 392.1451 396.1917 358.2945 527.7765 -4.0435 391.9535 395.9970 358.0948 529.3909 -4.0361 391.7460 395.7821 357.8902 530.9905 -4.0287 391.5342 395.5630 357.6905 532.6201 -4.0259 391.3355 395.3615 357.4894 534.2193 -4.0199 391.1340 395.1539 357.2680 535.8275 -4.0147 390.9366 394.9513 357.0420 537.4194 -4.0077 390.7299 394.7376 356.8268 539.0120 -4.0036 390.5133 394.5169 356.6212 540.6360 -3.9981 390.3155 394.3135 356.4004 542.2446 -3.9895 390.1179 394.1074 356.1851 543.8416 -3.9871 389.9139 393.9010 355.9653 545.4401 -3.9824 389.7198 393.7022 355.7581 547.0389 -3.9761 389.5004 393.4764 355.5356 548.6680 -3.9694 389.3070 393.2764 355.3306 550.2668 -3.9638 389.1034 393.0672 355.1139 551.8809 -3.9575 388.8979 392.8554 354.9124 553.4796 -3.9521 388.7030 392.6551 354.6947 555.0936 -3.9470 388.4919 392.4389 354.4870 556.7228 -3.9382 388.2820 392.2202 354.2641 558.3218 -3.9360 388.0846 392.0206 354.0590 559.9219 -3.9284 387.8812 391.8096 353.8499 561.5366 -3.9241 387.6794 391.6035 353.6397 563.1355 -3.9179 387.4779 391.3958 353.4325 564.7645 -3.9141 387.2630 391.1771 353.2237 566.3626 -3.9075 387.0770 390.9845 353.0247 567.9565 -3.9020 386.8642 390.7662 352.8108 569.5660 -3.8958 386.6558 390.5516 352.6110 571.1586 -3.8893 386.4485 390.3378 352.4063 572.7829 -3.8825 386.2453 390.1279 352.2005 574.3785 -3.8771 386.0456 389.9227 351.9928 575.9765 -3.8716 385.8441 389.7156 351.7855 577.5905 -3.8662 385.6345 389.5007 351.5913 579.1895 -3.8613 385.4233 389.2846 351.3852 580.8185 -3.8530 385.2148 389.0678 351.1818 582.4175 -3.8478 385.0177 388.8655 350.9776 584.0165 -3.8428 384.8104 388.6532 350.7939 585.6305 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